AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT

Overcoming Quality Challenges for Automotive T6 Heat Treating

/ ALUMINUM PROCESSING TECHNICAL CONTENT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, INSTRUMENTATION TECHNICAL CONTENT

Three elements in the T6 aluminum heat treatment process — high temperature solution heat treatment, drastic temperature change in the water quench, and a long age hardening process — challenge accurate temperature monitoring. Thru-process technology gives in-house heat treaters the power to control these variables to overcome the unknowns. In the following Technical Tuesday article, Dr. Steve Offley, “Dr. O”, product marketing manager at PhoenixTM, examines the path forward through the challenges of aluminum heat treating.

This informative piece was first released in Heat Treat Today’s August 2024 Automotive print edition.

Aluminum Processing Growth

In today’s automotive and general manufacturing markets, aluminum is increasingly becoming the material of choice, being lighter, safer, and more sustainable. Manufacturers looking to replace existing materials with aluminum are needing new methodology to prove that thermal processing of aluminum parts and products is done to specification, efficiently and economically.

To add strength to pure aluminum, alloys are developed by the addition of elements dissolved into solid solutions employing the T6 heat treatment process (Figure 1). The alloy atoms create obstacles to dislocate movement of aluminum atoms through the aluminum matrix. This gives more structural integrity and strength.

FIgure 1. Critical temperature phase transitions of the T6 aluminum heat treatment process
Source: PhoenixTM

Process temperature control and uniformity is critical to the success of T6 heat treat to maximize the solubility of hardening solutes such as copper, magnesium, silicon, and zinc without exceeding the eutectic melting temperature. With a temperature difference of typically 9–15°F, knowing the accurate temperature of the product is essential. Control of the later quench process (Figure 1, Phase 3) is also critical not only to facilitate the alloy element precipitation phase but also to prevent unwanted part distortion/warping and risk of quench cracking.

T6 Process Monitoring Challenges

The T6 solution reheat process comes with many technical challenges where temperature profiling is concerned. The need to monitor all three of the equally important phases — solution treatment, quench, and the age hardening process — makes the trailing thermocouple methodology impossible.

Figure 2. Thru-process temperature monitoring of the three T6 heat treatment phases
Source: PhoenixTM

Even when considering applying thru-process temperature profiling technology, sending the data logger through the process, protected in a thermal barrier (Figure 2), the T6 heat treat process comes with significant challenges. A system will not only need to protect against heat (up to 1020°F) over a long process duration but also withstand the rigors of being plunged into a water quench. Rapid temperature transitions create elevated risk of distortion and warping which need to be addressed to give a reliable and robust monitoring solution.

Certain monitoring systems can provide protection to the data logger at 1022°F for up to 20 hours (Figure 3).

Figure 3. Thru-process temperature profiling system installed in the product cage monitoring the T6 heat treatment (solution treatment, quench, and age hardening) of aluminum engine blocks

Thermal Protection Technology

To meet the challenges of the T6 heat treat process, the conventional thermal barrier design employing microporous insulation is replaced with a water tank design, with thermal protection using an evaporative phase change temperature control principle. Evaporative technology uses boiling water to keep the high temperature data logger (maximum operating temperature of 230°F) at a stable operating temperature of 212°F as the water changes phase from liquid to steam. The advantage of evaporative technology is that a physically smaller barrier is often possible. It is estimated that with a like for like size (volume) and weight, an evaporative barrier will provide in the region of twice the thermal protection of a standard thermal barrier with microporous insulation and heat sink. The level of thermal protection can be adjusted by changing the capacity of the water tank and the volume of water. Increasing the volume of water increases the duration at which the T6 temperature barrier will maintain the data logger temperature of 212°F before it is depleted by evaporation losses.

The TS06 thermal barrier design (Figure 4) incorporates a further level of protection with an outer layer of insulation blanket contained within a structural outer metal cage. The key role of this material is to act as an insulative layer around the water tank to reduce the risk of structural distortion from rapid temperature changes both positive and negative in the T6 process.

Figure 4. TS06 thermal barrier design showing water tank, housing the data logger at its core, installed within structural frame containing the insulation blanket surface layer; water tank shown with traditional compression fitting face plate seal
Source: PhoenixTM

Obviously, the evaporative loss rate of water is governed by the water tank geometry. A cube shaped tank will provide the best performance, but this may need to be adapted to meet process height restrictions. A TS06 thermal barrier with dimensions 8.5 x 18.6 x 25.2 inches (H x W x L) offering a water capacity of 3.5 US gallons provides 11 hours of protection at 1022°F. A larger TS06 with approximately twice the capacity 12.2 x 18.6 x 25.2 inches (H x W x L) and 7.7 US gallons gives approximately twice the protection (20 hours at 1022°F).

Innovative IP67 Sealing Design

Passing through the water quench, the data logger needs to be protected from water damage. This is achieved in the system design by combining a fully IP67 sealed data logger case and water tank front face plate through which the thermocouples exit. Traditionally in heat treatment applications, mineral insulated thermocouples are sealed using robust metal compression fittings. Although reliable, the compression seals are difficult to use, requiring long set-up times. The whole uncoiled straight cable length must be passed through the tight fitting which, for the 10 x 13 ft thermocouples, takes some patience. Thermocouples can be used and installed for multiple runs, if undamaged. Unfortunately, as the ferrule in the compression fitting bites into the MI cable, removal of the cable requires the thermocouple to be cut, preventing reuse.

To overcome the frustrations of compression fitting, an alternative innovative thermocouple sealing mechanism has been designed for use on the T6 thermal barrier (Figure 5).

Figure 5. TS06 thermal barrier IP67 bi-directional rubber gasket seal; installation of mineral-insulated (MI) thermocouples and RF antenna aerial

Thermocouples can be slotted easily and quickly, tool free, into a precision cut rubber gasket without any need to uncoil the thermocouple completely. The rubber gasket has a unique bi-directional seal, allowing both sealing of each thermocouple but also sealing of the clamp face plate to the data logger tray, which is then secured to the water tank with a further silicone gasket seal. The new seal design allows thermocouples to be uninstalled and reused, reducing operating costs significantly.

Accurate Process Data considerations

The T6 applications come with a series of monitoring challenges which need to be considered carefully to guarantee the quality of the data obtained. Although the complete process time of the three phases can reach up to 10 hours, it is necessary to use a rapid sample interval (seconds) to provide a sufficient resolution. The data logger is designed to facilitate this with a minimum sample interval of 0.2 seconds over 20 channels and memory size of 3.8 million data points, allowing complete monitoring of the entire process. A sample interval of 0.2 seconds provides sufficient data points on the rapid quench cooling curve. The high resolution allows full analysis and optimization of the quench rate to achieve required metallurgical transitions yet avoid distortion or quench cracking risks.

Employing the phased evaporation thermal barrier design, the high temperature data logger with maximum operating temperature of 230°F will operate safely at 212°F. During the profile run, the data logger internal temperature will increase from ambient temperature to 212°F. To allow the thermocouple to accurately record temperature, the data logger offers a sophisticated cold junction compensation method, correcting the thermocouple read out (hot junction) for anticipated internal data logger temperature changes.

Data logger and thermocouple calibration data covering the complete measurement range (not just a single designated temperature) can be used to create detailed correction factor files. Correction factors are calculated by interpolation between two known calibration points using the linear method as approved by CQI-9 and AMS2750G. This method ensures that all profile data is corrected to the highest possible accuracy. 

