Heat Treat Radio #126:  HIP Finds New Life in Modern Manufacturing

Hot isostatic pressing, or HIP, is experiencing a powerful resurgence across industries from aerospace to nuclear energy as manufacturers look for new ways to scale up. This panel of HIP experts explores how renewed investment, government collaboration, and additive manufacturing are driving HIP’s next era of growth. From large-scale production to powder-to-part innovations, discover why this decades-old process is suddenly critical to the future of U.S. manufacturing. 

In this episode, Heat Treat Radio host, Doug Glenn, is joined by Cliff OrcuttAmerican Isostatic Presses, IncOscar MartinezBodycoteVictor SamarovSynertech PMSoumya NagOak Ridge National LaboratoryMike ConawayIsostatic Forging International; and Dave GandyEPRI.

Below, you can watch the video, listen to the podcast by clicking on the audio play button, or read an edited transcript.




The following transcript has been edited for your reading enjoyment.

Introduction (00:05) 

Doug Glenn: Welcome everyone to another episode of Heat Treat Radio. We have gathered a panel of experts to discuss hot isostatic pressing (HIP). I’ve asked the panel to bring us up to date on the latest developments and trends in the HIP market.  

I want to jump into the questions here quickly so we can move through and let these experts do the talking. But I want these six gentlemen to very briefly introduce themselves.

Cliff, go ahead with your background, please.

Cliff Orcutt: Yes, I’m the vice president of the American Isostatic Presses. I’m also chairman of the International HIP Committee. I’ve been in isostatic pressing over forty-five years. I started building equipment and then began installing it. Now I’m mainly selling it. Our company is a small company which has supplied equipment to forty countries around the world.

Doug Glenn: Okay, very good. Victor, how about you?

Victor Samarov: I work for Synertech PM Technologies. My background goes back to the Soviet Union in Russia where I got my education and started to get involved in powder metal technology and HIP. I’ve been a part of pioneering the sophisticated and challenging tasks of building jet and rocket engines from powder materials and, since 2000, working in the United States in near net shape and net shape HIPing of parts and materials for critical applications.

Doug Glenn: Alright, thank you. That’s great. All right, Soumya, how about you?

Soumya Nag: Thanks, Doug, for having me. And good afternoon everybody. My name is Soumya Nag. I am a material scientist and metallurgist at Oak Ridge National Laboratory. I work on different types of materials and manufacturing processes to get large scale components.

The reason why I’m here is that I’m leading a big effort under the Department of Energy Office of Nuclear Energy’s a AMMT program — advanced materials and manufacturing technology program. This program actually looks at power metal HIP technology to make large scale components.

Doug Glenn: Super. And we’re going to talk about large scale things in a little bit here. Mike, how about you?

Mike Conaway: I’m the managing director of Isostatic Forging International, and we own operate and technically support about fifteen HIPs around the world.

I’ve had a lifetime involvement with HIP equipment design, construction operation maintenance. I started at Battelle when I was nineteen years old, I think. Cliff has got me beat on the youth point and maybe on a few other points too. Except for six years as a Navy pilot, I’ve done nothing else except HIP my entire life.

Our current development efforts are very large HIPs and very small HIPs at the lab scale tailored for additive manufacturing.

Doug Glenn: Appreciate your service, by the way, in the Navy. That’s great.

Mike Conaway: Well, it was great fun. Great to look back on.

Doug Glenn: Super. David, how about you?

David Gandy: Yeah, I’m a principal technical executive in EPRI’s nuclear materials areas. Doug indicated my background in metallurgy and welding for, I guess, the last fifteen years or so. I’ve spent time in advanced manufacturing looking at a variety of different topics, including PM and HIP. I have been in the business for a little more than forty years.

We’re all getting a little gray.

Doug Glenn: All well experienced, well-seasoned. All right, Oscar.

Oscar Martinez: Oscar Martinez. I’m the youngest of the group and learning from everybody here. I’m the regional sales manager for HIP North America, so I cover six different facilities in the North American market. I’m a metallurgical engineer by background. I have been in the oil and gas industry for about eight years with fader analysis and then jumped into HIP and product fabrication. Happy to be here; thanks for the invite.

Doug Glenn: Appreciate you joining us.

A New Renaissance of HIP? (7:41) 

The first question really deals with what has been bringing interest back to back to HIP. It seems like a lot of what we’re hearing about HIP processing deals with 3D printing and additive manufacturing. 

Is that the primary driver of the new renaissance of HIP? 

Victor Samarov: No, I wouldn’t say so. Basically, there are three areas of “HIPing.” The first has been rising steadily through decades, and that is HIPing of castings. You take a bad casting and bring it to the level of a better material by healing porosity cracks and changing the microstructure. 

The second area, which you mentioned, is 3D printing, which is, to some extent similar. HIPing of 3D-printed parts is similar to HIPing of castings, but there is more emphasis not on healing porosity but on changing the microstructure and making it more uniform and homogeneous. However, the parts are much smaller by far, and the share of the market is not large. Bodycote and others probably have a better understanding of this.

The third area is making parts from powders, which has been steadily at a relatively low level. This is because the only major industries interested in this have been aerospace, rocket engines, and oil and gas, all of which are  well developed in Europe and Sweden. For example, there’s a company that has been doing very large parts for that for decades. 

Recently, I mean the last fifteen years, we have to thank not only the Department of Energy (DOE) but David Gandy who was an enthusiast and a pioneer pushing this technology forward. There is much more interest from the nuclear industry in replacing very heavy forgings, which take years to fabricate and still usually are not good quality, by powdered metals.  

This leads to open doors in many other aspects because most of the nuclear parts are large, and many of them are larger than the existing HIP furnaces. So large that it requires 4 meter, 3 meter, 5 meter, etc. — we can discuss. So, the new driver to PM HIP is mainly from the nuclear industry with large parts since they bring a lot of technical problems, serious problems.  

This is very important, and this is the major perspective for HIP: rockets engines will still be there, aerospace will still be there, but nuclear is a new horizon.  

Doug Glenn: David, what’s driving the new renaissance from your perspective? It seems that there is somewhat of a renaissance of HIPing, more activity. The nuclear market, will you address that?  

David Gandy: Certainly  the nuclear area. We are looking to build quite a number of reactors over the next 30 years. In fact, we’re discussing 600 to 800 gigawatts of new build, which is quite enormous compared to what we have today. 

Much of this activity is being driven by things like data centers. There’s a lot of construction of data centers planned over the next ten years even, but certainly it will continue to grow. There’s a lot of additional power that is needed for things like electric vehicles. There’s a bit of work going on around that. 

In general, as we modernize our world, electricity certainly becomes more in demand, and we have to meet those demands. The other part of this is just looking at carbon issues and trying to reduce the overall carbon footprint in the world. Nuclear electric power provides a very clean generating product that can be used throughout the world. 

Doug Glenn: Larger parts seem to be a driver in HIP as well.  

The issue with getting larger HIP parts is actually building the equipment to carry out HIPing because, as the equipment gets larger in diameter, for example, the complexity and the engineering of it becomes extremely difficult. Soumya, can you address this aspect?  

Soumya Nag: There are very different aspects to what we are referring to when we say large parts. As you mentioned, in terms of whether you can HIP large parts, that is obviously a drawback. The other is, as you go into more complex parts or one-of-a-kind parts, can you make it cost effective and can you make it perform as well as your cast-forged counterparts? 

That’s a big question. We have a sizable team at Oakridge working on looking at U.S. domestic manufacturing resilience. Can we actually make customized parts by different manufacturing modalities and use different materials that could fit to that manufacturing scheme to produce components that are built to perform the way you want them to?  

PM HIP forms a big part of that portfolio. Using additive manufacturing along with PM HIP, which we call convergent manufacturing because we are converging two different manufacturing modalities using similar or even disciplined materials, is something that we are extremely focused on. 

Now what is advantage of additive manufacturing? The big advantage to additive manufacturing is design flexibility and customization of the parts, which helps your end product. Like Victor mentioned, all aspects of PM HIP are still good in terms of the densification, powder consolidations, and other factors, that are still as you would expect it to form. 

You are basically coupling a kind of technology: first, a newer process in the case of additive manufacturing with, second, one which has greater flexibility, that is PM HIP, a relatively well known technology.  

Click below for HIP technical articles

Doug Glenn: Let’s talk to the guys who are out there selling this process and/or building the equipment. First, Oscar, what are you seeing? What are the toll processing changes?

Oscar Martinez: The majority of what toll HIP service is going to see is castings by a magnitude of 60 or 80% of the business as a whole as of now. I have seen a lot more over the last couple of years on 3D printing and additive manufacturing.  

I do want to say that additive manufacturing has been growing in different markets as well. In the medical market, it is a little bit more established. We have seen the medical market take on some of the porous coating and those new technologies that help.  Within the aerospace market, I think it’s getting closer and closer to being more of a critical component. 

