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Heat Treat Radio #70: Lunch & Learn with Heat Treat Today – Heat Treatment vs. Thermal Processing

Heat Treat Radio host, Doug Glenn, and several other Heat Treat Today team members sit down with long-time industry expert Dan Herring, the Heat Treat Doctor®, to discuss the difference between heat treating and thermal processing. If you’ve ever wondered about the difference – if one actually exists(!), then you’ll enjoy this highly informative Lunch & Learn with Heat Treat Today.

Below, you can watch the video, listen to the podcast by clicking on the audio play button, or read an edited transcript.



The following transcript has been edited for your reading enjoyment.

Doug Glenn (DG):  So, Dan, I want to turn it over to you, but I want to give a context though of what we’re going to be talking about. As you just mentioned, before we hit the record button, we’re pretty heat treat centric in our world, but there are a lot of other thermal processes that go on that aren’t exactly heat treat. We talk about some of them in our publication, not all, so what we’d like to do is turn over to you to talk about the difference between “heat treating proper” and “thermal processing, generally speaking.”

Dan, welcome and thanks for educating us.

Dan Herring (DH):  Well, thanks, Doug, and good afternoon, everybody. First of all, for everyone listening, I hope to cover the basics providing information without confusing everyone. If there are any questions as I go along, please don’t hesitate to ask them. I think it’s always better to have an interactive, back and forth discussion on things.

You are absolutely correct, Doug. we live in a heat treat centric world. I’m going to start off in familiar territory by discussing a little bit about heat treating. Then, we’re going to move into the differences between heat treating and thermal processing.

To give a simple definition of heat treating — simple yet complicated at the same time — is heat treating is the controlled application of time, temperature and atmosphere to produce a predictable change in the internal structure (that means the microstructure to metallurgists) of the material being treated. Now, the interesting part is that heat treating is (a) predictable, which is why metallurgists exists in the world and it is (b) controlled, which is why heat treaters exist in the world, and the darndable thing about heat treating is that it happens inside the metal or the material and, unfortunately, you (c) can’t see the changes that are taking place.

"Let me give you an example, if I can: I’ll hold this up; I don’t know if people can see it that well, but what this is is a helicopter transmission gear."

Let me give you an example, if I can: I’ll hold this up; I don’t know if people can see it that well, but what this is is a helicopter transmission gear. And if we were manufacturing this particular gear, one of the things we would do to measure, if we were successful or to see if we were successful, is to measure the dimensions of the gear that we were actually taking and manufacturing. But in the world of heat treating, because the changes happen inside the material, it’s very difficult to know if the part is good or not. But heat treating has the ability, as we say, to vary the mechanical properties, the physical properties and the metallurgical properties of a material. The problem is that we can change them either for the better or, as most heat treaters know, we can change them for the worst. That’s why there is something called quality control and quality assurance. But I’m drifting away from the main point.

In the world of heat treating, with that definition — the controlled application of time, temperature and atmosphere to produce the predictable change in the internal structure of a material — not only are we heat treat centric in this industry, but we are also often steel or iron and steel centric in this industry. Metallurgists tend to be either ferrous metallurgists (specializing in irons and steels) or nonferrous metallurgists, specializing in things called aluminum, or as the British and Europeans would say, “aluminium,” titanium, and some of the super alloys and things of this nature. The idea being the fact that there are a lot of different materials that can be heat treated.

We often limit ourselves, if you will. But there are parts of our industry that heat treat: for example, precious metals — the golds, the silvers, the platinums and things of this nature. There are also parts of our industry that deal with copper and brass. There are parts of our industry that deal with ceramics which deal with powder metal, if you will. So, one of the things as heat treaters we must remember is that even under just the heat treat umbrella, there are a lot of different disciplines out there. There are a lot of things that we cover, and we look at. There are a lot of different materials that are processed. And again, we think, in general, as heat treaters and probably incorrectly so, we think about what are called “semifinished goods.” What we think about are parts that are manufactured from steel, aluminum, titanium, copper or powder metal. We think of automotive parts, aerospace parts. We think of something like weapons or military equipment, ammunition, firearms. We think of agricultural products, farm implement products and things of this nature. So, one of the things we must be aware of is that there is a whole world outside of our comfort zone, and that is something that we’re going to explore today.

Before I go on, does that make sense to everyone, or does anyone have any questions about the heat treatment side of what we do?

"Heat treating is the controlled application of time, temperature and atmosphere to produce a predictable change in the internal structure (that means the microstructure to metallurgists) of the material being treated." - Dan Herring

DG:  No, I think that makes sense. You mentioned on the inside of the part that things can’t be seen so much. You will probably get to this Dan, but I assume that also includes surface treatments, or would that be something different?

DH:  We’ll talk a little bit about the difference between surface treatments and they fall into an area probably referred, in general, as “coatings” and things of this nature. But that is a good question, Doug- plating and coating and things of this nature.

Also, one of the things about heat treating that seems a little bit, possibly confusing is that heat treaters consider processes like brazing (which is a joining process), and they think of soldering (which is a low temperature joining process), as heat treatments. Similarly, we think of sintering, and we think of heat treatments of powder metal products, or we think of powder metallurgy as falling under the subject of heat treatment because we think so much about sintering. But sintering is a bonding or a  diffusion process. So, heat treaters think of heat treatment, they think of brazing, and they think of powder metallurgy all combined into that big umbrella. For any brazers who are listening, or any powder metal people who are listening — they probably died of cardiac arrest at this moment in time — but, in general, that’s what heat treating does: it considers those separate entities as part of it.

Let’s go on and look at the fact that I can say to you — automotive components, gears, bearings, aerospace components, landing gear transmission boxes, fasteners, screws, nuts, bolts, farm implement equipment -- those are things that commonly come to mind. People don’t often think, for example though, of things like jewelry which is something that is commonly heat treated or “processed,” if you will, more on the thermal processing side. A lot of electronic materials are also thermally processed, and a lot of castings and things done in the foundry industry.

But, as I said, we think of semifinished goods where a semifinished goods-centric/heat treat-centric world; but there are other worlds out there. Let’s kind of talk about them. But mill practices, or what we call “primary metals,” are another area that’s covered, interestingly enough, under heat treating. Because in steel mills and things of this nature, you’ll find soaking pits, for example. In aluminum processing facilities or aluminum foundries, you might find solution heat treating and aging ovens and things of this nature. So, there is, in a very broad or general sense, heat treating also done on the mill or the material production side of things. Again, unless we’re in that industry, we don’t tend to think about it that much. So, we have to.

