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Staying Up to Speed with Sintering Parts and Additive Manufacturing for Heat Treat

OCThe powder metal industry continues to develop to keep up with production and industry needs. What exactly goes on with powdered metals and additive manufacturing? What is the sintering process? What should heat treaters know about the future of this industry?

In this original content article, three different resources -- an article, a radio broadcast, and a Heat Treat TV episode -- come together to answer these questions and much more.


"Heat Treating, Additive Manufacturing, and Serialization."

Ron Beltz
Director of Strategic Accounts
Bluestreak | Bright AM™

In this article, investigate the processes used to treat the metal powders. Sintering is one such process and others, like annealing and hot isostatic pressing, are examined too. Ron Beltz, director of strategic accounts at Bluestreak | Bright AM’s™  takes a look at these processes and also discusses other elements like software use and serialization. "One of the issues of additive manufacturing is the possibility of internal defects," Beltz explains. "Direct metal laser sintering (DMLS) regularly produces near 100% dense parts, but to provide another level of control to help reduce part failure, hot isostatic pressing (HIP), instead of heat treating, is successfully being used by many aerospace companies and in the casting industry."

Harb Nayar
TAT Technologies
(photo source: tat-tech.com)

Heat Treat Radio #36: "A Discussion with Harb Nayar, Sintering Guru."

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Hear from Harb Nayar, president and CEO, TAT Technologies; as he peers into the future of the industry; "The other [change in industry] I think that’s going to emerge is most probably making more and more parts by powder metallurgy from metal powder which are 100% free alloyed." Nayar is confident that the powder metal industry will keep growing, and this interview gives good insights from his depth of knowledge.

Heat Treat TV: Press-and-Sinter Powder MetallurgyHeat Treat TV episode: "Press-and-Sinter Powder Metallurgy."

John Engquist, FAPMI (past president of the Center for Powder Metallurgy Technology), gives some practical basics on what powder metallurgy (PM) is and how sintering helps produce automotive components. "Let's take a look at some PM applications: here we have a notch and pocket plate that are used in one way clutches. . . .made from sinter hardened steel and iron carbon steel. Here we have an automotive planetary carrier system. . . .Here we see stator cores for electric motors . . . ." Listen in on ways to use powdered metal.

These thought-provoking pieces give an opportunity dig a little deeper into sintering and additive manufacturing. Stay on top of education and developments within the powder metal industry.


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Back to Basics Before Heat Treat Boot Camp

OCIt's always a good idea to review the building blocks of the heat treat industry. In preparation for Heat Treat Boot Camp, get back to the basics to be ready for these five topics: Products, Processes, Players, Markets, and Materials. Take a look or listen to any of these 10 resources in this Technical Tuesday original content compilation to be geared up for Heat Treat Boot Camp.

See you in Pittsburgh on October 31st!


Products

Here's a look at one type of product that is used in heat treatment processes: a mesh belt heat treatment system. This article takes a look at advancements in improving fastener quality:

1. "Mesh Belt Heat Treatment System Advancements for Automotive Fastener Production"

Processes

Learn how nitriding and ferritic nitrocarburizing processes differ in this in-depth article. Keep it simple by referring to the easy-to-understand chart within the piece:

2. "Nitriding vs. FNC"

Players

At Heat Treat Boot Camp, the players in the industry will be discussed. Who are the movers and shakers? Here are some resources with a sampling:

3. "3 Aspirational Heat Treat Legends"

4. Heat Treat Radio #32: A Discussion with Jean-François Cloutier, Nitrex CEO

5. Heat Treat Radio #7: Former Bodycote CEO Re-Enters Heat Treat Market

Markets

The aerospace, automotive, energy, and medical markets are constantly evolving and improving. Just to keep the markets fresh in the mind, here is the latest technical item from each:

6. Aerospace. "Vacuum Gas Cooling: Pressure vs. Velocity, Part 1 of 2"

7. Automotive. "Guide To Conducting SATs According to CQI-9 4th Edition"

8. Energy. "Harnessing the Sun: A Heat Treat Case Study with General Atomics"

9. Medical. "Hot Take on HIPing"

Materials

This interview digs in to aluminum and different types of steel. A bit of a history lesson appears here too, as the raw materials are examined:

10. Heat Treat Radio #76: "Lunch & Learn with Heat Treat Today – Mill Processes and Production, Part 1"


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Heat Treat Supplier To Provide Andritz Group With Vertical Vacuum Furnace

HTD Size-PR Logo

Maciej Korecki
Vice President of Business of the Vacuum Furnace Segment
SECO/WARWICK

The Andritz Group, a manufacturer of complete lines for cold-rolled strip production and processing, has ordered a vertical vacuum furnace. The furnace for gas quenching processes will help produce consistent product quality.