There is still a gap between those two industries. However, the business is starting to grow. For companies that are doing this, I’m noticing they are increasingly starting to get involved in having additive manufacturing either in-house with their own machines or through a sub-contractor. I do agree that in the near future castings are always going to be predominantly the factor. 

The last aspect is there has to be a cost analysis. Your absolutely right on this, Victor. I’m seeing it on the additive manufacturing side; they want to implement rapid cooling and they want to implement different cycles and different properties to get various properties from the material itself. However, there’s a difference whenever we’re talking about toll HIP service. If they want to do those, then those fall into dedicated cycles, which are much more expensive.

So, there has to be a kind of in between where we consolidate features and processes, because price is going to be the leader in terms of how fast it grows in the market. 

Doug Glenn: Mike, what are you seeing in your organizations?  

Mike Conaway: We’ve run about 250,000 HIP cycles, and 95% of those are castings. 

To lay the foundation of what we consider a small or large part: to me a small part is something that’s less than 8 inches in diameter, a medium-sized part is maybe 2 feet, and current large parts are about 5 to 6 feet in diameter, though we are now  trying to make parts that may be as large as 12 or 15 feet in diameter. 

We have to have some idea of what scale we’re talking about of these parts. That being said, we are essentially all castings, with very little powder metal.  

Doug Glenn: Cliff, any drivers that you’re seeing for HIP?  

Cliff Orcutt: The main driver is that as the world keeps advancing and as we have higher technologies and computers with FEA and so forth, we’re looking for stronger, lighter, faster materials.  

The performance of materials in general is increasing throughout every industry, whether that’s a car or an airplane or a printer. Also, the technology is spreading worldwide faster because communication and the internet. I believe the United States used to have the lock on HIP, and now China and Russia and other places are all on par with us. It’s spreading throughout the whole world, and it snowballs too. 

Initially, it was slow, but now it’s snowballing faster and faster. 3D printing is an exciting technology that has brought about new applications, but I think even other applications are just growing faster and spreading.   

The Origin of HIP (20:12)

Doug Glenn: Is the origin of the HIPing process U.S.-based?  

Mike Conaway: It’s like asking, “who had the first airplane?” Everybody agrees it was the Wright Brothers.  Similarly, it’s agreed that HIP was invented at Battelle Memorial Institute in Columbus, Ohio. I came to Battelle a few years after it was invented, and I was in on the industrialization of the process. Obviously, some serious work has been done in Russia and China, but that’s where it came from. That’s where Cliff’s father and I worked together — at Battelle — and we consider ourselves “Fathers of the Industrialization of the HIP Process.” 

Doug Glenn: You’re not going to take credit for creating it, though, for the internet?  

Mike Conaway: No, no, that was Edwin Hodge, Stan Paprocki, and Henry Saller.  

Doug Glenn: Well, your humility is showing through here, Mike.   

HIP Worldwide (21:37) 

Doug Glenn: Let’s address how the technology is spreading across the world. 

Are there any major new players either on the manufacturing of equipment side or the use of the equipment side around the world?  

Cliff Orcutt: There are both players, manufacturing, and end users. As far as manufacturers, we’re now seeing there are five Chinese domestic manufacturers. There are new ones in Russia, Korea, and India. There’s also a major player in Spain; that’s Hyperbaric. They have been building high pressure equipment, but not necessarily HIP. We see companies like that opening up and starting to build. We don’t know which ones will survive, because HIP is an up and down market. We’ve seen some companies come and go — vacuum generators, and on and on. We will see how it will all play out.  

We have seen new manufacturers, as far as users or toll producers. There are large companies in China now starting up. Korea has some, India is probably the next big market, maybe ten years behind. 

Victor Samarov: I want Cliff to add more, because Cliff has wonderful stories. We’re talking mainly about metals, but Cliff is a great proponent of ceramics, and ceramics not only has great applications but requires different HIP equipment for high temperature and for high pressures. Ceramics is also the future.  

Cliff Orcutt: Yes, we do see a lot of ceramics. Everything from braces and teeth to ball bearings for electric motors, boron carbide armor, military applications, hafnium carbide, and odium carbide. Those things are coming. 

One of the hindrances to HIP is the cost of raw materials. People tell us, if you could make silicon nitride powder cheaper, we’d HIP everything out of silicon nitride.  

Soumya Nag: One thing I wanted to add is we talked about HIPing cast metal parts and several materials: HIPing is also used to densify or “heal” additive parts as well. You can look at an AM part, and we usually go through a HIPing process to kind of heal what we call the lack of fusion type of porosities, or even in some cases the gas porosities work as well if your operating temperature is not too high where the gas can come out again. HIP is being used for a lot of use cases for castings. You can actually HIP using powder for alloys that cannot be forged. So that’s another specialized use case for HIPing as well. 

Interactions with the DOD and DOE (25:16) 

Doug Glenn: Let’s jump into discussing how the DOD and the DOE are pressing hard on the industry to come up with a 4-meter HIP unit. 

David, can you tell us what the driving force is here, what we’re trying to accomplish, and why it’s a challenge?  

David Gandy: So much of this started back around 2017 when we started a DOE project. In that DOE project, we were looking at utilizing the new scale reactor design to try to produce components out of powder metallurgy HIP. We worked with Syntech quite a bit in that area, trying to build large components like the reactor head and other parts throughout. Those, ultimately, would go to about 10 feet in diameter. We are currently restricted right now by the size of the HIP units that we’ve been working on, so we’re only making things on the order of 60 or 70 inches. 

The real driver there comes out of our success in producing very large components that are near net shape — we would like to be able to expand that to be able to do very large parts. The 4 meter came from a little bit of the work around the projects with the Department of Energy (DOE). It also came from DOD, which was beginning to look at whether we can actually make big parts for nuclear reactors that sit on a submarine, an aircraft carrier, or another boat. 

How do we actually make some of those large parts? There is quite an interest from the DOD and from the DOE in trying to really push the technology. We kind of settled in that 4 meter range; it might be a little bigger, it might be a little smaller, but to make some of the large parts that we’re talking about, we need to have a much larger HIP unit than is available today. 

Doug Glenn: Are the larger parts for a nuclear reactor specifically or are we talking about a variety of different large parts? 

David Gandy: Parts of them are for the nuclear reactor, but there are a number of other components, like large valves or large pump housings — many different components that could be produced with this technology. 

Doug Glenn: What are the main impediments to a 4 meter HIP unit?  

Cliff Orcutt: Like anything that’s new, there are unknowns, and the big one is the ROI along with the cost of doing something on that scale. Many of us are looking at it; companies such as Bodycote are considering larger units and MTC is considering larger units. The U.S. government at one time had the largest HIP in the world. Now it’s owned by Japan. We are hoping the U.S. government will step up and try to do a large project again. 

“There’s unknowns and the big one is the ROI and the cost of doing something on that scale.”

We went to the moon and we did other things, but we’ve kind of pulled back. We hardly have large forging capability in the U.S. anymore, and we need to invest in these kinds of technologies and push this forward.  

David Gandy: I’d like to build just a little bit on what Cliff said. In terms of building reactors in the U.S. to support the civil fleet — the civil nuclear reactors — quite frankly, we don’t have the forging capacity in the U.S. that we once had to do that. 

So this would actually supplement the forging capabilities and allow us to reshore some of those capabilities in the U.S.  

Oscar Martinez: That is a good point, David, and it is part of where PM HIP will jump in and bridge the gap between the two. 

One thing I wanted to mention regarding what Cliff said about the ROI is that the biggest factor for HIP companies — like Bodycote and others out there — is making sure that we have the nuclear side. We have already seen what the ramp up is going to look like and everything. 

For us, if a HIP unit is not running, it’s not making money. So, we need to make sure that HIP unit is always running, and that it’s going to pay for itself. With these large units, the price of it doesn’t just double from previous one, it exponentially goes up.  

Victor Samarov: Double? It’s quadruple! 

Oscar Martinez: I know the DOD and DOE are working closer together to have more synergy in terms of what components they need to process. But I also think that in the industrial side of things, like general industrial, anything with heavy equipment, any of those components that probably were not something liable to use of HIP because of the size or price, it would be good to start looking at how we can incorporate those other markets to see if they would also use some of that equipment or those HIP services for their equipment.  

David Gandy: On the DOD side of the house, we have something called AUS, which is the agreement between Australia, the U.S., and the UK, wherein we’re actually going to be building quite a number of ships and submarines over the next few decades. That’s going to change the way we look at our supply chain. In trying to build these components, we need to have additional forging, casting, additive manufacturing, and HIP capabilities — we need to have it all. It cannot happen without a number of different technologies engaged.   

The Path to Commercial (34:00)

Doug Glenn: In discussing these additional needs and supply chain logistics, Victor mentioned that the commercial viability of the 4 meter is difficult. Victor, could you expand? 