But, if I also said to you that things like cosmetics are being processed, not heat treated, but thermally treated, if you will.  Or things like cement, or minerals in raw ore, ore materials and things- these all fall in the category of now “thermal processing.”

Let me try to give everybody just a feel for what the different categories of thermal processing are. The number one category, of course, is heat treatment. There is another thermal process . . . . And, by the way, thermal processes are also confused a little bit because we use heat, or we use cold — those are both thermal processes. For all the heat treaters out there, we do things like deep freezing, and we do things like cryo-treatments, cryogenic treatments. Those fall under the umbrella of heat treating. But there are other deep cooling or cooling processes that fall under this umbrella of thermal processing.

Besides heat treatment, thermal processing consists of a few areas which you are maybe familiar with and then again maybe you’re not that familiar with. One of them is calcining which I often call the drying of powders, if you will. This can be in the form of ores, it can be in the form of minerals, it can be in the form of coke (which is a coal byproduct, if you will), it can be in the form of cement. So, there are drying processes that occur under thermal treatment which is in the area of calcining.

There is also a big category called fluid heating where what we’re doing, (and by the way, air is a fluid as well as water and liquids are fluids), so we can turn around and do things like chemical processing which is done at elevated temperature. I had a client that was producing mayonnaise and the mayonnaise has held at 180 degrees Fahrenheit- it is a thermal process, if you will.

Distillation. We won’t talk about alcohol much in the world. I will only comment that all of you think this is a bottle of water, but you could be mistaken about that.

The idea is that fact that fluid heating, calcining, drying, smelting, metal heating in general, curing and forming — which is done a lot on ceramics, on paints, paint drying and things of this nature. There is, just in general, other methods of heating. I’ll give you a simple example: waste incineration. We know that our trash is burned at ultra-high temperatures to reduce emissions, if you will, but avoid going into landfills or, worse yet, dumping it in the ocean and believing that somehow it won’t return to our ecosystem. But incineration is an example of a thermal process.

There are quite a number; there are literally hundreds of thermal processes that are occurring all the time that we don’t, in general, think very much about. Heat treating is typically divided into two general categories — processes that soften a material and processes that harden a material. So, in the category of softening, we think of things like aging, we think of things like annealing, we think of things like normalizing, or even stress relieving (in other words, taking the stress out of material is a softening process).

DG:  Tempering, as well, Dan? Would it be in that?

DH:  Well, tempering, in a sense, could be considered a softening process. It’s a good one. I consider it more a softening process than a hardening process, but it’s typically so intimately linked with hardening that people think of it as a hardening process. But, hardening and case hardening, austempering, and then, of course, brazing which is a joining process, soldering, sintering which is a bonding process, homogenizing (when we talk about aluminum), solution treating (when we talk about aluminum). Solution treating is not a hardening process, interestingly enough- it’s the aging or the precipitation hardening process after the solution heat treatment that is actually the hardening process.

The idea of the fact is that we’re very familiar with those terms; we’re less familiar with coke ovens or waste incinerators or distilling facilities, or things of this nature. We’re not used to processing resins or composite materials, even though there are autoclaves that use a combination of high pressure and temperature to form some of the composite materials that are used in the aerospace industry.

The way I like to think about it is there is a giant umbrella which is called thermal processing. Under that umbrella is a small segment, maybe not so small, called heat treating, and then heat treating is divided into semifinished goods and raw materials (or primary goods), and then it’s subdivided into irons and steels and nonferrous alloys. Now, in my day, when you graduated university, you graduated with a degree in metallurgy. Today, you become a material scientist which means that you’re dealing with composites, ceramics, electronic materials, a whole series of materials outside the realm of just iron and steel and aluminum and titanium, if you will.

The other thing that’s very interesting about our industry, in general, is probably the aspect of energy usage. The thermal processing industry, in general, and this is a rather stunning number, uses, in round numbers, about 38% of the energy produced in the United States. Now think about that as a number. Of all the energy consumed by people in the U.S. or in Canada or in Mexico or anywhere else in the world, two-thirds of it or greater — 40% of it, almost — is used in thermal processing. About 25% is used by transportation, and another 20% or so is used by residential. Then, there’s about 15% used in, what we call, “other” category. But, in thermal processing, which is also true in heat treating, about 80% of the energy comes from natural gas. And only 15%, (round numbers), comes from electricity.

We have to realize that we’re not only, as heat treaters “heat treat-centric,” “iron and steel-centric,”  “aluminum-centric,” but we’re also “natural gas-centric.” Those are staggering numbers to consider. The reason for it, the reason we’re natural gas centric, not only in the heat-treating industry but in the thermal processing industry as a whole, is simply because natural gas is the cheapest energy source available right now. And, these numbers, although they apply specifically to North America, can also apply, if you will, to the world in general. The numbers vary a little bit throughout the world, they may be different in Europe and different in Asia, but not so much that it varies so greatly.

What I’ve tried to cover — and I realize I haven’t left a lot of room for questions here and I apologize for that — but I’ve tried to give you the idea that heat treating is a very important part of a much larger industry that services the manufacturing community.

Let’s open for discussion from anybody.

Dan Herring and the Heat Treat Today team: Karen Gantzer, Bethany Leone, Doug Glenn, Dan Herring, Evelyn Thompson, and Alyssa Bootsma

DG:  That sounds good. Do any of you have questions, at all?

Alyssa Bootsma:  I did have one. I think it was very helpful in understanding everything and the idea that thermal processing is an umbrella and heat treatment is just a part of that really clicked for me. I was wondering if you could talk about calcining a little bit more and what that process actually is.

DH:  Sure. But before I do that, I want to mention one thermal process that I forgot to mention. Because I have a number of clients that work in the baking of cookies, and because I’ve consumed a few of those in my life, I don’t want to forget the baking industry.

DG:  The brewing industry?

DH:  Absolutely! By the way, the brewing hall of fame is located here in Chicago, unless I’m grossly mistaken.