Addressing Real-Time, Thru-Process Temperature Monitoring Challenges

For a process time as long as the T6, real-time monitoring capability is a significant benefit. The unique two-way RF telemetry system used on the PhoenixTM system helps address the technical challenges of the three separate stages of the process. The RF signal can be transmitted from the data logger through a series of routers linked back to the main coordinator connected to the monitoring PC. The wirelessly connected routers are located at convenient points in the process (solution treatment furnace, quench tank, aging furnace) to capture all live data without any inconvenience of routing communication cables.

A major challenge in the T6 process is the quench step from an RF telemetry perspective. An RF signal cannot escape from water in the quench tank. To overcome this limitation, a “catch up” feature is implemented. Once the system exits the quench and the RF signal is re-established, any previously missing data is retransmitted guaranteeing full process coverage.

Process Quality Assurance and Validation

In the automotive industry, many operations will be working to the CQI-9 special process heat treat system assessment accreditation. As defined by the pyrometry standard, operators need to validate the accuracy and uniformity of the furnace work zone by employing a temperature uniformity survey (TUS).

The thru-process monitoring principle allows for an efficient method by which the TUS can be performed employing a TUS frame to position a defined number of thermocouples over the specific working zone of the furnace (product basket). As defined in the standard with particular reference to application assessment process Table C (aluminum heat treating), the uniformity for both the solution heat treatment and aging furnace needs to be proven to satisfy ±10°F of the threshold temperature during the soak time.

Complementing the TUS system, the Thermal View Survey software provides a means by which the full survey can be set up automatically allowing routine full analysis and reporting to the CQI-9 specification as shown in Figure 6.

Figure 6. View of TUS for T6 aluminum processing in Phase 1 Solution Re-heat
Source: PhoenixTM

Interestingly, a significant further benefit of the thru-process principle is that by collecting process data for the whole process, many of the additional requirements of the process Table C can be achieved with reference to the quench. From the profile trace, key criteria such as quench media temperature, quench delay time, and quench cooling curve can be measured and reported with full traceability during the production run.

Summary

To fully understand, control, and optimize the T6 heat treat process, it is essential the entire process is monitored. Thru-process monitoring solutions, designed specifically, allow not only product temperature profiling of all the solution heat treatment, water quench, and age hardening phases, but also comprehensive temperature uniformity surveying to comply with CQI-9.

About the Author:

Dr Steve Offley (“Dr O”), Product Marketing Manager, PhoenixTM

Dr. Steve Offley, “Dr. O,” has been the product marketing manager at PhoenixTM for the last five years after a career of over 25 years in temperature monitoring focusing on the heat treatment, paint, and general manufacturing industries. A key aspect of his role is the product management of the innovative PhoenixTM range of thru-process temperature and optical profiling and TUS monitoring system solutions.

For more information: Contact Steve at Steve.Offley@phoenixtm.com.

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Advantages of Laser Heat Treatment, Part 2: Energy Efficiency, Sustainability, and Precision

/ AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, FEATURED NEWS, HARDENING TECHNICAL CONTENT, OP-ED

A discussion of laser heat treating begun in Heat Treat Today’s Air & Atmosphere 2024 print edition would not be complete without highlighting key sustainability advantages of this new technology. In this Technical Tuesday installment, guest columnist Aravind Jonnalagada (AJ), CTO and co-founder of Synergy Additive Manufacturing LLC, explores how sustainability and energy-efficiency are driven by precision heat application and minimal to zero distortion. The first part, “Advantages of Laser Heat Treatment: Precision, Consistency, and Cost Savings”, appeared on April 2, 2024, in Heat Treat Today, as well as in Heat Treat Today’s January/February 2024 Air & Atmosphere print edition.

This informative piece was first released in Heat Treat Today’s May 2024 Sustainability Heat Treat print edition.

Laser heat treating is a transformative process that promises superior performance and sustainable practices. Laser heat treating epitomizes precision in surface heat treatment techniques, targeting localized heating of steel or cast-iron components. Laser radiation raises the surface temperature of the metal in the range of 1652°F to 2552°F (900°C to 1400°C), inducing a transformation from ferritic to austenitic structure on the metal surface. As the laser beam traverses the material, the bulk of the component self-quenches the heated zone. During this process, carbon particles are deposited in the high temperature lattice structure and cannot diffuse outward because of quick cool down resulting in the formation of hard martensite to a case depth up to 0.080” (2 mm), crucial for enhancing material properties.

Sustainability through Energy Efficiency

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When considering the energy consumption of a typical laser heat treating operation, it’s essential to acknowledge the continuous advancements in laser technology. Modern laser heat treating systems integrate high-power lasers, water chillers, and motion systems, such as robots or CNC machines. With a typical wall plug efficiency of around 50% for diode lasers, these systems represent a significant improvement in energy utilization compared to conventional methods. The typical energy consumption cost for running a 6 kW laser heat treating system is $20-$30/day. The calculation is based on an 8-hour shift with a duty cycle of 80% calculated at national average electric cost of 15.45 cents/kilowatt-hour.

Self-Quenching Mechanism

Laser heat treating operates on the essential principle of self-quenching, leveraging the bulk mass of the material for rapid cooling. This eliminates the dependence on quenchants required in flame and induction heat treating processes, further reducing environmental impact and operational costs.

Precision and Minimal Distortion

At the heart of laser heat treating lies its sustainable and energy-efficient attributes, driven by two fundamental features: precision heat application and minimal to zero distortion of components post-heat treatment. When compared to the conventional methods such as flame and induction hardening, laser heat treatment offers significantly localized heating. This precision allows for targeted heat treatment within millimeter precision right where the hardness is needed, optimizing energy utilization and operational efficiency. Furthermore, the high-power density of lasers enables hardening with minimal to zero distortion, eliminating or reducing the need for subsequent machining operations like hard milling or grinding.

Case Study image; 16 small boxes of auto parts undergoing die machining, laser heat treat; blue inset box
Comparison of the die construction process before and after laser hardening
Source: Autodie LLC

A Case Study of Laser Heat Treating in Automotive Stamping Dies

The image above identifies process steps typically involved in construction of automotive stamping dies. During the process of manufacturing automotive stamping dies, the cast dies are first soft milled, intentionally leaving between 0.015” and 0.020” of extra stock material on the milled surfaces. This is done to account for any distortions that will result from the subsequent conventional heat treatment processes such as flame or induction. After heat treating, the dies are then hard milled back to tolerance and assembled.

In the laser heat treating process, by contrast, dies are finish machined to final tolerance in the first step and then laser heat treated without distortion. No secondary hard milling operation is necessary. Typical cost savings for our automotive tool and die customer exceeds over 20% due to elimination of hard milling operation. Total energy reduction is significant, although not computed here. This may result in savings if carbon credits become monetized.

Laser heat treating’s precision, efficiency, and minimal environmental footprint position it as an environmentally friendly option for heat treat operations. As industries continue to prioritize sustainability, laser heat treating may set new standards for excellence and environmental stewardship.

About the Author:

Aravind Jonnalagadda
CTO and Co-Founder
Synergy Additive Manufacturing LLC
Source: LinkedIn

Aravind Jonnalagadda (AJ) is the CTO and co-founder of Synergy Additive Manufacturing LLC. With over 15 years of experience, AJ and Synergy Additive Manufacturing LLC provide high-level laser systems and laser heat treating, specializing in high power laser-based solutions for complex manufacturing challenges related to wear, corrosion, and tool life. Synergy provides laser systems and job shop services for laser heat treating, metal based additive manufacturing, and laser welding.