Victor Samarov: If ATLAS HIP appears tomorrow, we’re ready to make parts with it. There is powder supply and we know how to make the casts. With some small underwater stones, we can make the parts, but we’ve been waiting for this HIP system for at least ten years.   

“If ATLAS HIP appears tomorrow, we’re ready to make parts with it.” -Victor Samarov

There is no commercial company to build it, and there is no commercial company to order it unless it’s the U.S., Chinese, or Korean government. The technological idea is based on very advanced developments done by EPRI and other scientists in joining already manufactured power parts. 

We did try it already. We made very large parts that were cut in half and then joined by electron beam welding. It may be this faster route to provide U.S. industry with very large parts: first make parts as large as they can be and then electron-beam weld them. 

Working with David Gandy’s new scale projects, one part was so large that we had to split it into six segments. So, we made the segments and then they were successfully electron-beam welded. Practically, we were keeping all the advantages of powder metallurgy and HIP: lead time, material quality, faster development, so on and so forth. So, this may be a very viable direction.  

Doug Glenn: Mike, is that the path to commercial viability? 

Mike Conaway: I’m not quite sure. I call it jumbo additive manufacturing where you make these parts that have to be cut apart in, in concept, and then put together physically — that’s the additive manufacturing of jumbo parts. I think it’s a great idea.  

We are looking at the same sort of idea. To make a very large HIP, we would make it as a composite of segmented pieces that fit together. We call it the Lego HIP. That’s an approach, and we’re still working on that.  

Oscar Martinez: To add to something Cliff mentioned about going in between. We’ve talked about ATLAS, and I think Victor mentioned it too. 

From a commercial standpoint, I think it would be beneficial for us to venture into a kind of in-between size that does give us capabilities and proves out what we have to do. That would be probably a step in the right direction of where we need to be, because it will cover a lot of the components that we are not able to see. 

The oil and gas industry also has some components, and even on the IGT and aerospace side, if we go in between on some of those things, they will then design based on that size. If we’re looking at just commercially what HIP unit makes most sense for us to run, toll HIP services is always going to be between the 30 to 45-inch zone because it is able to fill in quickly. 

But again, that’s the biggest challenge. If we to go to an in-between larger component, what else could we bring in there that we could run all the time and make commercially viable for whoever jumps in — whether it be Bodycote, anybody else, or a collaboration — that it actually makes sense to be used.  

Cliff Orcutt: From an economic standpoint, if you’re only building one 4 meter HIP and you have to decide whether it goes to the East Coast or West Coast — that’s a tough decision. But if you build a couple 2 meter HIPs, you could afford to put one on the West Coast and one on the East Coast, and you solve not only the submarine building on the East Coast, but you might solve some of the SMR building on the West Coast.  

Doug Glenn: Or you put a 4 meter HIP in St. Louis and that takes care of it all.  

Cliff Orcutt: If you can get it there.  

Doug Glenn: Yes, if you can get it there, correct.    

Powder to Part (37:05)

Doug Glenn: Let’s talk about powder to part. What is it, what current processes might it replace, and what are the obstacles to using it?

Soumya Nag: At Oakridge, we are testing whether you can actually make custom powders, scale up that powder production, and then utilize PM and AM, or different type of modalities, to make large-scale parts or customized parts. With powder to part, you have a powder and you have a certain chemistry specification for that powder. Can we actually find out whether we are going to have a PM HIP as a plausible way to make the part out of it? Make a mold, fill it up, and predict how the part will behave in the post-HIP, the machine changes, etc., and then inspect the properties.  

One more caveat: When we talk about powder, where is the powder coming from?  

We have to look at the feed stock that has been used to make the powder and ask: What is the chemistry of the powder? What is the shape of the powder? What’s the flowability of the powder? The physical and chemical properties of the powder itself?

Doug Glenn: Dave, what appears to be the most promising avenue to bring this about? 

David Gandy: Well, I think one of the things that you’ve really got to consider for powders is powder cleanliness. 

We’ve worked quite a number of years on trying to reduce things like oxygen in the powder so that as you consolidate that component, you don’t end up with oxides that are trapped at the grain boundaries or prior particle boundaries. It’s very important that we get powder manufacturers to work with us to bring the technology forward. 

Understanding the molecular chain of powder: reducing oxides
“Reduce things like oxygen in the powder so that as you consolidate that component, you don’t end up with oxides that are trapped at the grain boundaries or prior particle boundaries.”

In addition to that, if we start making very large parts in a 4-meter HIP unit, we’re going to have to really scale up our powder production capabilities in the U.S., and quite frankly, that’s not happened at this point.

Doug Glenn: They’re not going to want to upgrade their powder manufacturing if there’s not a market for it.  

Victor Samarov: Yes, exactly. One really large part may need a hundred thousand pounds of powder in it. We have already completed these calculations. I completely agree with David.  

One more piece I want to add: From powder to part, all the processes, except HIPing and maybe ceramic, are based on melting the material and then giving it some shape. Cast and rot investment casting, even additive manufacturing, is based on melting every particle. However, when powder metallurgy started in the ‘80s in the U.S. aerospace industry, the basic advantage it was looking at was the quality of the powder particles themselves. As you know, as heat treaters, the maximum cooling rates in cooling the billet are some hundreds of degrees per minute. But the powder particle crystallizes, and it crystallizes at the rate of 10,000 degrees per second because of its very tiny size. So, it can freeze almost any type of unbalanced metastable microstructure in it. 

HIPing is a solid-state bonding process. Nothing is melting in HIP. This means that during this process, we can retain this unique microstructure of the powder particles and then create and transfer this to parts of any size. For steel alloys, it may not be so critical, but for nickel base and some other alloys it’s absolutely essential. 

The caveat here is that going from powder to part via HIPing, you can create very large parts with unique properties brought by the rapid solidified powder particle materials.    

Doug Glenn: Mike, anything you’d like to add on the powder to part?  

Mike Conaway: No, I don’t have anything to offer much there. 

We’re intrigued with the additive manufacturing. Our focus has been on the binder jet that’s based on sintering where I think it offers a lot more advantages than it does to the laser fusion approach. 

Oscar Martinez: From our end, we’ve been doing this for a while already in Sweden with the oil and gas industry being a major, almost an established, process. However, one thing that I did want to bring up is not only is there a challenge with the current powder suppliers in the U.S. — there is some movement in terms of bringing new suppliers —but whenever we’re discussing some of these components being so critical, where the powder is coming from is going to also be critical. As David mentioned, just as much as the HIP needs to be ramped up and that large unit needs to be built, just as quickly we need to do the same thing with the powder suppliers as well. If we need to keep it in-house, the U.S. is going to have to grow very quickly as well. 

Doug Glenn: Much of what was discussed at Oak Ridge recently by the DOD and DOE was about bringing home the supply chain, including powder production.   

Cliff Orcutt: The technology of making parts concerns how to model those parts and how to predict shrinkage. 

There’s people that understand it but making it more accessible to companies is key to expanding the market for it. 

David Gandy: We are currently working with Oak Ridge National Labs and a few others to look at bringing modeling to your laptop, basically to allow you to do modeling for the HIP process, very similar to what maybe you do with forging technologies today, where you can have that capability to design as a conventional engineer.  What we’re trying to accomplish in working on this project is really looking at how we make modeling more mainstream for industry. As you make the modeling portion of this more mainstream, then the HIPing technology becomes more mainstream. The more people are exposed to it, the more people are engaged in it, the more companies want to work with it. I’d also like to thank Victor Samarov because Victor has certainly been a huge proponent of this and of trying to help move the technology forward.

Oak Ridge National Lab (48:07)

Doug Glenn: Soumya, I understand Oak Ridge National Laboratory has taken an active role in the PM HIP market. What exactly are you guys doing there what are you hoping to accomplish?  

Soumya Nag: We want to make components that are relevant towards nuclear in the DOE space as well as national security in the DOD space. That’s where the drivers are.  

The first thing I want to mention is that we don’t want to replace your traditional manufacturing, casting, or forging by any means. As Dave was mentioning, the need for production is going to ramp up so high within the U.S. that we will need alternative manufacturing pathways to really augment some of the troubles we have on supply chain side.  

PM HIP is one of the technologies that we have chosen. Under PM HIP, we have done three things. First, can we actually use an AM, what we call a directed energy deposition process or WAM, our AM process, where we are basically making these five mile long wells that are used as a shell for the outside surface. Can that withstand the temperatures, pressures, and times (i.e., a reactor or pressure vessel), can it actually withstand that cycle? So that was the big thing: Can the five mile long well actually withstand that temperature, pressure cycle, and then move or deform during the HIPing process without a failure? 