Before we get to far afield, let’s talk about calcining a little bit. A number of powders, whether they be ores or whether they be things like cement or various minerals, are often processed in, what we call, a slurry. They’re processed in a form in which they are either cleaned or washed with water or with different chemicals. As a result, you have a wet mixture of a mineral and, let’s say, water, or in some cases they can be different chemicals, if you will, that go to either clean the minerals or dilute the minerals or things of this nature. But to go to further processing of those minerals, you have to dry them and put them into a form that they can be used. If this makes any sense, then let’s take cement as an example. It’s no good to keep the cement in a slurry because what’s going to happen to the cement? It’s going to dry and harden. So, what you have to do to send it to the consumers is you have to dry the powder, if you will, deliver it to the end-user who will then add liquid to it to once again form it or turn it into liquid cement. Calcining, is really, in simplest terms, to answer the question directly, I always consider it, a powder-drying process.

DG:  Dan, any idea why they call it “calcining?”  I’ve always wondered this.

DH:  Well, in the old days, I believe that limestone, (which is calcium carbonate), and so "calcining" and "calcium" from the calcium carbonate, I think that’s where the name originally came from. A good thing to look up, however- that’ll be my homework assignment.

DG:  There you go. Just as another example of a thermal process, it’s certainly not heat treat, just down the road from where I live, north of Pittsburgh, they have a lot of sand and gravel places. Believe it or not, there is a large, what I would call a, horizontally-oriented “screw furnace” — it’s a cylinder and it just rotates, and inside it’s heated up and they’re just simply burning off the moisture so that they can get the materials, or whatever it is they’re harvesting out of the earth, and get it down to a certain level of moisture so that they can process it. So, sand and gravel. That’s just another area.

Here's another one — and Dan, I want you to hit on glass if you don’t mind, in a minute — but here’s another one where thermal processing is used, which you might not think of, and that’s in the manufacturing of paper production. They’ve got to actually dry the paper and you wouldn’t think of it but they’re passing paper through flame (between flames, not actually in the middle of the flames) simply to dry paper before it goes onto these huge rolls.

One last comment, Dan:  We often talk about energy intensity and how much energy it actually takes to perform a certain process. One of the highest thermally intense processes that is used is not so much a heat treatment, but it is actually the manufacturing of concrete, believe it or not. There is very, very high energy intensity — it takes a lot of gas, in this case, to produce concrete.

But Dan, if you don’t mind, could you hit on glass production? We’re all looking out windows here and the manufacturer of glass is a thermal process.

DH:  Absolutely it is. But before I do that, quickly, that rotary drum that you saw, the one with the screw inside it, if you will, that helps move the powder, if you will, or the sand and gravel through, is a very typical calcining furnace. Rotary drums are also used in the heat treatment industry to process screws and fasteners, nuts and bolts, small products, if you will, typically.

But yes, paper is a good example but glass furnaces, too, where the glass is actually brought up and the sand and other elements, if you will, are melted into glass. Very disconcerting. You may find this interesting but roughly the walls on a glass furnace (I’ve seen 10-20,000-pound glass furnaces) are something like 4 inches thick, holding back all that molten glass. But again, you’re taking glass that is basically silicone dioxide, its sand is a major component of it. In colored glasses, you add different chemicals. Like, for example, if you want to form a bluish colored glass, you might add a copper oxide, for example, which will change or tint the glass to a different color.

You’ve heard of leaded glasses, for example. In the old days you added lead to glass to make it, again, more formable, if you will. But yes, glass furnaces or the manufacture and production of glass is very energy intensive, as well as cement, as is the production of aluminum, by the way, which basically uses electricity, which is why all of the aluminum facilities are located either near hydroelectric or thermal energy like in Iceland, for example, where you have geothermal energy which is used to heat and produce electricity. But yes, glass is definitely an example of a thermal process, as well.

Glass is interesting because we don’t necessarily do a lot of heat treatment of glass, but you may have heard of glass-to-metal sealing, where we’re actually taking a glass and sealing it into or onto a metal component. Like, for example, the site ports of burners where we look in to see the flame — those site ports are made by glass-to-metal sealing. But, in general, yes, melting and production of glass is a thermal process.

DG:  Dan, correct me if I’m wrong, and I could be wrong on this, but cellphones, right? Your glass on the front of that — the reason it is actually quite strong and won’t break is because it’s been thermally processed, a tempering process of some sort, I believe. Correct me if I’m wrong, but isn’t it the thermal process that can make a glass really, really difficult to break?

DH:  It is, plus the fact that glass is a quasi-solid, as we say. It’s a solid but it’s really not; it has more characteristics of a liquid, which, again, makes it more ductile or resistant to things It makes it more shock absorbing, for example. But yes, cellphones and cellphone glass are something I’ve got to do some more research on.

DG:  Right. They’ve got some stuff called “gorilla glass.”

I just want to recap a couple things for our team here and for other people that might be listening: When we talk about heat treat, which is what we’re centered on, it’s helpful for us to know what processes, materials and things that includes, and what processes and materials that doesn’t include, and that’s why this conversation on thermal processing versus heat treat is helpful for us. The way I like to describe it to our team and to most of the people who would be reading our publication or listening to this podcast, is typically Heat Treat Today is not involved with the making of steel but almost everything else after the making of steel we would deal with, almost everything. So, we don’t really do the steel making. Steel making, however, is very much a thermal process but we just don’t cover it. There are other publications that cover that. And we are very much steel-centered; we do aluminum, as well. However, in the aluminum world, we actually do deal with aluminum making. For reasons that basically have to do with the temperature range: the temperature range isn’t quite as high with aluminum making as it is with steel making. So, we do some of that. We don’t do a lot with aluminum making but a lot after aluminum is made. We do a lot of the homogenizing, annealing, solution heat treating and that type of stuff.

So, that is us. In heat treating, we define things like brazing, even though it’s a joining process, we tend to cover it. Soldering we don’t tend to cover because it tends to be a lower temperature. Dan didn’t mention it, but I’m sure he would, is welding: it’s a joining process but it’s not exactly anything we cover either. It’s not what we consider to be heat treating.

There is another joining process that we didn’t cover, and maybe we could hit on it briefly next time, and that is diffusion bonding which, to be quite honest with you, I haven’t done a lot of study on it so it would be interesting to know what that is. I know it’s done in vacuum and under high pressures, I believe, but things of that sort.

At any rate, that what’s we mean when we talk about heat treat — it’s primarily steels, aluminums, titaniums and typically not steelmaking and probably not titanium making either, but aluminum making and everything downstream from that tends to be us, and our temperature ranges tend to be, very generally speaking, 800 degrees Fahrenheit and above, or as Dan mentioned, ­­we can also do some things in the cryogenic range which are subzero temperatures. So, that is us. Everything that falls outside of that we would consider to be a thermal process, which is a lovely thing, but just not our cup of tea.