SECO/WARWICK Group , a manufacturer with North American  locations, equipped the Vector® furnace with a graphite chamber, gas cooling system, and a rotating hearth. The Andritz Group, with this system, adds to their heat treat capabilities in hydraulic power, pulp, and paper as well as metals processing industries.

This is the first vacuum furnace manufactured in the Tianjin facility of the SECO/WARWICK Group. “We have already worked with the Andritz Group, but this time it is the first contract with our Chinese branch. The Vector furnace is manufactured in our Chinese factory, which significantly shortens the solution’s delivery time to the customer," says Maciej Korecki, vice president of the Vacuum Products Segment at SECO/WARWICK Group.


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Manufacturer Expands HIP Capabilities for Energy Industry

HTD Size-PR LogoMTC Powder Solutions received a hot isostatic press (HIP) that will extend the onsite size parameters of the Powder Metallurgy Near-Net Shape (PM-NNS) HIP components for the oil and gas, chemical, nuclear, and power generation industries.

Quintus Technologies HIP System
Source: Quintus Technologies

Quintus Technologies, a HIP provider with North American locations, installed the press QIH 286L M URC® to accommodate the core components for many different mission-critical applications. MTC Powder Solutions will use the system with a work zone of more than 11 ft. high to increase productivity with components, having improved fatigue strength and extended service life.

Dr. Magnus Nyström
managing director
MTC Powder Solutions
Source: LinkedIn

“We see a lot of opportunity in the areas of renewables, civil nuclear, small nuclear reactors, and the food industry,” reveals Dr. Magnus Nyström, managing director at MTC Powder Solutions. “In many of these sectors, the projects are becoming increasingly challenging in terms of higher pressures and more corrosive environments, and there is a strong desire for implementing PM HIP where traditional manufacturing technologies such as forgings and castings fall short.”

Jan Söderström
CEO
Quintus Technologies

"We have seen the need for hot isostatic pressing increase steadily,” says Jan Söderström, CEO of Quintus. He continues, "The push for faster fabrication and lead times favors PM HIP technology as its freedom-of-design benefit can remove costly fabrication processes such as welds and/or machining."

 


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Reader Feedback: Measuring Junction Construction in AMS2750 Rev. G

Readers are checking out recent AMS2750 Rev. G changes and want some more information from Heat Treat Today about a specific clarification. Read the correspondence about the implications of AMS2750 Rev. G paragraph 3.1.1.5 about how to measure junction construction.

Douglas Shuler, lead auditor at Pyro Consulting, has written numerous articles with Heat Treat Today about AMS2750 standards. Check them out by searching "Doug Shuler" at www.heattreattoday.com.

Submit your question, comments, thoughts, or queries here or email Bethany Leone at editor@heattreattoday.com.


READER QUESTION: After combing the new AMS2750 Rev. G, I found that paragraph 3.1.1.5 no longer allows thermocouples to be tack welded directly to parts, OR to representative dummy parts. This has been standard practice for decades. So I dug into it further with the folks from PRI and it turns out to be true. They’re now expecting load thermocouples to be either placed inside of a part (ends twisted and inserted), or inside the hole of a dummy block.

I’d done some searching online and there isn’t a single source talking about this major change. This could lead to a lot of failed upcoming Nadcap audits.

Doug Shuler
Lead Auditor
Pyro Consulting

Douglas (Doug) Shuler (Pyro Consulting) for Heat Treat Today: Historically (i.e. prior to Rev. F), AMS2750 was silent on measuring junction construction. In Rev. F, the construction of the measuring junction was as follows:

Measuring junctions shall be made by any combination of twisting and/or welding the thermal elements provided there is no addition of filler metal.

This raised concerns about both the use of quick tips and spot welding to make the measuring junction. The AMEC AMS2750 revision team engaged with Cleveland Electric Laboratories to perform testing on these measuring junctions as compared to the twisting/welding combinations.

The conclusion of the tests were that both quick tips and spot welding to a part/heat sink became unstable at temperatures above 2000°F. The quick tip crimping point and the spot welds showed rapid oxidation and increased errors in a short period of time. Based on the results of these tests the AMEC AMS2750 revision team put forth the following update in Rev. G:

Measuring junctions shall be made by either of the following methods:

        • Any combination of twisting and/or welding the thermoelements provided there is no addition of filler metal (including ungrounded and grounded MIMS).
        • Spot welding the thermoelements directly to a part, simulated part, or heat sink is permitted for temperatures ≤2000°F or 1100°C.