Secondly, if you look at a traditional HIP cycle, what does that temperature, pressure, and hold time do to the material? Can you break it up into ramp up time, ramp up pressure, ramp up temperature, and then hold time, etc., and see microstructural changes, property changes, performance changes as a function of each of these segments that we use or take for granted for the HIP cycle. Those are more science-driven questions that we need to answer.  Thirdly, where some of the challenges that we have encountered [with scalability]. When we did a PM HIP workshop here at Oak Ridge last year in October, we had about a couple of hundred people show up from academia, national labs, DOD and DOE, customers, stakeholders, etc. The question was, what is the scalability of a part when you go from a small to large part or small to a more complex part in terms of powder compaction, size and scale of the powders, property variations, and chemistry? That is another PM HIP question that we are trying to solve.

At the end of the day, the goal is to make sure that the industry can adopt this more freely and employ it for large scale production. Then, also giving them the option of using additive cans — a more customized shell. The good thing about AM and PM combination, if you choose that, is that you can use AM can as a “shell,” which you can remove afterwards or keep. When you keep it, you are basically looking at a HIP-clad type of option where you can use similar or dissimilar materials and depending on the functionality of the surface versus the core, you can utilize that combination of two materials with two different manufacturing modalities. 

I think the workshop that we had in October last year was exceptionally well received from our end. It was driven for the voice of the customers — what does the customer want from us? What are the gaps and challenges around PM HIP that would really remove some of the angst that they have.  

That was the first thing that we did, but we also had people from the powder side, from the modeling side. 

Victor was leading the attendees, Dave Gandy was there giving plenty of talks about the need for PM HIP. Cliff was there talking about the utilization of HIP as a technology. We had industries from every bit of the segment come in and they wanted to help. 

The thought was, can we actually take personal spaces out and then talk and have a cross interaction across industries to try to solve a problem on national level. Like Victor and Dave said, we need our government to instill the idea that this is an important technology for the country. Can we move towards this? We were facilitating that and saying what the voice of the customer is. This is what everybody wants. The demand is absolutely there. Can we actually build on it?  

At the next workshop that we plan, we want to actually talk about real parts. We will be bringing in real parts to see how we can make it PM HIP. What are the success factors around it? I think that would be more end-product driven rather than the science part of the discussion.    

Doug Glenn: Yes, more practical and specific and less theoretical, if you will, but not that it was all theory. 

Soumya Nag: We have an active PM HIP steering committee with about twenty people from industry. Dave, Victor, and Cliff are a part of it. They have been tremendous in terms of providing us with guidance and seamless thoughts in terms of how we should move as an industry. 

Doug Glenn: Is that next workshop scheduled? 

Soumya Nag: Not yet, but that is in the planning process right now. 

Doug Glenn: We’ll certainly help publish that when the time comes, so keep us posted.  

Soumya Nag: We have a report from the first workshop that is in limbo right now, but we will publish it relatively soon.  

It discusses what we learned from the workshop, the gaps and challenges, and how we should move forward. We have about a 60 to 65-page report that we compiled from that workshop. These are the demand signals for everybody that we compiled together.  

Doug Glenn: Let us know if we can help you publish that as well and help you get it out to the right people.  

Toll Manufacturing vs. Ownership of Equipment (55:47)

Doug Glenn: Cliff, let’s discuss the differences between toll processing and ownership of equipment. When it comes to HIPing, does it make sense for manufacturing companies to send their HIPing out to toll manufacturers or is it better to buy your own equipment?  

Cliff Orcutt: That’s an economical question that you have to calculate and look at. Number one, if you only have one part, you’re not going to buy a HIP unit. 

Evaluating the cost of toll processing versus purchasing your own HIPing equipment. Basic rule of thumb: use toll HIPing until you cannot afford it, then go in-house.

But if you have the quantity and the quality, and the cost works to the favor of owning your own HIP unit, then you should purchase it. However, if you also don’t have the floor space, location, people, or infrastructure to support it, then sometimes it’s easier to toll HIP. If you’re in the middle of nowhere and your parts are lead, and you can’t afford to ship them, then you might want to have your own HIP unit located in your facility. It’s important to analyze these aspects to decide if there’s ROI and if it’s the best way to economically make your parts.

Doug Glenn: Mike, what are your thoughts on toll processing versus owning your own? 

Mike Conaway: I think you toll process until you can’t stand the cost anymore, and then you bring it in house.  

You plan the investment for it. There may be tipping points, I don’t know how to quantify those. But I think that Cliff’s remarks are well taken. It’s a little bit complicated and you have to have a believer; let’s say you’re a user of HIP equipment and you’re getting it done by toll. Sometimes you don’t want to have it; you don’t have anybody in-house that has insight into HIPing and therefore is not a champion for it. I recommend toll HIPing until you can’t afford it, and then we go in-house.  

Used Equipment Market for HIP (58:26) 

Doug Glenn: Let’s discuss the International HIP Conference. 

Cliff Orcutt: The 2028 conference is going to be held in South Korea in the town of Busan, very beautiful. And it’ll be a great conference, so we’re hoping to have over 200 people at it. 

It will cover all aspects of HIPing, not just powder metallurgy, but it’s all the latest technology from the makers, the toll people. Everybody that’s in the HIP industry is usually there from all countries. Hopefully by 2028 we can have the Eastern Block Country there attending again as well. 

Doug Glenn: If I remember correctly, it was in Columbus in 2022. 

Cliff Orcutt: Yes, 2022 in Columbus, 2025 in Germany. It moves from USA to Europe to Asia every three years.  

Doug Glenn: The committee is a group of people who have a common interest in putting this together. 

Mike Conaway: Yes, it’s group of enthusiasts.  

Doug Glenn: The most recent one was this year in Aachen, Germany, right?  

Mike Conaway: Yes.  

Doug Glenn: How many people attended that one?  

Victor Samarov: Around 250.  

Doug Glenn: HIP 2025 is currently on the website, and then when you’re ready, you’re going to have a HIP 2028. 

Cliff Orcutt: It’s reserved, and it’ll be coming online probably next year. 

The paper from 2025 has been released and made available to people.  

Doug Glenn: Anybody else have any other comment on the HIP event?  

Soumya Nag: It was my first time going there.  

I felt that it was a great exposure to what the world is doing on the PM HIP side. Sometimes we are bottled down in what we are doing in the U.S., and we think we are doing the best thing in the world. That’s not true. There are countries who are superseding us and they have ideas and thoughts and future goals which are very possible for them to succeed. We want to make sure that we learn from them and really act upon that.  

Cliff Orcutt: One thing we might want to mention is the Metal Powder Industry Federation, MPIF, for about 15 years has been promoting it as a green technology. I think that we all could agree that we should lean green, towards green things.

There’s less energy usage, less machining. It’s a near net shape technology, and so even if it does economically cost more, we still should look at it from that green aspect, I believe.  

Doug Glenn: And you’re talking just about HIPing in general or PM HIP?

Cliff Orcutt: Mainly PM, but all forms of would be more of a green technology compared to your big carbon melting type technologies. 

Doug Glenn: Good point, Cliff, thank you.

All right, gentlemen, thanks very much. I appreciate your time, your expertise, and it’s been a pleasure talking with you all.


About the Guests

Mike Conaway
Managing Director
Isostatic Forging International

   

Mike Conaway is the managing director at Isostatic Forging International. He began in the HIP field at 19 years old, where the process was invented and developed (Battelle Institute in Columbus, Ohio). Many consider Mike a pioneer in the business of HIP equipment: analysis design, construction and operations. He has ten issued patents related to high pressure design, and received the Lifetime Achievement Award by the International HIP Committee. 

For more information: Contact Mike at conaway@hot-isostatic.com or visit his LinkedIn.

David Gandy
Principal Technical Executive, Nuclear Materials
EPRI

David Gandy is the principal technical executive in the Nuclear Materials sector for EPRI. He has 40+ years of experience in materials, welding, and advanced manufacturing. He is an ASM International Fellow and currently also is a member of ASME Section III. 

For more information: Contact David at davgandy@epri.com or visit his LinkedIn.

Oscar Martinez
Regional Sales Manager
HIP North America, Bodycote

Oscar Martinez is the regional sales manager of HIP North America, Bodycote. He is a metallurgical and materials engineer with a degree from the University of Texas at El Paso. In 2022, he took his current position for the Hot Isostatic Pressure and Powdermet® divisions at Bodycote IMT, serving the North American market.

For more information: Contact Oscar at Oscar.Martinez@bodycote.com or visit his LinkedIn.

Soumya Nag
Group Leader of Materials Science and Technology
Oak Ridge National Library

Soumya Nag is in the group leader of the Materials Science and Technology Division at Oak Ridge National Laboratory. His research interest is understanding processing (additive and conventional) — structure (phase transformation across different length and time scales) — property (mechanical and environmental property) relationships in light weight and high temperature structural alloys. 

For more information: Contact Soumya at nags@ornl.gov or visit his LinkedIn.

Cliff Orcutt
Vice President
American Isostatic Presses, Inc.