For more information: Contact AJ at aravind@synergyadditive.com or synergyadditive.com/laser-heat-treating.

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All About the Quench and Keeping Cool: Thru-process Temp Monitoring and Gas Carburizing

/ ATMOSPHERE AIR FURNACES TECHNICAL CONTENT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, CARBURIZING, CARBURIZING TECHNICAL CONTENT, CONTROLS, CONTROLS TECHNICAL CONTENT, FEATURED NEWS, QUENCHING TECHNICAL CONTENT

The future of heat treating requires new manufacturing solutions like robotics that can work with modular design. Yet so also does temperature monitoring need to be seamless to know how effectively your components are being heat treated — especially through being quenched. In this Technical Tuesday, learn more about temperature monitoring through the quench process.

Gas Carburization

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Carburizing has rapidly become one of the most critical heat treatment processes employed in the manufacture of automotive components. Also referred to as case hardening, it provides necessary surface resistance to wear, while maintaining toughness and core strength essential for hardworking automotive parts.

Figure 1. Typical carburizing heat treat temperature profile showing the critical temperature/time steps: (i) carburization, (ii) quench, and (iii) temper. (Source: PhoenixTM)

The carburizing process is achieved by heat treating the product in a carbon rich environment (Figure 1), typically at a temperature of 1562°F–1922°F (850°C–1050°C). The temperature and process time significantly influence the depth of carbon diffusion and other related surface characteristics. Critical to the process is a rapid quenching of the product following the diffusion in which the temperature is rapidly decreased to generate the microstructure, giving the enhanced surface hardness while maintaining a soft and tough product core.

The outer surface becomes hard via the transformation from austenite to martensite while the core remains soft and tough as a ferritic and/or pearlitic microstructure. Normally, carburized microstructures following quench are further tempered at temperatures of about 356°F (180°C) to transform some of the brittle martensite into tempered martensite to enhance ductility and grindability.

Critical Process Temperature Control

As discussed, the success of carburization is dependent on accurate, repeatable control of the product temperature and time at that temperature through the complete heat treatment process. Important to the whole operation is the quench, in which the rate of cooling (product temperature change) is critical to achieve the desired changes in microstructure, creating the surface hardness. It is interesting that the success of the whole heat treat process can rest on a process step which is so short (minutes), in terms of the complete heat teat process (hours). Getting the quench correct is not only essential to achieve the desired metal microstructure, but also to ensure that the physical dimensions and shape of the product are maintained (no distortion/warping) and issues such as quench cracking are eliminated.

Obviously, as the quench is so critical to the whole heat treat process, the correct quench selection needs to be made to achieve the optimum properties with acceptable levels of dimensional change. Many different quenchants can be applied with differing quenching performances. The rate of heat transfer (quench rate) of quench media in general follows this order from slowest to quickest: air, salt, polymer, oil, caustic, and water.

Technology Challenges for Temperature Monitoring

When considering carburization from an industry standpoint, furnace heat treat technology generally falls into one of two camps, embracing either air quench (low pressure carburization) or oil quench (sealed gas carburization/LPC with integral or vacuum oil quench). Although each achieves the same end goal, the heat treat mechanisms and technologies employed are very different, as are the temperature monitoring challenges.

To achieve the desired carburized product, it is necessary to control and hence monitor the product temperature through the three phases of the heat treat process. Conventionally, product temperature monitoring would be attempted using the traditional trailing thermocouple method. For many modern heat treat processes including carburization, the trailing thermocouple method is difficult and often practically impossible.1 The movement of the product or product basket from stage to stage, often from one independent sealed chamber to another (lateral or vertical movement), makes the monitoring of the complete process a significant challenge.

With the industry driving toward fully automated manufacturing, furnace manufacturers are now offering the complete package with full robotic product loading that includes shuttle transfer systems and modular heat treat phases to process both complete product baskets and single piece operations. Although trailing thermocouples may allow individual stages in the process to be measured, they cannot provide monitoring of the complete heat treat journey. Testing is therefore not under true normal production conditions, and therefore is not an accurate record of what happens in normal day to day operation.

Figure 2 shows schematic diagrams of two typical carburizing furnace configurations that would not be possible to monitor using trailing thermocouples. The first shows a modular batch furnace system where the product basket is transferred between each static heat treat operation (preheat, carburizing furnace, cooling station, quench, quench wash, temper furnace) via a charge transfer cart. The second shows the same heat treat operation but performed in a continuous indexed pusher furnace configuration where the product basket moves sequentially through each heat treat operation in a semi-continuous flow.

Figure 2.1. Modular batch furnace system (Source: PhoenixTM)
Figure 2.2. Continuous pusher furnace schematic (Source: PhoenixTM)

Thru-process temperature monitoring as a technique overcomes such technical restrictions. The data logger is protected by a specially designed thermal barrier, therefore, can travel with the product through each stage of the process measuring the product/process temperature with short, localized thermocouples that will not hinder travel. The careful design and construction of the monitoring system is important to address the specific challenges that different heat treat technology brings including modular batch and continuous pusher furnace designs (Figure 2).2

The following section will focus specifically on monitoring challenges of the sealed gas carburizing process with integral oil quench. Technical challenges of the alternative low pressure carburizing technology with high pressure gas quench have previously been discussed in an earlier publication.3

Monitoring Challenges of Sealed Gas Carburization — Oil Quench

Figure 3. “Thru-process” temperature monitoring system for use in a sealed carburizing furnace with integral oil quench — (3.1) Monitoring system entering furnace with thermocouple fixed to automotive gears, product test pieces (3.2) System exiting oil quench tank (3.3) System inserted into wash tank with product basket (Source: PhoenixTM)

Presently, the most common traditional method of gas carburizing for automotive steels is often referred to as sealed gas carburizing. In this method, the parts are surrounded by an endothermic gas atmosphere. Carbon is generated by the Boudouard reaction during the carburization process, typically at 1562°F–1832°F (850°C –1000°C). Despite the dramatic appearance of a sealed gas carburizing furnace, with its characteristic belching flames (Figure 3), from a monitoring perspective, the most challenging aspect of the process is not the heating, but the oil quench cooling. For such furnace technology, the historic limitation of “thru-process” temperature profiling has been the need to bypass the oil quench and wash stations, missing a critical process step from the monitoring operation. Obviously, passing a conventional hot barrier through an oil quench creates potential risk of both system damage from oil ingress and barrier distortion, as well as general process safety. However, the need to bypass the quench in certain furnace configurations by removing the hot system from the confined furnace space could create significant operational challenges, from an access and safety perspective.

Monitoring of the quench is important as ageing of the oil results in decomposition (thermal cracking), oxidation, and contamination (e.g. water) of the oil, all of which degrade the viscosity, heat transfer characteristics, and quench efficiency. Control of physical oil temperature and agitation rates is also key to oil quench performance. Quench monitoring allows economic oil replacement schedules to be set, without risk to process performance and product quality.