This allows spot welding measuring junctions for process temperatures at or lower than 2000°F. The team and AMEC members decided that quick tips were to unstable to permit their use going forward.

READER FOLLOW-UP: Our current method that we’re using is to twist the thermocouple using a set of Twister Pliers, then tack-weld that twist onto the part (first photo below). We’ve been doing this for parts up through brazing temperatures (~2150°F) without issue. We recently ran a furnace run around 2100°F with parts tack-welded as I’ve described AND had T/Cs that were just twisted with no tack weld. We noticed there was no significant difference in the temperature the TCs were reading. This was also our technique that we used at my previous company.

The way I read AMS2750 Rev. G was: You may twist and weld thermocouples to a part, but only for temperatures less than or equal to 2000°F.

To comply with Rev. G, we have gone ahead and made heatsink blocks to make sure we’re in compliance. Our new method of temperature measurement is twisting the wires and sticking the twisted end down inside of a block of solid metal (like the one I’ve shown below).

Source: Heat Treat Today Reader


We welcome your inquiries to and feedback on Heat Treat Today articles. Submit your questions/comments to editor@heattreattoday.com.

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Twin Heat Treat Furnaces Delivered to RIDGID® TOOLS

HTD Size-PR Logo

Nic Willis
Metallurgist/Heat Treat Manager
Emerson Professional Tools
Source: DELTA H

RIDGID® TOOLS received twin furnace systems from a North American supplier. These systems will heat parts from ambient to 975°F, soak for two hours, cool to 120°F, soak two hours, and then repeat. This will increase the production capacity of the company's current operations. 

The furnaces, from DELTA H®, feature a stainless steel interior with low mass ceramic fiber insulation for minimal heat retention, are designed to receive baskets with parts from an Ipsen Titan vacuum furnace, and include a floor guide system to enable precise load placement.

Roseanne Brunello, director of Sales at DELTA H®, has the honor first revealing the company's logo.
Source: DELTA H

"We had a challenge with utilization of our [current] vacuum furnace where a secondary heat treatment might be better accomplished with a convection furnace," explained Nicolas (Nic) Willis, metallurgist/heat treat manager at Emerson Professional Tools, provider of RIDGID® TOOLS. "This would dramatically increase the production capacity of our vacuum furnace and fully [optimize] this process. The extreme and demanding rapid heating and cooling cycles called for a unique convection furnace design."  

"I have known Nic for many years, including the Cleveland Chapter of ASM International where we both served as officers – and was honored to nominate him to the Heat Treat Today's 40 Under 40 Class of 2020," comments Rosanne Brunello, director of sales at DELTA H. "The process here was a challenge, but our CTO, Richard Conway, answered the call with an innovative and unique furnace design."

Main Photo Caption: Nicolas (Nic) Willis, Metallurgist/Heat Treat Manager at RIDGID® TOOLS and Richard Conway, Director/Chief Technology Officer at DELTA H®

 

 


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Heat Treater’s New Switch Saves Production Run Time

HTD Size-PR LogoSolar Atmospheres in Souderton, Pa, has had an automatic disconnect switch installed into a production car bottom vacuum furnace. The switch saves time by eliminating the manual maneuver of disconnecting and then re-connecting the power terminal bars at each end of the car bottom during each production run.

The switch, from Solar Manufacturing, Inc., is rated for 1,000 amps, 50V AC per pole, and the switches are installed at each end of the hot zone. Not only have the disconnect switches performed as well as expected since installation at Solar Atmospheres Souderton, PA, location, but they also have improved production.

Source: Solar Atmospheres


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Heat Treat Quench Questions Answered with Radio Review

OCTwice a month, Heat Treat Today publishes an episode of Heat Treat Radio, an industry-specific podcast that covers topics in the aerospace, automotive, medical, energy, and general manufacturing realms. Each episode provides industry knowledge straight from the experts.

Stay abreast of quenching tips, techniques, and training --- especially in the auto industry --- with this original content piece that draws from three video/audio episodes.


Heat Treat Radio: The Greenness and Goodness of Salt Quenching with Bill Disler

Bill Disler
President, CEO
AFC-Holcroft
Source: AFC-Holcroft

Sure, salt quenching has been around for quite some time, but this method is coming more to the forefront when we consider some of the concerns and costs of oil quenching. In this Heat Treat Radio episode, listen in to Bill Disler of AFC-Holcroft discuss the pros and cons of salt quenching. His brief overview and then salt versus other quench options will leave you ready to embrace quenching at your heat treat shop.