Cliff Orcutt is vice president of American Isostatic Presses, Inc. and has been involved in more than 200 HIP installations in 25 countries over a 48 year span. Orcutt is Chaiman of the International HIP Committee , helping to organize the HIP22 and HIP25 conferences to spread HIP knowledge. 

For more information: Contact Cliff at corcutt@aiphip.com or visit his LinkedIn.

Victor Samarov
Vice President of Engineering
Synertech PM

Victor Samarov is the vice president of Engineering for Synertech PM. He has a masters degree in mechanical engineering from MPTU in Russia and a Ph.D. and full doctor’s degree from VILS Russia. He has spent over 45 years in PM HIP, and has over 250 publications and over 50 issues patents. With more than 45 years of experience in powder metallurgy and hot isostatic pressing (PM HIP), he has authored over 250 publications and is the holder of more than 50 patents. 

For more information: Contact Victor at Victor@synertechpm.com or visit his LinkedIn.



Heat Treat Radio #126:  HIP Finds New Life in Modern Manufacturing Read More »

Heat Treater Expands Furnace Operations and Nadcap Readiness

A metal heat treater is expanding their operations with a new vacuum furnace. The high-pressure quench vacuum furnace will be used for a wide range of processes such as vacuum hardening, tempering, solution treatment, aging, annealing, brazing and high-pressure gas quenching, servicing the automotive, aerospace, toolmaking and machinery sectors.

Shital Vacuum Treat will receive the furnace from SECO/WARWICK, and it will comply with the NADCA (North American Die Casting Association) global standard for the heat treatment of tools and dies and enable faster preparation for NADCAP certification.

The single-chamber Vector vacuum furnace will be equipped with an advanced 15 bar (abs) gas cooling system, enabling rapid and uniform cooling of loads with complex geometries. It features a round heating chamber with high temperature uniformity ±5°C (9°F), convection heating up to 850°C (1562°F), and a vacuum system based on Leybold mechanical and Roots pumps.

“SECO/WARWICK is not just a supplier – they are part of our family. The new furnace will allow us to increase our production capacity and serve customers better. Quality and repeatability are paramount for us…Thanks to high-pressure cooling and the ability to work with different process gases, the furnace fits perfectly with the requirements of a commercial hardening plant that serves clients from various industrial sectors. Its NADCA compliance and readiness for Nadcap certification allows us to provide services to clients from the most demanding industries, such as aerospace and automotive,” commented Vilas Kolekar, marketing director for Shital Vacuum Treat Pvt. Ltd.

Shital Vacuum Treat Pvt Ltd in the Indian market not only provides comprehensive heat treatment services but also acts as a technology advisor. 

Press release is available in its original form here.

Heat Treater Expands Furnace Operations and Nadcap Readiness Read More »

Modernizing TUS Tuning on Heat Treat Furnaces

Maintaining precise temperature uniformity is a cornerstone of pyrometry compliance and part quality in heat treating. Yet, traditional manual tuning of multi-burner furnaces is slow, labor-intensive, and prone to inefficiencies due to nonlinear system responses.

In this Technical Tuesday installment, Ben Witoff, manager of Information Systems and Data Strategy for Fives North American Combustion, Inc, outlines a new linearization-based approach to combustion tuning. This approach offers a data-driven method to shorten uniformity adjustments, improve survey outcomes, and elevate furnace performance to higher AMS2750H classes with greater repeatability and less operator intervention.

This informative piece was first released in Heat Treat Today’s October 2025 Ferrous & NonFerrous Heat Treatments and Mill Processing print edition.


The Manual Uniformity Tuning Model

Heat treat furnaces require precise combustion system tuning to produce high-end parts for aerospace, automotive, and construction industries. Temperature uniformity surveys (TUS) are the accepted industry standard for verifying the quality of these metal processing furnaces. Current standards such as AMS2750H specify a temperature uniformity that must be maintained inside the furnace work zone. End users, like Boeing, GE, and Pratt & Whitney, have mandated these temperature uniformity quality standards for their suppliers who heat treat components for their products.

Today’s furnace and combustion system TUS tuning methods are slow, inefficient, and outdated. These methods require skilled technicians to make precise, manual adjustments to single components in an iterative fashion. Adjustments require this recursive approach because the system of equations governing an industrial furnace’s heat distribution is nonlinear — an adjustment in one part of the furnace system will require tweaking the set up in other area(s).

In the typical case of a multi-burner furnace which has more than one temperature measurement point, the temperature distribution across a measurement array is not directly proportional to the change in a single burner’s firing rate. Due to the system’s nonlinearity, each independent tuning adjustment has incidental, cascading downstream effects on the rest of the system. Every attempt to resolve temperature disparity in one area of the furnace can consequently bring another area out of compliance.

Reinvention of the Tuning Process

Fives North American Combustion, Inc. (FivesNA) has developed a solution that shortens the time of the temperature uniformity tuning process when used before each TUS and optimizes the furnace temperature uniformity. The North American CertiFire panel implements a patented (Robertson and Dzik 2024) temperature mapping algorithm that creates a linear approximation of any furnace’s system of equations, regardless of its geometry or complexity. Once linearized, the temperature distribution can be resolved through simultaneous adjustments.

The temperature mapping algorithm creates a response matrix that correlates changes to the furnace’s heat inputs with changes in the steady-state distribution of heat throughout the furnace’s work zone. A thermocouple array is used to measure the work zone’s three-dimensional temperature distribution while the furnace’s burners are modulated. It is critical to the accuracy of this response matrix that the burner modulations are precise and repeatable. To accomplish this, actuated gas valves are inserted in the gas line to individual burners taking the place of a manually adjusted limiting orifice valve.

Each individual burner modulation has its own characteristic effect on the entire work zone’s temperature distribution. Figure 1 shows two different burner modulations and Figure 2 shows the resulting furnace temperature distribution over the same period. Nine thermocouples were placed on a rack within a furnace in accordance with the AMS2750H standard for this furnace volume and class, with eight thermocouples at each of the cubic work zone’s vertices and one in its center (SAE International 2022, p 44, Table 17).

Figure 1. Two different burner modulations (Source: FivesNA)
Figure 2. Temperature response to two different burner modulations (Source: FivesNA)

The firing rate of each burner was increased to a fixed amount for a set number of minutes. The second burner was not adjusted until the work zone’s bulk temperature returned to the baseline average temperature. The two burners noted in Figure 1 were firing in the same plane, several feet from one another. Despite the burners’ close proximity and similar adjustments, their effects on the temperature distribution shown in Figure 2 are uniquely different. Not only does the overall rate of temperature change differ between the curves, but so do the individual thermocouple reactions. Thermocouple 5 (shown in orange), for example, shows the largest change in temperature for the first burner’s modulation, but experiences a much weaker response during the second burner’s modulation.

Mathematical Approach

The linear approximation of the furnace’s system of equations can be written as shown in Figure 3. Where vector T represents the temperatures of q thermocouples, vector B represents the bleed valve modulations of r burners, and response matrix K represents their relationship. By compiling each of these burner modulations and their resulting temperature effects, the furnace’s unique response matrix can be calculated using the formula shown in Figure 3.

Figure 3. Linearized furnace equation and response matrix creation

Once the response matrix is known, the linearized furnace equation can be reversed. By dividing a vector of thermocouple temperatures T by the response matrix K, the equation yields a vector of automated burner gas valve positions B. In a steady state furnace, starting with a vector ΔT representing the required changes in temperature for each thermocouple to reach the survey temperature, this equation can solve for ΔB, the necessary burner gas valve adjustments to achieve temperature uniformity.

The process of training entails the CertiFire map out the general valve positions needed to bring the furnace close to uniformity. Metaphorically, it is writing the manual of the furnace’s behavior which takes time to develop (a few hours). The tuning operation, which is the next and final step after the training, is like reading the manual and applying the guidelines set by the training. This process takes only a few minutes to dial in the valve positions for improved uniformity, as discussed below in the case study.

Case Study: SIFCO Industries, Inc. – Cleveland, Ohio

SIFCO furnace 8001 is a single zone box furnace with four high velocity burners firing above the load on the left wall of the furnace and four high velocity burners firing through piers below the load on the right side of the furnace. All burners were configured with a cross-connected variable ratio regulator. The combustion air was fixed for fuel-only turndown, and furnace control was achieved through a single impulse air bleed valve, which affected all regulators equally.

Adding the linearizing technology to furnace 8001 required the installation of eight actuated gas valves, replacing the existing manually adjusted limiting orifice gas valves, and a PLC subpanel. This added subpanel controls each motorized actuator independently. To drive the actuators, the subpanel was wired with two inputs from the existing panel: the tuner control variable (CV) over a 4-20mA signal, and the controller set point (SP) over ModbusTCP. The existing control panel was left in-place and is still the primary furnace control interface.