Figure 4. “Thru-process” temperature monitoring system oil quench compatible thermal barrier design: (1) Robust outer structural frame keeping insulation and inner barrier secure; (2) Internal thermal barrier — completely sealed with integral microporous insulation protecting data logger; (3) Mineral insulated thermocouples sealed in internal thermal barrier with oil tight compression fitting; (4) Multi-channel high temperature data logger; and (5) Sacrificial insulation blocks replaced after each run. (Source: PhoenixTM)

To address the process challenges, a unique thermal barrier design has been developed that both protects the data logger in the furnace (typically three hours at 1697°F/925°C) and also protects during transfer through the oil quench (typically 15 mins) and final wash station (Figure 3). The key to the barrier design is the encasement of a sealed inner barrier with its own thermal protection with blocks of high-grade sacrificial insulation contained in a robust outer structural frame (Figure 4).

Quench Cooling Phases

Monitoring the oil quench in carburization gives the operator a unique insight into the product’s specific cooling characteristics, which can be critical to allow optimal product loading and process understanding and optimization. From a scientific perspective, the quench temperature profile trace, although only a couple of minutes in duration, is complex and unique. From a zoomed in quench trace (Figure 5) taken from a complete carburizing profile run, the three unique heat transfer phases making up the oil quench cool curve can be clearly identified:

Figure 5. Oil quench temperature profile for different locations on an automotive gear test piece shows the three distinct heat transfer phases: (1) film boiling “vapor blanket”, (2) nucleate boiling, and (3) convective heat transfer. (Source: PhoenixTM)
  1. Film boiling “vapor Blanket”: The oil quenchant creates a layer of vapor (Leidenfrost phenomenon) covering the metal surface. Cooling in this stage is a function of conduction through the vapor envelope. Slow cool rate since the vapor blanket acts as an insulator.
  2. Nucleate boiling: As the part cools, the vapor blanket collapses and nucleate boiling results. Heat transfer is fastest during this phase, typically two orders of magnitude higher than in film boiling.
  3. Convective heat transfer: When the part temperature drops below the oil boiling point. the cooling rate slows significantly. The cooling rate is exponentially dependent on the oil’s viscosity.

From a heat treat perspective, the quench step relative to the whole process (hours) is quick (seconds), but it is probably the most critical to the performance of the metallurgical phase transitions and achieving the desired core microstructure of the product without risk of distortion. By being able to monitor the quench step, the process can be validated for different products with differing size, form, and thermal mass. As shown in Figure 6, the quench curve profile over the three heat transfer phases is very different for two different automotive gear sizes.

Figure 6. Oil quench temperature profile for different automotive gear sizes (20MnCr5 case hardening steel) with different thermal masses: Passenger Car Gear (2.2 lbs) and Commercial Vehicle Gear (17.6 lbs) (Source: PhoenixTM)

Summary

As discussed in this article, one of the key process performance factors associated with gas carburization is the control and monitoring of the product quench step. Employing an oil quench, the measurement of such operation is now very feasible as part of heat treat monitoring. Innovations in thru-process temperature profiling technology offer specific system designs to meet the respective application challenges.

References

[1] Dr. Steve Offley, “The light at the end of the tunnel – Monitoring Mesh Belt Furnaces,” Heat Treat Today, February 2022, https://www.heattreattoday.com/processes/brazing/brazing-technical-content/the-light-at-the-end-of-the-tunnel-monitoring-mesh-belt-furnaces/.

[2] Michael Mouilleseaux, “Heat Treat Radio #102: Lunch & Learn, Batch IQ Vs. Continuous Pusher, Part 1,” interviewed by Doug Glenn, Heat Treat Radio, October 26, 2023, audio, https://www.heattreattoday.com/media-category/heat-treat-radio/heat-treat-radio-102-102-lunch-learn-batch-iq-vs-continuous-pusher-part-1/.

[3] Dr. Steve Offley, “Discover the DNA of Automotive Heat Treat: Thru-process Temperature Monitoring,” Heat Treat Today, August 2023, https://www.heattreattoday.com/discover-the-dna-of-automotive-heat-treat-thru-process-temperature-monitoring/.

About the Author

Dr Steve Offley (“Dr O”), Product Marketing Manager, PhoenixTM

Dr. Steve Offley, “Dr. O,” has been the product marketing manager at PhoenixTM for the last five years after a career of over 25 years in temperature monitoring focusing on the heat treatment, paint, and general manufacturing industries. A key aspect of his role is the product management of the innovative PhoenixTM range of thru-process temperature and optical profiling and TUS monitoring system solutions.

For more information: Contact Steve at Steve.Offley@phoenixtm.com.

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Advantages of Laser Heat Treatment: Precision, Consistency, and Cost Savings

/ AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, FEATURED NEWS, HARDENING TECHNICAL CONTENT, OP-ED

Laser heat treating, a form of case hardening, offers substantial advantages when distortion is a critical concern in manufacturing operations. Traditional heat treating processes often lead to metal distortion, necessitating additional post-finishing operations like hard milling or grinding to meet dimensional tolerances.

This Technical Tuesday article was originally published in first published in Heat Treat Today’s January/February 2024 Air & Atmosphere print edition.

In laser heat treating, a laser (typically with a spot size ranging from 0.5″ x 0.5″ to 2″ x 2″) is employed to illuminate the metal part’s surface. This results in a precise and rapid delivery of high-energy heat, elevating the metal’s surface to the desired transition temperature swiftly. The metal’s thermal mass facilitates rapid quenching of the heated region resulting in high hardness.

Key Benefits of Laser Heat Treating

Consistent Hardness Depth

Laser heat treatment achieves consistent hardness and hardness depth by precisely delivering high energy to the metal. Multiparameter, millisecond-speed feedback control of temperature ensures exacting specifications are met.

Minimal to Zero Distortion

Due to high-energy density, laser heat treatment inherently minimizes distortion. This feature is particularly advantageous for a variety of components ranging from large automotive dies to gears, bearings, and shafts resulting in minimal to zero distortion.

Precise Application of Beam Energy

Unlike conventional processes, the laser spot delivers heat precisely to the intended area, minimizing or eliminating heating of adjoining areas. This is specifically beneficial in surface wear applications, allowing the material to be hardened on the surface while leaving the rest in a medium-hard or soft state, giving the component both hardness and ductility.

Figure 1. Laser heat treating of automotive stamping die constructed from D6510 cast iron material (Source: Synergy Additive Manufacturing LLC)

No Hard Milling or Grinding Required

The low-to-zero-dimensional distortion of laser heat treatment reduces or eliminates the need for hard milling or grinding operations. Post heat treatment material removal is limited to small amounts removable by polishing. Eliminating hard milling or grinding operations saves substantial costs in the overall manufacturing process of the component. Our typical tool and die customers have seen over 20% cost savings by switching over to laser heat treating.

Figure 2. Laser heat treating of machine tool
components (Source: Synergy Additive Manufacturing LLC)

Applicable for a Large Variety of Materials

Any metal with 0.2% or more carbon content is laser heat treatable. Hardness on laser heat treated materials typically reaches the theoretical maximum limit of the material. Many commonly used steels and cast irons in automotive industry such as A2, S7, D2, H13, 4140, P20, D6510, G2500, etc. are routinely laser heat treated. A more exhaustive list of materials is available at synergyadditive.com/laser-heat-treating.

Conclusions

Aravind Jonnalagadda CTO and Co-Founder Synergy Additive Manufacturing LLC Source: LinkedIn

Laser heat treatment is poised to witness increased adoption in the automotive and other metal part manufacturing sectors. The adoption of this process faces no significant barriers, aside from the typical challenges encountered by emerging technologies, such as lack of familiarity, limited hard data, and a shortage of existing suppliers. The substantial savings, measured in terms of cost, schedule, quality, and energy reduction, provide robust support for the continued embrace of laser heat treatment in manufacturing processes.