DH:  Look at this, Doug, a whole new business opportunity for you. With that, I’m extending myself beyond metallurgy, so I’ll quit there.

DG:  Dan, we really appreciate it. We look forward to more of these. We are going to try to do other topics, again, what I would call heat treat 101 type topics, our Lunch & Learn series with Dan Herring, The Heat Treat Doctor®. Dan, thanks a lot, we appreciate your time.

DH:  A pleasure, everyone. Thank you.

For more information:

www.heat-treat-doctor.com

dherring@heat-treat-doctor.com

 

Doug Glenn <br> Publisher <br> Heat Treat Today

Doug Glenn
Publisher
Heat Treat Today


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Heat Treat Radio #70: Lunch & Learn with Heat Treat Today – Heat Treatment vs. Thermal Processing Read More »

Delivery Scheduled for Medical Brazing Heat Treat Solution

Maciej Korecki
Vice President of Business of the Vacuum Furnace Segment
SECO/WARWICK

HTD Size-PR LogoA medical device manufacturer is set to receive a vacuum furnace for annealing and brazing processes at their plant in France. The parts processed in this furnace will include X-ray and radiotherapy equipment among other products that require high quality standards of heat treatment.

The vacuum furnace scheduled for delivery is called the Vector®. "[This furnace] has proven performance in many fields in precision industries such as aviation, automotive and medical branches," commented Maciej Korecki, vice president of the Vacuum Furnace Segment at SECO/WARWICK Group, and international heat treat systems supplier. Korecki continued, "This time, our partner is an expert when it comes to brazing complex components that require high precision."

The high-tech medical industry is one of the most demanding industries in terms of standards, procedures, and process parameters to be met by the equipment involved in the production process. Medical equipment components (e.g., RF components, X-ray tube components, ceramic components) are precision manufactured to the highest quality standards. This is because these components are used for processes that are decisive not only for the quality of treatment, but also for human life.


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“The light at the end of the tunnel” — Monitoring Mesh Belt Furnaces

OCAccording to "Dr. O" – Dr. Steve Offley, product marketing manager at PhoenixTM – temperature control of the heat treatment application is critical to the metallurgical and physical characteristics of the final product, and hence its ability to perform its intended function. Explore today's Technical Tuesday article to find the light at the end of your mesh belt furnace tunnel.

This article first appeared in Heat Treat Today’s February 2022 Air & Atmosphere Furnace Systems print edition.


Dr. Steve Offley, “Dr. O"
Product Marketing Manager
PhoenixTM

Introduction – The Need for Accurate Product Temperature Measurement

Even though modern furnaces are supplied with sophisticated control systems, they are still not always capable of truly giving an accurate picture of the actual product temperature as it passes through the process. Temperature sensors positioned along the furnace give a snapshot of what the environmental temperature is possibly zone by zone. Furnace controllers, as the name suggests, can give confidence that the process heating is performed in a controlled manner but will never give an accurate view of what the actual product temperature is. When monitoring, it is important to be able to distinguish between process and product.

The challenge to any process engineer is understanding how the product heating cycle relates to the operation of the furnace. A furnace environment may be well controlled, but very different product temperatures can be experienced with variation in key properties such as product material, size, shape, thermal mass, and position/orientation in the furnace. Infrared (IR) pyrometers and thermal imagers can provide surface temperature measurements only and require line of sight, so they limit the areas of the product that can be measured. Setup can sometimes be complex considering surface characteristics (emissivity) and process background/atmosphere compensation. As with air sensors, being fixed, typically IR sensors only give information at that specific furnace location which prevents accurate calculation of soak times at critical temperatures. Without additional information, soak times and temperatures may need to be extended well beyond the target to guarantee the heat treat process is completed with confidence with an obvious compromise to throughput and energy conservation.

Product Temperature Profiling

To fully understand the operational characteristics of the heat treat process it is necessary to measure both the environment and product temperature continuously as it travels through the process. Such technique provides what is referred to as a “temperature profile” which is basically a thermal fingerprint for that product in that furnace process. This thermal fingerprint will be unique but will allow understanding, control, optimization, and validation of the heat treat process.

Table 1. Table showing the numerous benefits of thru-process temperature monitoring over traditional trailing thermocouples methodology for a mesh belt furnace

Historically, trailing thermocouples have been the go-to technique for product temperature monitoring. A very long thermocouple is attached to the product in the furnace. The data logger measuring the live temperature reading is kept external to the furnace. Although possible for static batch processes, the technique has significant limitations in a continuous/semicontinuous process, especially mesh belt furnaces (See Table 1).

Fig 1. Robust multichannel data logger designed specifically for thru-process temperature profiling

In thru-process temperature profiling the data logger travels with the product through the furnace. The data logger (Figure 1) is protected by an enclosure, referred to as a thermal barrier, which keeps the logger at a safe operating temperature (Figure 2). Temperature readings recorded by the data logger from multiple short length thermocouples can be retrieved post run. Alternatively, if feasible, the data can be read in real time as the system passes through the furnace using a two-way radio frequency (RF) telemetry communication option. The resulting temperature profile graph (Figure 3) provides a comprehensive picture — product thermal fingerprint — of the thermal process.

Fig 2. Thermal barrier protecting the data logger safely entering the conveyor furnace during the temperature profile run. Barrier size is customized to suit process credentials.

Fig 3. Typical temperature profile recorded for an aluminum CAB brazing line giving a complete temperature history for a brazed radiator at different product locations.(1)

Monitoring Your Heat Treat Process Temperature at the Product Level

Applying thru-process temperature monitoring product temperature measurement can focus on the micro product level which at the end of the day is most important. Static control thermocouples give an environmental temperature of the furnace in a zone, but this only reflects the true temperature wherever the thermocouple is located. This may be some distance from the product and may give some bias to its position if located on one side of the furnace. The thru-process monitoring system allows simultaneous product and/or air temperature measurement directly at the mesh belt. Monitoring can be performed across the belt with thermocouple placement on and in the core of the product and can be made to identify areas of different thermal mass resulting in differing heating characteristics.