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"I’d say, in general, the most common thoughts with salt are to use it for bainitic quenching. If you’re quenching into a bainitic structure, salt has always been the only way to do this," comments Bill. "But what we’re seeing the growth into, and much more activity, is martensitic quench." As you listen, key into the point of salt quenching offering a "green-minded" solution due to recyclability.

Get the complete episode here.

Heat Treat Radio: Water in Your Quench with Greg Steiger, Idemitsu

Greg Steiger
Senior Key Account Manager
Idemitsu Lubricants America

Water in the quench tank? How much is too much? What do you do to get rid of it? Is it possible to prevent water from getting into the tank? Greg Steiger of Idemitsu answers these questions and more in this essential episode.

"Our research has shown that basically about 200-250 ppm water, you start to get uneven cooling," Greg Steiger cautions. "When you start getting up to large amounts of water, somewhere around 750 ppm to over 1000 ppm, it becomes a safety issue."

The entire episode gives answers to how to identify, prevent, and remove water in the quench.

Heat Treat Radio: All Things Auto Industry Quenching with Scott MacKenzie

D. Scott MacKenzie, Ph.D
Senior Research -- Metallurgy
Quaker Houghton, Inc.

This interview gets to some nitty gritty details regarding quenching and the shift to electric vehicles. What does the future of heat treating look like for electric vehicles (EVs)? Where is aluminum heat treat fitting in? Listen in to get industry insight on these answers. Scott MacKenzie of Quaker Houghton also explores simulation and modeling, the need for trained metallurgists in our industry, and more broad heat treat considerations.

"The next thing you have to understand is the quenchant itself," Scott MacKenzie advises. "You have to understand the physical properties."

Take in the full episode here.


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Perryman Company Orders 2 Forging Systems

HTD Size-PR LogoAmerican titanium producer Perryman Company, in Houston, PA, has placed an order for the supply of two forging machines: a high-speed open-die forging press in the pull-down design and a hydraulic radial forging machine with two forging manipulators as well as the order and production control system for the entire forging line. The titanium materials are intended for parts in the aerospace industry and for medical applications.

The open-die forging press from SMS group will be used to forge cast titanium billets first to the required size. After that, they can be finish-forged in the radial forging machine to produce bars – round, square or flat – up to a maximum length of 14,000 millimeters.

Dr. Thomas Winterfeldt
Head of Forging Plants
SMS Group
SMS Group

"We see strong growth in the aerospace industry and medical sector," emphasized Frank Perryman, president and CEO of Perryman Company. "This [new forging line] enables us to produce forgings for turbines and safety-relevant structures that comply with our high quality standards."

"With the whole SMS plant package, including digitalization tools and technology packages, Perryman is able to increase its production efficiency and maintain consistent quality levels," said Dr. Thomas Winterfeldt, head of forging plants at SMS group.

The forging line is scheduled to go on stream in Q1 2024.


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General Atomics Heat Treats 7 Modules for Superconducting Magnet

HTD Size-PR LogoGeneral Atomics has heat treated the seventh and final module for a large superconducting magnet for ITER, a multi-national science experiment, with a vacuum furnace from a heat treat furnace supplier in Pennsylvania.

In order to convert the 6 km long stainless-steel-jacketed coil of Niobium-Tin conductors into superconductors for the ITER (International Thermonuclear Experimental Reactor) experiment, each of these 4-meter by 2-meter 110-ton solenoid sections had to be heat treated for five weeks, exceeding 650°C (1202°F) at its peak. The heat treatment served to alloy the Niobium and Tin strands together into Nb3Sn, which becomes a superconductor when chilled with liquid helium to 4 Kelvin.

No such heat-treating furnaces existed, so General Atomics turned to SECO/VACUUM, a SECO/WARWICK Group company in Meadville, PA, to build a heat-treating furnace large enough to fit these solenoids and packed with all the technology needed to meet the strict quality control standards of this experiment.

Peter Zawistowski
Managing Director
SECO/VACUUM TECHNOLOGIES, USA
Source: secowarwick.com

"SECO/WARWICK Group did a great job designing in backup systems and robust design," commented Nikolai Norausky, program manager at General Atomics. "Any time we had questions or needed maintenance they were there to help."

The vacuum furnace that the supplier provided had to perform multiple tasks, including to bake off residual impurities from coil fabrication and to anneal internal stresses introduced at different stages of part fabrication. “General Atomics put so much time and money into these coils we really didn’t have any room for error," added Peter Zawistowski, managing director of SECO/VACUUM, "so nearly every component had to be doubly redundant."

Explore the experiment in Heat Treat Today original content article.


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