For more information: Contact AJ at aravind@synergyadditive.com or synergyadditive.com/laser-heat-treating.

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Aluminum Extrusion Operations Bring Nitriding In-House

/ ALUMINUM PROCESSING NEWS, ATMOSPHERE AIR FURNACES NEWS, AUTOMOTIVE HEAT TREAT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, FEATURED NEWS, MANUFACTURING HEAT TREAT NEWS, NITRIDING, NITRIDING NEWS

Extral SP. Z o.o., a Polish company specializing in aluminum extrusions, has bolstered its manufacturing capabilities to better serve the construction, automobile, and machinery industries. Alongside acquiring a new aluminum extrusion press, the company ordered a nitriding system to nitride H11 and H13 extrusion dies of various sizes.

Nitriding pit furnace from Nitrex

The Nitrex turnkey nitriding system includes an NX-1015 pit-type furnace with a 2-ton (4410-lb) load capacity and NITREG® technology, offering nitriding treatments that optimize die performance and throughput while concurrently reducing tooling costs.

This investment coincides with Extral’s expansion of its operational footprint in Poland, including the construction of a new building to house the extrusion press and furnace. This expansion enables the company to diversify its range of extruded products while maintaining a focus on sustainability and energy efficiency. The new nitriding installation will contribute to these objectives by providing more efficient use of process gases and electricity.

Marcin Stokłosa
Project Manager
Nitrex Poland
Source: LinkedIn.com

Previously, Extral outsourced its nitriding operations to a local heat treater, due to quality issues encountered with an underperforming in-house nitriding unit. However, this latest investment enables them to bring nitriding operations back in-house, ensuring better control over the quality and consistency of their nitrided dies while also benefiting from expedited turnaround times.

Marcin Stoklosa, project manager at Nitrex, said, “Working with Extral on this project has been a pleasure. . . . Seeing customers invest in their business and achieve their goals, especially when it aligns with our values of innovation and sustainability, is always rewarding.”

This press release is available in its original form here.

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Common Automotive Heat Treat Processes To Get Into Gear

/ ANNEALING TECHNICAL CONTENT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, FEATURED NEWS, NITRIDING TECHNICAL CONTENT, NITROCARBURIZING TECHNICAL CONTENT, TEMPERING, TEMPERING TECHNICAL CONTENT

How long have you been heat treating automotive gears? Which thermal processing techniques do your operations gravitate towards? In this best of the web article, uncover some of the common heat treatment functions and the properties they create in gears. Let us know what you think of this general overview of the world of heat treating gears in our Reader Feedback form!

Contact us with your Reader Feedback!

Additionally, when you read to the end of the article, future trends that we can anticipate for heat treaters in the automotive industry are offered; as one might guess, they include digital and energy-saving technologies.

An excerpt: “Automotive gear heat treatment (process) includes two aspects: firstly, conventional heat treatment such as annealing, normalizing, quenching, tempering, and quenching and tempering; secondly, surface heat treatment, which encompasses methods like surface quenching (e.g., induction quenching, laser quenching) and chemical heat treatment (e.g., carburizing, carbonitriding, nitriding, nitrocarburizing).”

Read the entire article from Beyond Gears via LinkedIn, by clicking here: “Characteristics and Development Trends in Automotive Gear Heat Treatment“

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Thermal Loop Solutions, Part 1: A Path to Improved Performance and Compliance in Heat Treatment

/ AEROSPACE HEAT TREAT, AEROSPACE HEAT TREAT TECHNICAL CONTENT, ATMOSPHERE AIR FURNACES TECHNICAL CONTENT, AUTOMOTIVE HEAT TREAT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, CONTROLS TECHNICAL CONTENT

How often do you think about the intelligent designs controlling the thermal loop system behind your heat treat operations? With ever-advancing abilities to integrate and manage data for temperature measurement and power usage, the ability of heat treat operations to make practical, efficient, and energy-conscious change is stronger than ever. In part 1, understand several benefits of thermal loop systems and how they are leveraged to comply with industry regulations, like Nadcap.

This Technical Tuesday article by Peter Sherwin, global business development manager – Heat Treatment, and Thomas Ruecker, senior business development manager, at Watlow was originally published in Heat Treat Today’s January/February 2024 Air & Atmosphere Heat Treat print edition.

Introduction

Heat treatment processes are a crucial component of many manufacturing industries, and thermal loop solutions have become increasingly popular for achieving improved temperature control and consistent outcomes.

A thermal loop solution is a closed loop system with several essential components, including an electrical power supply, power controller, heating element, temperature sensor, and process controller. The electrical power supply provides the energy needed for heating, the power controller regulates the power output to the heating element, the heating element heats the material, and the temperature sensor measures the temperature. Finally, the process controller adjusts the power output to maintain the desired temperature for the specified duration, providing better temperature control and consistent outcomes.

Performance Benefits

Heat treatment thermal loop solutions offer several advantages over traditional heat treatment methods, including improved temperature control and increased efficiency. The thermal loop system provides precise temperature control, enabling faster heating and cooling and optimized soak times. In addition, the complete design of modern thermal loop solutions includes energy-efficient heating and overall ease of use.

Figure 1. Watlow Industry 4.0 solution (Source: Watlow)

Heat treatment thermal loop solutions are integrated with Industry 4.0 frameworks and data management systems to provide real-time information on performance. Combining artificial intelligence and machine learning algorithms can also provide additional performance benefits, such as the ability to analyze data and identify patterns for further optimization. Ongoing performance losses in a heat treatment system typically come from process drift s. Industry 4.0 solutions can explore these drift s and provide opportunities to minimize these deviations.

Heat treatment thermal loop solutions can be optimized using Failure Mode and Effects Analysis (FMEA). FMEA is a proactive approach to identifying potential failure modes and their effects, allowing organizations to minimize the risk of process disruptions and improve the overall efficiency of their heat treatment processes. Historically, this was a tabletop exercise conducted once per year with a diverse team from across the organization. Updates to this static document were infrequent and were primarily based on organization memory rather than being automatically populated in real time with actual data. There is a potential to produce “live” FMEAs utilizing today’s technology and leveraging insights for continuous improvement.

Th e effectiveness of heat treatment thermal loop solutions can be measured using metrics such as overall equipment effectiveness (OEE). OEE combines metrics for availability, performance, and quality to provide a comprehensive view of the efficiency of a manufacturing process. By tracking OEE and contextual data, organizations can evaluate the effectiveness of their heat treatment thermal loop solutions and make informed decisions about optimizing their operations.

Regulatory Compliance

Nadcap (National Aerospace and Defense Contractors Accreditation Program) is an industry-driven program that provides accreditation for special processes in the aerospace and defense industries. Heat treatment is considered a “special process” under Nadcap because it has specific characteristics crucial to aerospace and defense components’ quality, safety, and performance. Th ese characteristics include:

  • Process sensitivity: Heat treatment processes involve precise control of temperature, time, and atmosphere to achieve the desired material properties. Minor variations in these parameters can significantly change the mechanical and metallurgical properties of the treated components. This sensitivity makes heat treatment a critical process in the aerospace and defense industries.
  • Limited traceability: Heat treatment processes typically result in changes to the material’s microstructure, which are not easily detectable through visual inspection or non-destructive testing methods. Th is limited traceability makes it crucial to have strict process controls to ensure the desired outcome is achieved consistently.
  • Critical performance requirements: Aerospace and defense components often have strict performance requirements due to the extreme conditions in which they operate, such as high temperatures, high loads, or corrosive environments. The heat treatment process ensures that these components meet the specifications and can withstand these demanding conditions.
  • High risk: The failure of a critical component in the aerospace or defense sector can result in catastrophic consequences, including loss of life, significant financial loss, and reputational damage. Ensuring that heat treatment processes meet stringent quality and safety standards is essential to mitigate these risks.