A useful strategy to use before looking at the product temperature is to thermally map the furnace. Thermocouples, connected to the data logger protected within the thermal barrier, are positioned across the mesh belt using a mount jig such as that shown in Figure 4. The jig guarantees reliable location of the measurement sensor run to run and adjustment means it can be adapted to different belt widths. Applying this principle, the thermal uniformity of air across the belt width through the entire furnace can be measured.

Fig 4. Thermocouple mount jig allowing accurate positioning of thermocouples (1) across the mesh belt width with adjustment to suit different belt dimensions (2).

Such data can be compared with zone control thermocouples to see what temperature differential the product may be experiencing at the belt level. Temperature imbalances across the belt and hot or cold spots along the process journey can be identified.

Furnace mapping can be further developed to satisfy either CQI-9/CQI-29 or AMS2750F pyrometry standards where a two-dimensional jig is constructed to perform the temperature uniformity survey (TUS).Employing the plane method, a frame jig is constructed to match the furnace work zone with the necessary number of thermocouples to satisfy the furnace cross section dimensions. Temperatures recorded over the working zone are compared to the desired TUS levels to ensure that they are within tolerance as defined in the standards.

Discover the True Root Cause of Your Furnace Problems

When it comes to product quality and process efficiency in any mesh belt furnace applications, temperature monitoring is only part of the story. Gaining an insight into what is physically happening in the product’s furnace journey can help you understand current issues or predict issues in the future, which can be corrected or prevented. To allow true root cause analysis of temperature related issues, it is sometimes necessary to “go to Gemba” and inspect what the product is experiencing, directly in the furnace. This is not always possible under true production conditions.

For a classic mesh belt furnace application such as controlled aluminum brazing (CAB), internal inspection of the furnace is not a quick and easy task. Operating at 1000°F, the cool down period is significant to allow engineers safe access for inspection and corrective action and then further delay to get the furnace back up to a stable operating temperature. Such maintenance action may mean one or two days lost production, from that line, which is obviously detrimental to productivity, meeting production schedules, satisfying key customers, and the bottom line.

In addition to process temperature problems there are many other production issues that can be faced relating to the furnace operation and safe reliable transfer of the product through the furnace. In the CAB process a day-to-day hazard is the build-up of flux debris. Flux materials used to remove oxides from the metal surface and allow successful brazing can accumulate within the internal void of the furnace. These materials are most problematic at the back end of the muffle section of the furnace where, due to the drop in temperature entering the cooling zone, materials condense out. Flux buildup can create many different process issues including:

  • Physical damage to the conveyor belt or support structure requiring expensive replacement
  • Reduction in belt lubricity creating jerky movement and causing unwanted product vibration
  • Lifting of the mesh belt creating an uneven transfer of products causing possible excessive product movement, clumping, or clashing
  • Reduction in inner furnace clearance creating possible product impingement issues and blockages

To prevent such problems, regular scheduled inspection and clean out of the furnace is necessary. This is not a pleasant, quick operation, and requires chipping away flux debris with pneumatic tools. Often requiring a furnace down time of 1 to 2 days, this task is only performed when essential. Leaving the clean-up operation too long can be catastrophic, causing dramatic deterioration in product quality or risk of mid-production run stoppages.

Figure 5. PhoenixTM Optical profiling ‘Optic’ System - Optical Profile View. System adaptable for both temperature and optical profiling.

Optical Profiling – The Efficient Alternative

Optical profiling is a new complementary technique to that of thru-process temperature profiling. The innovative technology allows for the first-time process engineers to view the inner workings of the furnace under normal production conditions. Traveling through the furnace with the products being processed, the optic system gives a product’s eye view of the entire heat treatment journey. A thermal barrier, similar in design to that used in temperature profiling, protects a compact video camera and torch that are used to record a video of what a product would see traveling through the furnace (Figure 5). The principle is just like your car’s dash cam, the only difference being that your journey is being performed in a furnace at up to 1000°F. The resulting video, “Optical Furnace Profile,” shows process engineers so much about how their process is operating without any need to stop, cool, and dismantle the furnace. This allows safe routine furnace inspection without any of the problems of costly lost production and days of furnace down time.

Summary

Monitoring your mesh belt furnace from a temperature and optical perspective allows you to fully understand what truly happens in that black box. Understanding leads to better control, which helps you get the optimal performance out of your heat treat process from a quality, productivity, and energy efficiency perspective.

Don’t get left in the dark. Consider the power of temperature and optical profiling which will literally provide a light at the end of your furnace tunnel!

References:

[1] Steve Offley, “Unveiling the Mystery of Your Al Brazing Furnace with ‘Thru-Process’ Temperature Profiling," Heat Treat Today Magazine, June 2020, p40.

[2] Steve Offley, “Applying ‘Thru-process’ Temperature Surveying To Meet the TUS Challenge of CQI-9.” HeatTreatToday.com. June, 2019. https://www.heattreattoday.com/heat-treat-news/automotive-heattreat-news/applying-thru-processtemperature-surveying-to-meet-thetus-challenges-of-cqi-9/

About the Author:

Dr. Steve Offley, “Dr. O,” has been the product marketing manager at PhoenixTM for the last 4 years after a career of over 25 years in temperature monitoring focusing on the heat treatment, paint, and general manufacturing industries. A key aspect of his role is the product management of the innovative PhoenixTM range of ‘thruprocess’ temperature and optical profiling and TUS monitoring system solutions.

For more information, contact Dr. O at Steve.Offley@phoenixTM.com.

“The light at the end of the tunnel” — Monitoring Mesh Belt Furnaces Read More »

IHEA Monthly Economic Report: Lions, Tigers, and Bears?

"The inventory levels for almost every industrial metal have been as low as they have been in decades and at the same time there has been more demand as industry starts to stage a recovery in key areas."

As we emerge from pandemic slowdowns and disruptions, there are still "lions, tigers, and bears — oh my!" that manufacturers face. The monthly Industrial Heating Equipment Association’s (IHEA) Executive Economic Summary released in February notes that in economic terms, it has been "inflation, supply chain, and labor — oh my!" for several months, but at least two of these may be letting up in 2022.

First, inflation. Inflation is the highest it has been in decades: 7.5%. The report reveals the reasons why this is the case: "For the better part of the last four decades the US was able to essentially export inflation . . . If one was facing higher labor costs and higher production costs the easiest response was to either produce or source overseas where the costs were dramatically lower." Now, many U.S. companies are undoing this in light of rowing costs from overseas suppliers and supply chain upheaval.