Pyrometry

Furnace 8001 is certified according to the AMS2750H pyrometry standard at the following three temperature SPs: 900°F, 1500°F, and 2100°F. Additionally, the survey process requires first holding the furnace 100°F colder than each SP (800°F, 1400°F, and 2000°F) before increasing the temperature to the desired production SP to prevent overshoot.

According to the AMS2750H standard, the furnace’s internal volume requires nine type-K thermocouples placed at each vertex of the cubic work zone and one at the geometric center for temperature measurements during certification. Furnace 8001 had historically been certified as a Class-III furnace (±15°F). The client’s goal was to reduce the overall temperature span at each of the six SPs to move furnace 8001 to AMS7250 Class-II (±10°F).

Installation Overview

The solution was deployed on furnace 8001 the week of March 31, 2025. Six SPs across four calendar-days (April 4–7) were trained and tuned. The training and tuning algorithms run unattended, so the estimated labor hours to set up and run the process at all six SPs was approximately two hours.

Example Training Experience – 800°F

Training at 800°F ran from 7:52 a.m. to 10:16 a.m. on April 5, 2025, for a total of 2 hours and 24 minutes. The furnace PID tuner was disabled for this training, and each burner’s actuated gas valve was locked in place at its last position. One at a time, each automated burner gas valve was opened by 50% to allow more fuel to flow for three minutes before lowering back to its initial position for 15 minutes. An adjustment amount of 50% was arbitrarily chosen to elicit a strong temperature response.

As each burner’s firing rate was adjusted, a unique temperature characteristic was measured across all 12 thermocouples (SIFCO requires three additional thermocouples for its TUS). The difference in each thermocouple’s temperature rate of change and amplitude is the foundation for the training algorithm’s furnace map.

Example Tuning Experience – 800°F

After the 800°F training was completed, three tuning iterations spaced eight minutes apart at 10:40 a.m., 10:48 a.m., and 10:56 a.m. on April 5, 2025, were conducted. The result of the tuning iterations was a reduction in the temperature span (hottest minus coldest) from 20.2°F to 5.3°F, and a reduction from +4.7°F, -15.5°F to +1.3°F, -4.0°F with respect to the SP, well within the range of an AMS2750H Class-I furnace.

Figure 4. Thermocouple temperatures during 800°F tuning (Source: FivesNA)

The temperature range, shown in Figure 4, illustrates the initial span on the left half of the chart. A clear reduction in span can be noted at the inception of the first tuning iteration around the 10:40 a.m. mark. Note how not only are the coldest and hottest thermocouples brought in towards center, but the overall spread is also closer centered on SP. The same process was done for five additional SPs yielding the data in Table 1.

SP [°F]Operating TimeTemperature Span [°F]SP Variation [°F]Effective AMS2750 Class
TrainingTuningInitial SpanTuned SpanInitial SPVTuned SPV
8002.4h15m20.25.3+4.7, -15.5+1.3, -4.0Class-I
90010m6.35.7+1.9, -4.4+1.5, -4.2Class-I
14002h1h42.99.7+22.7, -20.2+4.6, -5.1Class-II
150010m11.911.0+9.0, -2.9+7.2, -3.8Class-II
20002.4h25m21.311.5+13.9, -7.4**+3.4, -8.1**Class-II
21008.5h*28.69.0+20.1, -8.5**+4.8, -4.2**Class-I
* Tuning at 2100°F was left to run overnight to test the effectiveness of longer hold times.
** Bulk furnace temperature read on average 20°F hotter at 2000°F and 2100°F than the controller SP. Reported SP variations are referenced to the median thermocouple instead of controller SP.

Note that the training was only needed for three temperatures. Since this initial data was captured, SIFCO has conducted three monthly TUS surveys. Prior to each survey, only tuning by the Certifire at the required temperatures was performed. The simplicity, efficiency, and accuracy of the linearizing technology ensures the subsequent client TUS will easily pass and maintain Class II uniformity.

Operating this linearizing technology does not violate furnaces with multiple temperature survey temperatures per AMS2750H because the valve positions are repeatable and maintain the original settings and pressures from the tuning prior to the TUS and will remain in that position until the next tuning (SAE International 2022, Section 3.5.4.1.1k).

Conclusion

Figure 5. Nick Klusty of SIFCO Forge

The adoption of linearization-based combustion tuning represents a significant step forward for the heat treat industry. SIFCO’s Facilities & Maintenance Manager Nick Klusty reflected on their new capabilities, saying, “We had been struggling to maintain Class III on this 8001 furnace for years. It took days to tune the furnace in preparation for every monthly TUS. Now it literally takes minutes. The North American CertiFire tunes so much better than we could ever achieve by hand. So good that we now have a second furnace available for Class II work, which opens up a new channel for production saving us the time and money of using outside services to heat treat Class II products.”

By replacing manual, iterative adjustments with a data-driven, repeatable process, furnace operators can achieve tighter temperature uniformity in less time, reduce the risk of failed surveys, and expand furnace capabilities to higher AMS2750H classifications. Beyond compliance, this approach enhances process stability and operational efficiency, ensuring that heat treaters are better equipped to meet the increasingly stringent demands of aerospace, automotive, and other critical industries.

References

Robertson, T., B. Witoff, and J. Dzik. 2024. Method and Apparatus for Improving Furnace Temperature Uniformity. U.S. Patent 12,104,788, filed October 1, 2024.

SAE International. 2022. AMS2750H: Pyrometry. Warrendale, PA: SAE International.

About The Author:

Ben Witoff
Manager, Information Systems and Data Strategy
Fives North American Combustion Inc.

Ben Witoff is the manager of Information Systems and Data Strategy at Fives North American Combustion Inc. After founding the company’s data engineering department in 2019, his work focuses on the development of IIoT-enabled combustion technologies and integrating data connectivity and advanced analytics into industrial processes. A Class of 2023 Heat Treat Today 40 Under 40 honoree, Ben has also been a guest on Heat Treat Radio Episode #77: Algorithmic Combustion Tuning with Justin Dzik and Ben Witoff at Fives.

For more information: Contact Ben Witoff at ben.witoff@fivesgroup.com.

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MTI Technical Standards Committee Meets at Nadcap

The Metal Treating Institute (MTI) Technical Standards Committee met to advance industry initiatives at a Nadcap meeting in Pittsburgh, PA. Critical issues which shape the heat treatment industry’s technical standards and audit compliance were addressed.

The meeting provided a collaborative platform for MTI members and technical leaders to exchange updates, align on upcoming revisions, and identify priority actions related to key AMS and ASTM specifications and Nadcap audit compliance.

“Our Technical Standards Committee plays a vital role in ensuring MTI members remain informed, compliant, and at the forefront of technical excellence,” said Tom Morrison, CEO of the Metal Treating Institute.

Highlights of the discussion included:

  • AC7102 Technical Comments: Review and clarification of current interpretations and their impact on member audits.
  • MTL Update: Insights into the latest developments from the Materials Task Group (MTL) and implications for ongoing audit cycles.
  • Audit Planning: Discussion of potential cutting days for audits to improve scheduling efficiency and reduce operational disruptions.
  • Product Impact and Auditor Training: Evaluation of recent updates in auditor training and product-impact assessment to ensure consistency across facilities.
  • AMEC and Commodity Committee Collaboration: Updates from AMEC and engagement with commodity committee sponsors to strengthen standard alignment efforts.
  • RAIL 387 Discussion: Review of ASTM hardness testing recommendations as potential requirements within future revisions.
  • AMEC Spec Updates: Deep dive into specifications currently under review, including:
  • AMS 2759: Cleaning Requirements
  • AMS 2759/1/5/7/8/9, 2769, 2753, 3025, 2771, 2761, and 81200 (Titanium & Raw Materials)
  • Turning ARPs to AMS Specs: Continued efforts to transition Aerospace Recommended Practices (ARPs) into full AMS specifications for greater clarity and industry consistency.
  • Spec 13100 and CMMC: Examination of updates to AMS 13100 and the integration of Cybersecurity Maturity Model Certification (CMMC) requirements across supplier operations.

The committee also gathered member input through “Table Questions” which invited attendees to share challenges in audit preparation, findings management, and upcoming questions for the Heat Treating Task Group (HTSTG) meeting.

Press release is available in its original form here.

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Our People

Heat Treat Today publishes twelve print magazines a year and included in each is a letter from the editor. This letter is from the September 2025 Annual People of Heat Treat print edition. In today’s letter, Bethany Leone, managing editor at Heat Treat Today, shares about the value of people in the heat treatment publication industry, highlighting individuals in the Heat Treat Today family.


We’re in business because people matter. Heat treating just happens to be our industry — which means we like making things hot (and then cold). But at our core, our business is people.

The Business of People

When I ask someone their favorite thing about the heat treating industry, most of the time, the answer is “the people.” Engineers, operations managers, sales reps, and operators all echo the theme.