Nadcap heat treatment accreditation ensures suppliers meet industry standards January/February and best practices for heat treatment processes. The accreditation process includes rigorous audits, thorough documentation, and ongoing process control monitoring to maintain high quality, safety, and performance levels.

The aerospace industry’s AMS2750G pyrometry specification and the automotive industry’s CQI-9 4th Edition regulations are crucial for ensuring consistent and high-quality heat treated components. Adherence to these regulations is essential for meeting the stringent quality requirements of the aerospace and automotive industries and other industries with demanding specifications.

Temperature uniformity is a crucial requirement of both AMS2750G and CQI-9 4th Edition, mandating specific temperature uniformity requirements for heat treating furnaces to ensure the desired mechanical properties are achieved throughout the treated components. AMS2750G class 1 furnaces with strict uniformity requirements +/-5°F (+/-3°C) provide both quality output and predictable energy use. However, maintaining this uniformity requires significant maintenance oversight due to all the components involved in the thermal loop.

Calibration and testing procedures are specified in the standards to help ensure the accuracy and reliability of the temperature control systems used in heat treat processes.

Detailed process documentation is required by AMS2750G and CQI-9 4th Edition, including temperature uniformity surveys, calibration records, and furnace classifications. This documentation ensures traceability, enabling manufacturers to verify that the heat treat process is consistently controlled and meets the required specifications.

Figure 2. Eurotherm data reviewer (Source: Watlow)

Modern data platforms enable the efficient collection of secure raw data (tamper-evident) and provide the replay and reporting necessary to meet the standards.

The newer platforms also offer the latest industry communication protocols – like MQTT and OPC UA (Open Platform Communications Unified Architecture) – to ease data transfer across enterprise systems.

MQTT is a lightweight, publish-subscribe-based messaging protocol for resource-constrained devices and low-bandwidth, high-latency, or unreliable networks. IBM developed it in the late 1990s, and it has become a popular choice for IoT applications due to its simplicity and efficiency. MQTT uses a central broker to manage the communication between devices, which publish data to “topics,” and subscribe to topics that they want to receive updates on.

OPC UA is a platform-independent, service-oriented architecture (SOA) developed by the OPC Foundation. It provides a unified framework for industrial automation and facilitates secure, reliable, and efficient communication between devices, controllers, and software applications. OPC UA is designed to be interoperable across multiple platforms and operating systems, allowing for seamless integration of devices and systems from different vendors. The importance of personnel and training is emphasized by CQI-9 4th Edition, which requires manufacturers to establish training programs and maintain records of personnel qualifications to ensure that individuals responsible for heat treat processes are knowledgeable and competent. With touchscreen and mobile integration, a significant development in process controls has occurred over the last decade.

Figure 3. Watlow F4T® touchscreen and Watlow PM PLUS™ EZ-LINK®
mobile application

By integrating these regulations into a precision control loop, heat treatment thermal loop solutions can provide the necessary level of control and ensure compliance with AMS2750G and CQI-9 4th Edition, leading to the production of high-quality heat treated components that meet performance requirements and safety standards.

Continuous improvement is also emphasized by both AMS2750G and CQI-9 4th Edition, requiring manufacturers to establish a system for monitoring, measuring, and analyzing the performance of their heat treatment systems. This development enables manufacturers to identify areas for improvement and implement corrective actions, ensuring that heat treat processes are continuously improving and meeting the necessary performance and safety standards.

To Be Continued in Part 2

In part 2 of this article, we’ll consider the improved sustainability outcomes, potential challenges and limitations, and the promising future this technology offers to the heat treat industry.

About the Authors

Peter Sherwin, Global Business Development Manager – Heat Treatment, Watlow
Thomas Ruecker, Senior Business Development Manager, Watlow

Peter Sherwin is a global business development manager of Heat Treatment for Watlow and is passionate about offering best-in-class solutions to the heat treatment industry. He is a chartered engineer and a recognized expert in heat treatment control and data solutions.

Thomas Ruecker is the business development manager of Heat Treatment at Eurotherm Germany, a Watlow company. His expertise includes concept development for the automation of heat treatment plants, with a focus on aerospace and automotive industry according to existing regulations (AMS2750, CQI-9).

For more information: Contact peter.sherwin@watlow.com or thomas.ruecker@watlow.com.

This article content is used with the permission of heat processing, which published this article in 2023.

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“Quench” Your Thirst: 3 Technical Articles To Satisfy Your Needs

/ AUTOMOTIVE HEAT TREAT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, FEATURED NEWS, MANUFACTURING HEAT TREAT, MANUFACTURING HEAT TREAT TECH, QUENCHING TECHNICAL CONTENT

Thirsting for knowledge about quenching, but not sure where to start? Heat Treat Today has coalesced technical information across articles and podcast episodes from key experts, including significant quenching methods, innovative developments with quenching, and how to control temperature during the process.

Discover more about these three topics in today’s Technical Tuesday original content feature.

Monitor Quench Temperatures with Unique Thermal Barrier Designs

Automotive heat treating operations require repeatable operations to ensure that the composite parts within an automobile perform reliably. Steve Offley, also known as “Dr. O," the product marketing manager at PhoenixTM, outlines case studies of several temperature-critical operations to demonstrate how unique thermal barrier design for thru-process monitoring systems can solve temperature measuring problems. These processes include sealed gas carburizing into an integrated oil quench as well as LPC followed by transfer to a sealed high-pressure gas quench chamber.

Offley comments on the quenching process following LPC, saying, "During the gas quench, the [thermal] barrier [for temperature monitoring] needs to be protected from Nitrogen N2(g) or Helium He(g) gas pressures up to 20 bar." If you are facing heat treat processing with integrated quench, learn more about this temperature monitoring solution.

Read the full article here: Discover the DNA of Automotive Heat Treat: Thru-Process Temperature Monitoring

Intensive Quenching: An Answer for a "Greener" Heat Treat? 

Gas furnaces have the potential to be a significant source of carbon emissions in many essential heat treat processes. However, an innovative approach combining induction through heating with intensive quenching could be one answer for greener heat treating, particularly for steel production.

In this article, Chris Pedder, Edward Rylicki, and Michael Aronov share that an “ITH + IQ” technique "eliminates, in many cases, the need for a gas-fired furnace when conducting through hardening and carburizing processes." A lot of this comes down to shortening the time it takes to perform this process, but there is so much more that the authors illuminate in their tests and graphs.

Read the full article here: Induction Through Heating + Intensive Quenching: A “Green Ticket” for Steel Parts

Drinking from a Firehose: Answering Your Quench Questions with a Thorough Radio Review 

Stay afloat in a sea of quenching tips with this Heat Treat Radio review, summarizing three recent podcast episodes centered around quenching tips, techniques, and training — especially applying to the auto industry.