And high inflation rates and the supply chain are recovering. While the "stimulus effort dumped the equivalent of the Japanese GDP into the hands of consumers," they were unable to continue normal purchasing habits, and cash tied up in savings contributed to inflation. But now, consumers have fed most of that cash back into the economy. Additionally, producers are slowly catching up with demand, which will stabilize commodity costs from contributing to inflation. The last contributing factor to inflation is less positive; the report notes that cost of labor -- having risen over the course of the pandemic -- are unlikely to come down, which will likely inhibit the full return "back to normal." Still, even the supply chain's 2021 recovery is cause for celebration, having been "far more aggressive than anyone had expected and producers were unprepared. They are starting to gain ground and by mid-year they are expected to have caught up with the majority of current consumer demand. The primary issue now is China."

Steel consumption will surge later this year as orders from Congress's infrastructure spending plan are placed.

Unfortunately, the retirements of key workers as well as a simple lack of hands put pressures on labor costs. Paired with increased wage demands, "Skilled workers have more leverage than they have ever had and the number one means by which companies are expanding their workforce is by poaching from one another." This leads to paying new hires and longtime employees higher wages to disincentivize job hopping.

Anne Goyer, Executive Director of IHEA
Anne Goyer, Executive Director of IHEA

The report concludes, "labor costs soared by over 5.0% last year and these costs are heading in the same direction in 2022."While we may not be out the thicket yet, there is still hope along two of the three economic indicators.

Check out the full report to see specific index growth and analysis which is available to IHEA member companies. For membership information, and a full copy of the 12-page report, contact Anne Goyerexecutive director of the Industrial Heating Equipment Association (IHEA). Email Anne by clicking here.


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This Week in Heat Treat Social Media


Welcome to Heat Treat Today's This Week in Heat Treat Social MediaYou know and we know: there is too much content available on the web, and it’s next to impossible to sift through all of the articles and posts that flood our inboxes and notifications on a daily basis. So, Heat Treat Today is here to bring you a hot take of the latest compelling, inspiring, and entertaining heat treat chatter from the world of social media.

We're looking at helicopters for space, celebrations in heat treat, quick diagrams to keep you on your toes, and much more.

If you have content that everyone has to see, please send the link to editor@heattreattoday.com.


1.  Aerospace Happenings

We're moving faster and further into the journey beyond earth. . . "At the end of Ingenuity’s mission, Perseverance will drive off, leaving the little helicopter that could behind, and continue its own mission: to search for signs of past life in Jezero crater, and to store rocks for a future mission to return to Earth." (NASA’s Ingenuity Helicopter Made History by Flying on Mars)

 


2. Heat Treating "Wow" Factors

Quick social media posts that make you go "wow."

"We Work Well Together" -Robot 1

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Enjoying the North American Market?

When Steel Loses Its Magnetism

 


3. Deep Dive Learning 

Have a little extra time? Check out these engaging media about heat treatments below.

Tips to reduce retained austenite in carburizing and carbonitriding by David Pye (www.htcourses.com)

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What To Do In the Event of a Safety Failure

Tensile Properties


4. Social Moments in Our Community

There's almost (almost) always a reason to celebrate. See some favorites from around the industry.

Employee Gets Some Kudos

."CELEBRATING THE KANTHAL STORY"

Children's Day and National Metallurgists Day in India


5. The Reading Corner

Soak in some knowledge on austenite, robotics, and salt quenching in these key podcasts that you can watch, listen to, or read the transcripts of.

Heat Treat Radio: Robotics in Heat Treat, a Conversation With Dennis Beauchesne, ECM-USA: Click to --> Watch | Listen | Learn

Heat Treat Radio: The Greenness and Goodness of Salt Quenching with Bill Disler: Click to --> Watch | Listen | Learn


6. Something To Set You Flying into Friday

Have a great weekend!


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This Week in Heat Treat Social Media Read More »

Flipping Through Heat Treat Today’s Technical Files

OCWe’re flipping through Heat Treat Today’s technical articles today to highlight four processes: annealing, brazing, carburizing, and forging. Read our top picks of technical articles from these categories like a case study on parts failure (annealing solution) and a new competitor to tried-and-true brazing.


ANNEALING: Part Failure Investigation & Resolution — a Case Study

When an automotive manufacturing began loosing time, money, and the steel itself due to frequent cracking, a third party stepped in to solve the part failure.

[blockquote author=”” style=”1″]In this case, the life cycle of these parts began in a steel mill, where coils of AISI 1045 carbon steel were produced. The parts were then annealed in preparation for fine blanking at our customer’s facility. Then, the parts would be through hardened and sent to the automotive manufacturer.[/blockquote]

BRAZING: The “Next Leap”: Diffusion Bonding for Critical Component Manufacturing

Electric vehicle production, semiconductor development, and a whole wealth of novel products are pushing at the fringes. Does this demand change to tried-and-true heat treat applications? You tell us!

[blockquote author=”” style=”1″]The most sophisticated global companies in electronic instrumentation and semiconductors view diffusion bonding as the wave of the future. The functional-value that 21st-century diffusion bonding technology now offers is a unique-and-beneficial solution in a class by itself; designers came to this realization after being confronted with component performance issues that could not be resolved by traditional brazing. Materials currently under consideration include pure aluminum, aluminum alloys, stainless steels, and nickel-based alloys as well as any other material, such as coated substrates for power electronics or glass and special material combinations (dissimilar joints).[/blockquote]

CARBURIZING: Elevate Your Knowledge: 5 Need-to-Know Case Hardening Processes

This technical article can be found under “Carburizing” in the navigation bar, but as the name implies, you’ll be diving into five essential case-hardening processes. BONUS! this one includes an excellent table to break down the differences.

[blockquote author=”” style=”1″]Case hardening processes are some of the most common heat treatments performed, but each process has its own unique needs. The table below [in the article] provides a summary of the considerations that need to be made when selecting the optimum process. This list is by no means exhaustive; it is encouraged to work with a furnace manufacturer familiar with each process to help select the correct process and equipment needed.[/blockquote]

FORGING: Forging, Quenching, and Integrated Heat Treat: DFIQ Final Report

Here’s a brain spinner: Direct from Forge Intensive Quenching. If you just asked “What?” Best read the full report (or at least the abstract) that tests this novel method — a method that could eliminate normalizing, quenching, and tempering.