Why is that? Maybe it’s the strong family values found in many family-founded, family-run operations. Or maybe the behind-the-scenes nature of the discipline draws a more people-focused crowd. It could be that the slower-paced, deliberate innovation attracts people motivated by collaboration more than competition. I’m not sure.

For whatever reason, it is a hallmark to our industry that those from various backgrounds and experiences can come to feel like family.

Welcome to the Family

Over the past year, we’ve welcomed several new individuals to the Heat Treat Today family. Each of them provides essential skills and abilities to making this publication helpful to you.

Jake Romano joined us in the summer of 2024. He embodies so many of our core values that it feels like he’s been here longer than just a year. Jake’s detailed eye for creative problem-solving has allowed our Heat Treat Radio podcast to reach new heights, funneling robust interviews to you seamlessly every month. He never fails to step up to the plate if time is of the essence and does so with the utmost professionalism and an ear for a good story: “My favorite thing that I’ve learned about the industry is just how diverse it is. There are so many people with fascinating backgrounds and reasons for joining the industry and I’ve been enjoying hearing their stories!”

Kelsha Wells has been the mastermind behind social media since fall of 2024 and recently coordinated the 40 Under 40 nomination process. The fruits of her labors are seen daily, connecting industry news and technical updates to you via social media. “From day one, I was struck by how incredible everyone is, not just in their talents, but in their willingness to support one another, celebrate wins, and work together seamlessly. That impression has only grown stronger over the past year.” This magazine edition is particularly special as she gets to see the many worthy young people featured on pages 36 to 71. She also supports various marketing campaigns for Heat Treat Today.

Michele Shaller found us through our legendary Laura Miller (now retired… we think). Michele assumed her position as editorial specialist in late-winter 2025. Every article you see in the print edition, every Heat Treat Radio transcript, and every, “hey, could you look at…?” piece of material gets an eagle-eye review by this whirlwind editor. Additionally, she is the editorial caretaker of several platforms, including the monthly e-newsletters.

Tiffany Ward connected with us in early spring 2025 and has been generating and formatting timely technical content for our website and Heat Treat Daily readers ever since. If you’ve ever had to scrap a heat treat plan and pivot fast under pressure, you have an idea of what Tiffany’s workday looks like every day. Can you say “pivot”?

Hamilton Pearman stumbled across the heat treat industry in 2014 and took a hiatus for a few years. Recently, he has returned, and in late-spring 2025, Hamilton assumed a sales role for Heat Treat Today’s European connections. Hamilton observed that the heat treat industry is like a large friendly family, “and that’s such a relief in the world we live today… Heat Treat Today is one the best examples of what I mean. Family, technical, focused, and yet still friendly.”

Mariah Roth, stepping into the critical role of administrative assistant as of this summer 2025, addresses the immediate challenges that our team faces. Fittingly, she commented the following: “Since joining the team, [I’ve been] realizing and affirming just how small the world is — this is something my grandpa had always said. The older I get, the more I understand this phrase. At the same time, I’m always learning how much I don’t know about the world. Coming from a metallurgy background to a heat treat industry, and now to a heat treat magazine company has really brought me full circle.”


Bethany Leone
Managing Editor
Heat Treat Today
Contact: Bethany Leone at bethany@heattreattoday.com



Our People Read More »

38 Heat Treating Furnaces for Aerospace

A U.S. Air Force contract has been awarded for 38 advanced aerospace heat treating furnaces. The furnaces will enhance mission-critical aircraft maintenance capabilities at bases across the United States and overseas.

Phillips Corporation Federal Division and DELTA H® Technologies will provide the furnaces. Of the 38 are 13 Model DCAHT®-181248-1200/500-MIL units and 25 Defender Series Model DEF-DC-RH-242436/1200-CH-242436/1200 units. Deliveries are scheduled over the next year to provide the USAF with heat treating capacity for aviation-grade metals to meet AMS2750H compliance and NAVAIR TO 1-1A-9 standards.

“Phillips Federal is honored to support the U.S. Air Force through this partnership,” said Kelley Padham, president of Phillips Corporation, Federal Division. “Our collaboration with DELTA H Technologies continues to expand the boundaries of advanced manufacturing for the Department of Defense — empowering readiness, resilience, and rapid innovation wherever our warfighters serve.”

Service member team working with new Delta H furnace
Source: Delta H Technologies

Richard Conway, director and CTO of DELTA H Technologies and a U.S. Air Force veteran, added: “Ten years ago, the Air Force asked us to help solve a problem. As an engineer and veteran, it became a personal mission to provide the best heat treating solutions possible. Today, knowing the USAF relies on DELTA H and Phillips Federal for this critical technology is deeply humbling.”

The DCAHT® Model has dual convection-heated chambers with certified TUS work volume at 18” W × 12” H × 48” L. The lower chamber operates to 1200°F for aluminum solution heat treating with a roll-away quench tank, and an upper chamber which operates up to 500°F for aluminum aging.

The Defender Series Model has dual TUS-certified work volumes at 24” W × 24” H × 36” L. The convection chamber operates between 200°F–1200°F with rapid cooling from 1000°F to <200°F in under 30 minutes, enabling complete solution heat treating, annealing, and aging (T6). The radiant chamber operates between 1000°F–2000°F, with inert gas atmosphere capability.

Press release is available in its original form here.

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IperionX Receives $25M to Accelerate Titanium Production

Iperion X has received $25 million from the U.S. Department of War to support the build-out of a resilient, fully integrated, and low-cost titanium supply chain. The funds will be applied to the scale-up of production to 1,400 tpa at IperionX’s Titanium Manufacturing Campus in Virginia.

The award has come through the Industrial Base Analysis and Sustainment (IBAS) program and is part of a $42.5 million obligation expected to be granted over time. The IBAS program is designed to reinforce U.S. defense supply chains mineral-to-metal titanium that reduces reliance on imports and establishes a secure, uninterruptible domestic source of critical materials.

This latest obligation follows prior tranches of $12.5 million and $5 million, which funded long-lead items for titanium manufacturing equipment and to advance the Titan Critical Minerals Project in Tennessee.

IperionX is an American titanium metal and critical materials company that uses patented metal technologies to produce high performance titanium alloys, from titanium minerals or scrap titanium, at lower energy, cost and carbon emissions. Their Titan critical minerals project is the largest JORC-compliant mineral resource of titanium, rare earth, and zircon minerals sands in the United States. Titanium metal and critical minerals are essential for advanced U.S. industries including space, aerospace, defense, consumer electronics, hydrogen, automotive and additive manufacturing.

Press release is available in its original form here.

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Heat Treat Humor: Heat Treatment For Your Funny Bone

Get your kicks out of today’s edition of Heat Treat Humor, featuring jokes from Publisher Doug Glenn, Heat Treat Today editors, and contributions from around the industry.

If you have a heat treatment joke to share please forward it along for the humor enthusiasts here at Heat Treat Today by emailing editor@heattreattoday.com. It may just end up being featured!


1. Why did the steel need therapy after quenching? It had too much unresolved stress. 

Which happens to any of us when we’re not treated right.

2. Why don’t metals gossip during annealing? They’re too busy relaxing.

Cue the shamisen music.

3. What did the furnace say to the cold titanium? You need to warm up to change.

The titanium felt it’d be hardened by the experience.

4. Why did the aluminum fail its heat treatment exam? It lost its temper under pressure.

Don’t be like aluminum.

5. What’s a heat treater’s favorite genre of music? Heavy metal.

And their favorite band? Metallica.

6. Heat treatment impacts almost every faucet of our lives.

It’s far reaching.

7. Why did Heat Treat Joe burn out in his job? He didn’t take enough time for stress-relief.

A mistake any of us can make.

8. Why did the metal fail its quenching process? Because it wasn’t all it was cracked up to be.

We and metal have that in common.

9. What kind of worship does a heat treater like? Metalliturgical.

Honey for lovers of the refiner’s fire.

10. Why did the knife adjust so easily to marriage? It had tempered expectations.

And that’s a wrap!



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Vacuum Furnace Boosts Aerospace Component Production

A single-chamber vacuum furnace will be provided to a manufacturer in the aerospace industry. The new furnace will expand their production capacity of aircraft gear manufacturing.

Maciej Korecki
Vice President of Business of the Vacuum Furnace Segment
SECO/WARWICK

“For decades, we have been working for the aerospace industry and continuously improving our equipment to not only meet high quality standards but also to ensure maximum efficiency. For manufacturers of aircraft and helicopter parts, we almost always prepare unique solutions tailored to defined needs,” shared Maciej Korecki, vice president, Vacuum Segment of SECO/WARWICK group, which is providing the furnace. SECO/WARWICK is an industrial furnace technology provider with North American locations.

“Thanks to the inverter control, we can activate the optimal cooling power at the appropriate stage of the process. A major advantage of this device is its low heat loss and excellent temperature distribution in the graphite heating chamber, which is resistant to rapid wear and simple to operate and maintain,” says Paweł Okinczyc, sales manager at SECO/WARWICK.