Explore the "green" process of salt quenching with Bill Disler of AFC-Holcroft, the topic of water in your quench tank with Greg Steiger of Idemitsu Lubricants America, and a broad review of auto industry quenching with Scott MacKenzie of Quaker Houghton, Inc.

Read the full article here: Heat Treat Quench Questions Answered with Radio Review

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Traveling through Heat Treat: Best Practices for Aero and Auto

/ AEROSPACE HEAT TREAT, AEROSPACE HEAT TREAT TECHNICAL CONTENT, ATMOSPHERE AIR FURNACES TECHNICAL CONTENT, AUTOMOTIVE HEAT TREAT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, CONTROLS TECHNICAL CONTENT, FEATURED NEWS, HARDENING TECHNICAL CONTENT, INSTRUMENTATION TECHNICAL CONTENT, MANUFACTURING HEAT TREAT, TECHNOLOGY

Thinking about travel plans for the upcoming holiday season? You may know what means of transportation you will be using, but perhaps you haven't considered the heat treating processes which have gone into creating that transportation. 

Today’s Technical Tuesday original content round-up features several articles from Heat Treat Today on the processes, requirements, and tools to keep planes in the air and vehicles on the road, and to get you from one place to the next. 

Standards for Aerospace Heat Treating Furnaces 

Without standards for how furnaces should operate in the aerospace, there could be no guarantee for quality aerospace components. And without quality aerospace components, there is no guarantee that the plane you're in will be able to get you off the ground, stay in the air, and then land you safely at your destination.

In this article, written by Douglas Shuler, the owner and lead auditor at Pyro Consulting LLC, explore AMS2750, the specification that covers pyrometric requirements for equipment used for the thermal processing of metallic materials, and more specifically, AMEC (Aerospace Metals Engineering Committee).

This article reviews the furnace classes and instrument accuracy requirements behind the furnaces, as well as information necessary for the aerospace heat treater.

See the full article here: Furnace Classifications and How They Relate to AMS2750

Dissecting an Aircraft: Easy To Take Apart, Harder To Put Back Together 

Curious to know how the components of an aircraft are assessed and reproduced? Such knowledge will give you assurance that you can keep flying safely and know that you're in good hands. The process of dissecting an aircraft, known as reverse engineering, can provide insights into the reproduction of an aerospace component, as well as a detailed look into the just what goes into each specific aircraft part.

This article, written by Jonathan McKay, heat treat manager at Thomas Instrument, examines the process, essential steps, and considerations when conducting the reverse engineering process.

See the full article here: Reverse Engineering Aerospace Components: The Thought Process and Challenges

Laser Heat Treating: The Future for EVs?

If you are one of the growing group of North Americans driving an electric vehicle, you may be wondering how - and how well - the components of your vehicle are produced. Electric vehicles (EVs) are on the rise, and the automotive heat treating world is on the lookout for ways to meet the demand efficiently and cost effectively. One potential solution is laser heat treating.

Explore this innovative technology in this article composed by Aravind Jonnalagadda (AJ), CTO and co-founder of Synergy Additive Manufacturing LLC. This article offers helpful information on the acceleration of EV dies, possible heat treatable materials, and the process of laser heat treating itself. Read more to assess the current state of laser heat treating, as well as the future potential of this innovative technology.

See the full article here: Laser Heat Treating of Dies for Electric Vehicles

When the Rubber Meets the Road, How Confident Are You?

Reliable and repeatable heat treatment of automotive parts. Without these two principles, it’s hard to guarantee that a minivan’s heat treated engine components will carry the family to grandma’s house this Thanksgiving as usual. Steve Offley rightly asserts that regardless of heat treat method, "the product material [must achieve] the required temperature, time, and processing atmosphere to achieve the desired metallurgical transitions (internal microstructure) to give the product the material properties to perform it’s intended function."

TUS surveys and CQI-9 regulations guide this process, though this is particularly tricky in cases like continuous furnace operations or in carburizing operations. But perhaps, by leveraging automation and thru-process product temperature profiling, data collection and processing can become more seamless, allowing you better control of your auto parts. Explore case studies that apply these two new methods for heat treaters in this article.

See the full article here: Discover the DNA of Automotive Heat Treat: Thru-Process Temperature Monitoring

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El ensayo de dureza Brinell para principiantes

/ AUTOMOTIVE HEAT TREAT, AUTOMOTIVE HEAT TREAT TECHNICAL CONTENT, FEATURED NEWS, HARDENING TECHNICAL CONTENT, HARDNESS TESTERS TECHNICAL CONTENT

Cuáles son las características más deseables de un probador de dureza Brinell? Esta reseña del equipo le permitirá evaluar si debe o no incorporarlo a su departamento de tratamiento térmico.

Read the Spanish translation of this article in the version below or read the English translation when you click the flag to the right. Both the Spanish and the English versions were originally published in Heat Treat Today's August 2023 Automotive Heat Treat print edition.

Toda empresa dedicada al tratamiento térmico deberá practicar ensayos de dureza, algunos de ellos utilizando la medición Brinell que data desde el año 1900, lo que lleva a que se amerite el análisis de tan perdurable técnica. La prueba en mención requiere de un penetrador de bola de carburo de tungsteno que impacte de manera vertical sobre la superficie del material a ser ensayado, previamente ubicado éste sobre un yunque fijo. Paso seguido, se mide el diámetro de la “huella” generada por la bola, mínimo por los ejes “x” y “y,” y se toma el promedio de estas mediciones como cifra operativa de la que se pueda valer el técnico para establecer la dureza, bien sea alimentando una ecuación o mediante la lectura de una tabla de valores en la que se relacione diámetro frente a dureza.

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Para el ensayo Brinell se dispone de una amplia gama de cargas de fuerza, al igual que de diámetros de penetradores, reflejando la gran variedad de metales a ser probados; no obstante, en la mayoría de ensayos se implementa una bola de 10mm bajo una carga de 3.000 kg. En las grandes máquinas de apoyo a suelo por lo general el penetrador es motorizado, aunque otras operan a partir de palancas y pesas, mientras que también las hay hidráulicas o neumáticas.

Existen tres razones principales por las que la prueba Brinell no deja de ser el método más opcionado para la medición de la dureza en muchas industrias de tratamiento térmico.

1. Preparación de la superficie

La preparación de la superficie de una muestra para las pruebas Brinell toma solo unos segundos con una amoladora. Siempre que la muestra esté firmemente asentada sobre el yunque presentando la cara superior en dirección perpendicular a la dirección de la fuerza del penetrador, de acuerdo a lo exigido por las normas, no es necesario lograr una superficie demasiado lisa.

Figura 1. Robusto probador Brinell in situ

2. Contaminación de la superficie

Es poco probable que los contaminantes diminutos en una superficie generen una “prueba errónea” bajo un penetrador Brinell, a diferencia de la prueba de dureza Rockwell (el método más común en la industria). En esta prueba un pequeño indentador de diamante penetra menos de una centésima de pulgada, arrojando como resultado el que cualquier contaminante o anomalía en la superficie que pueda impedir o favorecer el progreso del penetrador (incluído el paralelismo) represente un problema, y obligando a que las muestras para la prueba Rockwell se deban preparar cuidadosamente antes de realizar la misma.