[blockquote author=”” style=”1″]Data obtained on the mechanical properties of DFIQ forgings were compared to that of forgings after applying a conventional post-forging heat-treating process. Values of heat transfer coefficients in the DFIQ tank were determined experimentally using a special probe. This data was needed for calculating an optimal dwell time when quenching forgings in the DFIQ tank. It was shown that the application of the DFIQ process allows elimination of. . .[/blockquote]

 

 

 


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Heat Treating Furnace Dispatched to Military Contractor

HTD Size-PR LogoA large gas-fired normalizing furnace has been sent to a global manufacturer of pipe, tube, and fittings used for various military contracts. Supply chain issues prevented the manufacturer from receiving the furnace on the original delivery date in Q4 2021.

This L&L Special Furnace Co., Inc. car-bottom-style gas-fired normalizing furnace is rated to operate at temperatures from 1,300°F/704°C to 2,200°F/1204°C and heated with six medium-velocity burners. The furnace will be able to maintain uniformity of ±25°F/12.5°C at temperatures above 1,300°F/704°C.


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On-Site Hydrogen Generation: A Viable Option for Reducing Atmospheres in Heat Treating

OCHydrogen is a reducing gas used in thermal processing atmospheres for brazing, annealing, metal injection molding, metal additive manufacturing, and glass-to-metal and ceramic-to-metal sealing. Recent supply chain issues, safety concerns surrounding storage, and the growing metal additive manufacturing parts market are making on-site generated hydrogen a burgeoning trend among thermal processors.

This article first appeared in Heat Treat Today’s February 2022 Air & Atmosphere Furnace Systems print edition and was written by Lynn Gorman, a freelance writer.


Reliance on Hydrogen Delivery Can Be Risky

We learned in 2020 that when the pandemic hit, hydrogen gas supply declined, and liquid hydrogen production slowed accordingly.

Hydrogen is a byproduct of refineries processing crude oil, and when demand for gasoline and other crude oil-based products slows, so does hydrogen production. Even as the economy fights back post COVID-19 the long-term trends in crude oil processing are negative because of increasing fleet electrification.

Hydrogen scavenges oxygen, counteracting minor furnace leaks.
Photo Credit: Nel Hydrogen

Besides having more control and assurance that hydrogen will be available on demand as needed, there are other benefits to generating hydrogen on site. According to David Wolff, regional manager at Nel Hydrogen, the only raw materials required to produce hydrogen on site are water and electricity, which are among the most reliable of supply chains. “Essentially the hydrogen becomes another utility with little personnel attention required,” he said. “Electricity and water come into a plant in pipes and wires and are highly reliable. Additionally, there are no hydrogen storage tanks taking up a large amount of unusable space.” He added further that electrolyzers produce ultra-pure, extremely dry hydrogen for best processing results; companies can move the electrolyzers if they relocate to another facility; generating hydrogen eliminates the supply interruptions and contract issues; and producing hydrogen reduces costs over time.

Hydrogen cleans part surfaces to enhance processing results.
Photo Credit: Nel Hydrogen

Hydrogen Generation Facilitates Processing Atmospheres

For thermal processors, the ultimate priorities for a thriving business are parts and profits. Satisfying customers with high quality, heat treated components keep them coming back. To that end, generating hydrogen on site can play a significant role . For instance, hydrogen has the highest heat transmission of any gas, resulting in faster heating, faster cooling, and faster cycle times in both continuous and batch furnaces. Hydrogen atmospheres clean parts, and clean part surfaces enhance sintering/fusion. Hydrogen also scavenges oxygen which counteracts potential furnace leaks. Companies that make their own pure hydrogen, already formulated for their thermal process atmospheres and always available, can potentially improve plant productivity and part quality with the desired properties demanded by their customers.

“The many positives of hydrogen generation work for companies experiencing environmental pressures to choose alternatives to delivered and stored gases,” said Wolff. For instance, he cited a case in which a specialty wire producer in an urban area used dissociated ammonia for wire annealing for decades. However, a gradual shift in their neighborhood to less industry and more housing, schools, and places of worship made it risky to continue storing the toxic ammonia gas to make dissociated ammonia. The company chose to invest in hydrogen and nitrogen generation to replace their ammonia storage and dissociator. According to Wolff, the company is now using less electricity, and can use a leaner atmosphere blend because hydrogen is drier than dissociated ammonia. They are getting cleaner wire, saving money using less electrical power, and eliminating ammonia purchases and tank rental.

Dave Wolff
Regional Sales Manager
Nel Hydrogen
Photo Credit: Nel Hydrogen

In another case, a different specialty wire producer suffered a catastrophic fire that involved hundreds of hydrogen cylinders stored at their historic facility. The company had to replace the plant. To meet current safety and fire code standards, the decision to generate hydrogen was a great choice to comply with the demands of the local fire marshal. According to Wolff, “Authorities having jurisdiction are some of the best advocates for hydrogen generation versus storage.”

Certain Growing Applications Prefer Generated Hydrogen for Best Part Quality

The newest powder-based manufacturing technology is metal AM (metal additive manufacturing) which expands on the learnings and foundations of PM (powder metallurgy) and MIM (metal injection molding). Metal AM is growing rapidly in applicability. Several metal AM techniques are commercialized, and even more are in development. There are several ways that metal AM is revolutionizing fabrication by eliminating complex set-ups, molds, and fixtures, and thereby reducing the costs of short runs. The method allows for continuous design improvements, practically in real time. Metal AM enables parts to be very lightweight through internal strengthening, and parts can be directly translated and produced from a CAD file. In other words, metal AM can create parts that are impossible to make by other approaches. While there is a range of techniques that can be applied to the general category of metal AM parts, most of them use powder, as powder provides the best part finish quality. And, like previous powder fabrication technologies such as PM and MIM, metal AM uses sintering to adhere the metal powder particles together with metal-to-metal bonds.

Metal AM powders are miniscule (20 - 100 microns) and are highly susceptible to oxidation if unprotected by an inert or reducing atmosphere.
Photo Credit: Nel Hydrogen

Metal AM powders are miniscule (20–100 microns), uncoated, and handled gently during fabrication. They are highly susceptible to oxidation if unprotected by an appropriate atmosphere. These tiny particles have an enormous surface area (3kg of typical metal AM 316 SS powder has the surface area of a tennis court). Pure hydrogen (or blended with N2 or Ar gas) is the optimal reducing atmosphere for sintering metal AM parts in both atmosphere furnaces and vacuum furnaces. According to  Wolff, a company having the capability to produce its own hydrogen will have the best results with these kinds of parts that will grow in demand in the coming years.