The single-chamber Vector vacuum furnace enables the heat treatment of large components, while maintaining a compact design. The furnaces in this line are equipped with convective heating, improving heat transfer efficiency during lower temperature heating; directional cooling, allowing problematic components in terms of shape to be cooled in different ways; and isothermal hardening, enabling better cooling process control through enhanced charge temperature management and frequency converter-based fan control.

Press release is available in its original form here.

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What Is Hydrogen Embrittlement? Part 2

Ask The Heat Treat Doctor® has returned to bring sage advice to Heat Treat Today readers and to answer your questions about heat treating, brazing, sintering, and other types of thermal treatments as well as questions on metallurgy, equipment, and process-related issues.

This informative piece was first released in Heat Treat Today’s October 2025 Ferrous & Nonferrous Heat Treatments/Mill Processing print edition.

In today’s Technical TuesdayDan Herring continues his exploration of what hydrogen embrittlement is by contrasting it with other forms of embrittlement. Learn how to identify these various forms of brittle intergranular failure below!


We continue our discussion from last month concerning hydrogen-assisted cracking (aka hydrogen embrittlement) by looking at closely related phenomena, often mistaken for hydrogen embrittlement. Let’s learn more.

As a brief recap of what we discussed last month, the severity and mode of the hydrogen damage depends on:

  • Source of hydrogen — external (gaseous) or internal (dissolved)
  • Exposure time
  • Temperature and pressure
  • Level of residual and applied stresses
  • Type of alloy and its production method
  • Method of heat treatment
  • Treatment of exposed surfaces (barrier layers, e.g., oxide layers as hydrogen permeation barriers on metals)
  • Final treatment of the metal surface (e.g., galvanic nickel plating)
  • Presence of chemicals that may react with metals (e.g. acidic solutions)
  • Number of discontinuities in the metal

There are, however, several other embrittlement mechanisms that are often mistaken for hydrogen embrittlement and we will explore these here.

Quench Embrittlement

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Many high hardenability steels (e.g., 4140, 4340, 52100) are susceptible to a form of brittle intergranular failure from a phenomenon known as quench embrittlement. Under tensile or bending stress, higher carbon steels are susceptible to intergranular fracture in both the as-quenched condition and/or after low temperature tempering — generally considered “safe” from traditional embrittlement. A transition from ductile to intergranular fracture in martensitic steels having greater than 0.5% C can be embrittled even when tempered at low temperatures.

This phenomenon is different from tempered martensite embrittlement (TME) or temper embrittlement (TE), as explained below, as embrittlement occurs before tempering. The issue is exacerbated by the presence of certain embrittling elements (e.g., P, S, As, Sb, Sn, Pb) solely or when their combination reaches a high enough percentage (typically, 0.10%).

Temper Embrittlement

In broad based terms, TE involves a reduction in the normal ductility of a metal due to a physical or chemical change. TE is characterized by reduced impact toughness and occurs in certain quenched and tempered steels and even in ductile irons with susceptible compositions. This form of embrittlement does not typically affect room temperature tensile properties but causes significant reductions in impact toughness and fatigue performance. Although normally associated with tempered martensite, it can also occur if the matrix is tempered to the fully ferritic condition.

Types of Temper Embrittlement

When tempering steel, several types of embrittlement must be avoided. The first type, TME, is an irreversible phenomenon that can occur within 200−400°C (390−750°F). Years ago, it was called “blue brittleness” for the steel’s surface oxidation appearance, but this term is misleading since it can occur at temperatures below the onset of a blue coloration on steel.

Figure 1. Fracture modes in hardened steels

The second type is TE, a reversible phenomenon that occurs when steels are heated in and/or slow cooled through the temperature range of 375−575°C (705−1070°F).

Why Does it Happen?

TME and TE are examples of intergranular embrittlement. A common factor in such failures is the presence of elements that segregate to the grain boundaries. The chemical reaction rate or kinetics of segregation are such that they exhibit “C” curve behavior in the 350−550°C (660−1020°F) range; in other words, segregation does not occur uniformly. Both types of embrittlement are in part related to grain-boundary segregation of impurity elements (e.g., As, P, Sb, Sn), and both develop during thermal processing after austenitizing and quenching to martensite, usually indicated by an upward shift in ductile-to-brittle transition temperature.

TME is thought to result from the combined effects of cementite precipitation on prior-austenite grain boundaries or interlath boundaries and the segregation of impurities at prior-austenite grain boundaries. By contrast, TE is thought to be caused by the formation of carbides on decomposition of martensite, in particular, precipitation of carbides in the form of films at grain boundaries. At higher temperatures of tempering, this film disappears and cannot be restored on repeated heating at 250−400°C (480−750°F).

Which Steels Are Affected?

All steels are susceptible, so the real question becomes how susceptible and what factors affect that susceptibility. For example, while plain carbon steels may contain some of the same impurity elements that will cause the embrittlement phenomenon to occur in other steels, the segregation of these elements is often enhanced by or caused by the presence of other alloying elements in substantial quantities. As a result, alloy steels, in general, have more susceptibility than carbon steels.

It is important to understand that the degree of embrittlement is affected by the prior austenite grain size and hardness. So, if we are dealing with a fine-grained plain carbon steel of low hardness, it may not experience embrittlement symptoms despite its phosphorous content, whereas a more highly alloyed Cr-Ni steel used at higher hardness is more susceptible to its impurity content.

Widely used alloying elements, such as chromium, nickel, and manganese, tend to promote TE with the highest embrittlement effect observed in Cr-Ni and Cr-Mn steels. Small additions of molybdenum (0.2-0.3%) can diminish TE, while greater additions enhance the effect. TE can be prevented by keeping silicon and phosphorus levels as low as possible, adding up to 0.15% molybdenum and avoiding the embrittlement heat treating conditions.

Susceptibility also depends on impurity control and here is where the steelmaking process is critical. For example, in plain carbon and Cr-Mo steels (those with no Ni) where phosphorous is the most impactful embrittlement element, the percentage can be controlled by the steelmaking process. In steels that contain significant amounts of nickel, antimony and tin are more potent embrittlement elements. Phosphorous has an effect but not as large as it has in plain carbon and Cr-Mo steels. It should be noted, however, that antimony and tin in plain carbon steels can cause other hot working issues.

How Can We Correct It?

TME is irreversible, and its effects are permanent. By contrast, the effects of TE can be reversed. This is done by re-tempering above the critical temperature of 575°C (1070°F) then cooling rapidly. Impact toughness can be restored. If necessary, this process can be repeated.

A Simple Example

Alloy steel, which is susceptible to TE, will exhibit a relationship such as shown on Figure 2. Note that the impact toughness of quenched steel after tempering at 200−400°C (390−750°F) is lower than that obtained on tempering at temperatures below 200°C (390ºF). If brittle steel tempered in this range is heated above 400°C (750ºF) and transformed into a tough state, a second tempering at 250−400°C cannot return it to the brittle state. The rate of cooling from the tempering temperature range of 250−400°C has no effect on impact toughness.

Figure 2. Effect of temperature on impact toughness

The susceptibility of a given steel to TE depends on a number of factors, including grain size, hardness, steel grade, and the impurity control in the steelmaking process itself. Remember, not all steels and not all steelmaking processes are equivalent.

A heat treaters we must avoid the temptation to temper to a given hardness value without understanding the consequences of our actions. Since we do not have a simple embrittlement test that can be used on the shop floor, we must understand the phenomenon and question specifications that put us into TE ranges.

In Summary

The insidious nature of hydrogen embrittlement continues to cause concern and product failures during processing and during service, but as explained above, there are other heat treatment operations that can result in embrittlement. All of these and others (e.g., aluminum nitride embrittlement, overheating during forging, hot shortness) are responsible for many serious and in some instances catastrophic failures leading to injury or damage. All must be avoided.

References

ASTM International. 2022. ASTM B850-98 (Reapproved 2022): Standard Guide for Treatments of Steel for Reducing the Risk of Hydrogen Embrittlement. West Conshohocken, PA: ASTM International. https://www.astm.org.

Herring, D. H. 2014–2015. Atmosphere Heat Treatment, vols. 1–2. Troy, MI: BNP Media.

Herring, D. H. 2006. “The Embrittlement Phenomena in Hardened & Tempered Steels.” Industrial Heating, October.

Herring, D. H. 2004. “A Heat Treater’s Guide to Hydrogen Embrittlement.” Industrial Heating, October.

About the Author

Dan Herring
“The Heat Treat Doctor”
The HERRING GROUP, Inc.

Dan Herring has been in the industry for over 50 years and has gained vast experience in fields that include materials science, engineering, metallurgy, new product research, and many other areas. He is the author of six books and over 700 technical articles.

For more information: Contact Dan at dherring@heat-treat-doctor.com.

For more information about Dan’s books: see his page at the Heat Treat Store.

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