3. Portabilidad

Quizás el factor más significativo es que los robustos equipos portátiles de mano Brinell, con cabezales de prueba hidráulicos, permiten probar, in situ, piezas grandes, pesadas, de superficies rugosas o formas irregulares. Esta característica es de tal utilidad en la industria que ha motivado a que los órganos de normalización internacional otorguen una dispensación especial, una excepción si se quiere, a las máquinas portátiles, pese a que la ejecución de las mismas no sea susceptible de verificación directa como sí lo es la de sus equivalentes, las máquinas fijas.

Con fuerzas que van desde los 3000 kg hasta 1 kg, y bolas penetradoras tan pequeñas como 1 mm, las pruebas Brinell se pueden usar en una amplia gama de metales, pero los lugares en los que existiría la mayor probabilidad de encontrar un equipo de 10mm/3000kg son las forjas, las fundiciones, las plantas de tratamiento térmico, los laboratorios y las áreas de control de calidad. Previamente mencionamos que no se requiere que la superficie de las muestras de prueba sea absolutamente lisa; de hecho, es posible medir con un grado importante de precisión las superficies irregulares en materiales de configuración gruesa ya que el diámetro de la hendidura es tan grande en relación con cualquier irregularidad en la superficie.

Figura 2. Probador de Brinell, grado calibrador, en primer plano

En la Figura 2 se puede apreciar cómo un probador Brinell de grado calibrador introduce la bola de carburo de tungsteno en la muestra de prueba. Se mantiene la bola en posición para estabilizar la deformación plástica.

Las normas que rigen de manera detallada las pruebas Brinell son la ASTM E-10 y la ISO 6506, pero el procedimiento práctico para los técnicos es muy sencillo, tanto que el entrenamiento no debería tardar más de una hora. Para ensayar piezas forjadas, palanquillas y otras muestras, una hendidura debería bastar aunque, desde luego, en ciertas aplicaciones de extrema importancia se podrá utilizar más de una para mayor seguridad.

Saber si analizar o no cada muestra en un lote determinado deberá decidirse con base en la inconsistencia de las muestras mismas, más no responde a problemática alguna con las pruebas de Brinell en sí. En ciertas industrias se prueba cada pieza que se produce debido a que el riesgo de error es demasiado alto. Un buen ejemplo lo encontramos en la producción de los componentes de los eslabones para las orugas utilizadas en tanques y maquinaria pesada (retroexcavadoras y demás). Cada eslabón de cada oruga de un tanque en uso en el ejército británico ha sido probado por Brinell en una máquina totalmente automática, de alta velocidad, que cuenta con una poderosa abrazadera integral para mantener el componente absolutamente rígido durante la prueba. Por cierto, esa máquina es la de la primera foto. Con un cuidado adecuado y razonable, un probador Brinell robusto podrá generar cientos de miles de pruebas; de hecho, el probador de la Figura 1 ha realizado varios millones.

Las pruebas duran aproximadamente quince segundos ya que el penetrador se debe dirigir hacia el material de manera uniforme sin permitir la posibilidad de un “rebote” y evitando por completo llegar a golpear el material. Por otro lado, el metal debe recibir la presión por un período de tiempo suficiente que garantice que la hendidura se deforme de la manera más plástica posible, es decir, minimizando al máximo el riesgo de la más ligera contracción de la hendidura una vez retirado el penetrador.

Figura 3. Medición de una hendidura de prueba de dureza Brinell

Sin embargo, es en este punto que se presentan las complicaciones. Después de generar cuidadosamente la hendidura y retirar la muestra de prueba de la “boca” de la máquina probadora, es necesario medir la hendidura en al menos dos diámetros. Dado que las hendiduras de Brinell tienen como máximo 6 mm de ancho y que una diferencia de 0,2 mm en el diámetro podría equivaler a 20 puntos de dureza, obtener la medición correcta es esencial y de alta complejidad. La mayoría de los técnicos usan un microscopio iluminado para lograrlo, pero aún así puede ser un desafío. Considere la Figura 3.

Los microscopios de medición manual han mejorado a lo largo de los años, y cuando se obtiene una hendidura relativamente “limpia” con una retícula nítidamente iluminada, se le puede facilitar al técnico experimentado realizar una medición precisa. La Figura 4 presenta un escenario menos complejo que el anterior pero, aun así, ¿cómo podemos saber si realmente se ha juzgado con precisión la posición del borde?

Figura 4. Medición con microscopio mejorado y retícula bien iluminada.

Al crearse la hendidura se genera un cordoncillo en el perímetro de la misma debido a que el metal no solo presiona hacia abajo, sino también hacia los lados. Este cordoncillo puede difi cultar la ubicación del punto en el que comienza realmente la hendidura, y tres técnicos diferentes pueden hacer fácilmente tres estimaciones diferentes de su lugar de inicio. Es esta variación en la interpretación de los resultados por parte de los operadores la que ha llevado a que, durante más de 80 años, la prueba Brinell se haya considerado un poco “ordinaria”, apta tal vez para el maquinista en el taller, pero de dudoso valor para el científi co en el laboratorio.

En 1982 llegó a los mercados el primer lector automático, siendo éste la culminación de años de investigación, y valiéndose de software privado que llevó a las computadoras de la época a sus límites. El equipo podía hacer cientos de mediciones de un lado a otro de la hendidura y calcular el diámetro medio en una fracción de segundo. Poco después llegó a ser parte integral de una máquina de prueba Brinell. La noticia de la aparición de este equipo pronto llegó a algunos usuarios importantes en la industria de las herramientas petroleras quienes exigieron a sus proveedores valerse de él; quince años más tarde se había diseminado ampliamente el uso de esta tecnología generando la transformación de la percepción que se tenía de la prueba Brinell. Podríamos decir que la prueba Brinell había llegado a la mayoría de edad.

Figura 5. La última versión de ese microscopio automático en acción

Desde luego, como con cualquier equipo de medición importante, la calibración y el mantenimiento regulares son aconsejables, si no obligatorios. Los fabricantes mismos suelen estipular un cronograma de mantenimiento que se debe tener en cuenta junto con las reglas de calibración establecidas por las agencias internacionales.

Al considerar las opciones para la prueba de dureza en muestras con tratamiento térmico, en última
instancia existen tres métodos: Brinell, Rockwell y Microdureza (Vickers o Knoop).

Pese a que no es adecuada para muestras muy pequeñas o demasiado delgadas, la prueba Brinell es relativamente “inmune” a los contaminantes pequeños, los penetradores no son costosos, y, gracias al ancho de la hendidura, las pruebas de superficies con acabado áspero e irregular no presentan dificultades. Con el desarrollo, hace 40 años, de la medición automática de la hendidura, se superó la única deficiencia grave de la prueba Brinell, proporcionando las garantías que tan vital importancia revestían para los proveedores de piezas esenciales en industrias de toda índole, incluídas las de petróleo y gas, aeroespaciales y de defensa y transporte.

Sobre el autor: Alex Austin se viene desempeñando desde 2002 como gerente de Foundrax Engineering Products Ltd. Foundrax es proveedor de equipos de prueba de dureza Brinell desde1948, siendo en realidad la única compañía en el mundo especializada en el campo.

Alex funge en el Comité de Prueba de Dureza por Hendidura ISE/101/05 del British Standards Institution. En su calidad de miembro de la delegación británica de la Organización Internacional de Normalización, ha aportado como consultor para el desarrollo de la norma ISO 6506 “Materiales metálicos–prueba de dureza Brinell” y preside en la actualidad la revisión ISO de dicha norma.

Mayor información en www.foundrax.co.uk

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