Compliance Considerations in Hydrogen Use

While generating hydrogen for on-site use without storing inventory is far safer than storing hydrogen or ammonia, there are still rules to follow. There are issues surrounding exhaust, pressure balancing, air flow, heating/cooling, and other considerations. Safety, of course, is paramount when using hydrogen. Helpful publications to review include NFPA 2, NFPA 55, ASME Code for Pressure Piping B31.1, and FM Global Property Laws Hydrogen Data Sheet. Additionally, if the building is leased, the landlord should be aware of the use of hydrogen as should the insurance agent.

Water electrolyzers are available in a variety of sizes and configurations to meet the hydrogen requirements of any thermal processing facility.
Photo Credit: Nel Hydrogen

“Thousands of hydrogen users have proven that, given the right set of circumstances, it’s in their interest and their customers’ interest to generate hydrogen on site,” said Wolff. “And that’s because hydrogen generators produce high purity, pressurized, dry hydrogen with zero hydrogen storage. It’s also a compact, portable, and reliable system, that provides a range of flow rates to suit any thermal processing requirement. And, the hydrogen cost is relatively fixed, so as production goes up, the cost per part goes down.”

For more information: Please send your inquiry to info@nelhydrogen.com or visit www.nelhydrogen.com.


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Weight Loss and Shrinkage: Comparing Furnace Insulation Exposed to Hydrogen Gas

OCWhat material is best suited as thermal insulation, fixtures, and setters in furnaces with hydrogen atmospheres? To find out, ZIRCAR Ceramics, Inc. reports on a series of test results that determine the weight loss and shrinkage of six materials you may use in your heat treat furnace.


Multiple types of fibrous alumina insulation materials were tested to determine their stability in hydrogen gas. Silica bonded types have been known to give superior performance in oxidizing and neutral environments. Alumina bonded types have classically been used as thermal insulation, fixtures and setters in applications where reduction by aggressive furnace atmospheres is encountered. One such aggressive reducing atmosphere is hydrogen, a common cover gas in furnaces for sintering powder metal parts. In hydrogen gas atmospheres, silica -- a common binder which imparts high temperature stability and increased mechanical strength -- is attacked, dissociates and volatilizes resulting in premature failure of the refractory.

Test Method

Cubes of insulation, roughly 1 inch per side, were measured and weighed. They were fired at 1450°C in a model 1725 HTF box furnace manufactured by CM Furnaces, Inc. The furnace was purged with 15 scfh hydrogen gas with a dew point of <40°C. It was heated at a rate of 200°C per hour with soak times of 1, 2, 10 and 50 hours. The samples were removed after each soak, measured and weighed. Weight loss and thickness shrinkage were calculated using experimental data. Shrinkage in the length and width directions were averaged to obtain the data displayed. The materials tested are described in the following table.

Results

Weight Loss results for all types tested.

Weight Loss results for alumina bonded types tested. Shrinkage results in length and width directions for all types tested.

Shrinkage results in length and width directions for all types tested.

Shrinkage results in thickness directions for all types tested.

Conclusions

Premium (ZAL-45AA) and special (ZAL-60AA) grade fibrous alumina insulation materials appear best suited for use as thermal insulation, fixtures, and setters in furnaces with hydrogen atmospheres as they exhibited the least weight loss and thermal shrinkage of all specimens tested.

Alumina bonded materials (ZAL-15AA, ECO-20AA, ZAL-45AA and ZAL-60AA) showed significantly less weight loss after exposure to hydrogen gas at 1450°C than did the silica bonded types tested.

Silica bonded materials (SALI and AL 25/1700) exhibited significant weight loss after testing at 1450°C in hydrogen.

Thermal shrinkage is inversely proportional to density, independent of the bond type.

 

Acknowledgements

The data presented in this article was collected by CM Furnaces, Inc. (www.cmfurnaces.com) and provided to ZIRCAR Ceramics, Inc. by Donald T. Whychell Sr., director of Research and Development at CM Furnaces, Inc. (dwhychell@cmfurnaces.com)


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12 Quick Heat Treat News Chatter Items to Keep You Current

Heat Treat Today offers News Chatter, a feature highlighting representative moves, transactions, and kudos from around the industry. Enjoy these 12 news bites that will help you stay up to date on all things heat treat.

 

Equipment Chatter

  1. Plastometrex, a materials science startup, is working with global testing and inspection provider Element Materials Technology.
  2. National Test Pty Ltd. has been contracted by AusGroup Ltd. to provide NDT and heat treatment services on 58 stainless steel and carbon steel tanks for the covalent lithium refinery in in Australia.


Personnel/Company Chatter

  1. Bodycote increases hot isostatic pressing capacity in Greenville, SC.
  2. PEER Energy GmbH and SCHWING Technologies GmbH signed a long-term cooperation agreement to further technical development and marketing of fluidized bed technology for the heat treatment of metal components.
  3. Nitrex, a global provider of fully integrated surface treatment solutions, has announced that G-M Enterprises has made its official market debut under the Nitrex banner as of January 2022.
  4. Nancy Easterbrook has joined HarbisonWalker International (HWI), a refractory products and services supplier in North America, as the director of Recycled Materials.
  5. GHI Smart Furnaces celebrated the 84th anniversary of their founding in December 1937.
  6. HeatTek announced the purchase of an additional facility in Ixonia, WI to serve primarily as a distribution center for the rapidly growing company’s components and spare parts inventory. This expansion follows another plant acquisition in West Allis, WI.
  7. Hubbard-Hall announced that they’ve made the Dow product line available on their e-commerce site.


Kudos Chatter

  1. Bodycote in Syracuse, NY passed certification to AS9100 standard with zero findings.
  2. A group of 70 employees and management of SECO/WARWICK located in Świebodzin, Poland planted 3,000 beech seedlings on Lumberjack and Forester World Day.
  3. Nitrex Metal, Inc., global of fully integrated surface treatment solutions and technologies, was selected to be part of a “Global Thought Leaders” series broadcast on CBS News.

 

 

 


Heat Treat Today is pleased to join in the announcements of growth and achievement throughout the industry by highlighting them here on our News Chatter page. Please send any information you feel may be of interest to manufacturers with in-house heat treat departments especially in the aerospace, automotive, medical, and energy sectors to bethany@heattreattoday.com.


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