The Mint of Egypt which manufactures both circulation and numismatic coin will receive a vacuum heat treat furnace. The furnace will be used to heat treat circulation and numismatic coin, embossing dies, medals, and special orders. This furnace to the Mint of Egypt is the first furnace provided by the furnace manufacturer to the country of Egypt.
The Mint of Egypt was established in 1950. After 70 years of operation, the first Egyptian Museum of Circulating Coins was created at the mint. It displays a rare collection of special coins representing important historic figures and events, such as the construction of the Suez Canal and the Aswan High Dam. The Vector furnace will be used by the Mint of Egypt mostly for producing collection seals.
"We needed equipment that would significantly increase our production capacity," commented General / HossamKhedr, head of Egyptian Mint Authority, "With heat treatment in the vacuum furnace, our embossing dies will provide the highest possible quality and the durability that is important for the customers. Mints are very special companies. The ban on carrying embossing dies outside the mint prevents us from using commercial hardening plants. That is why it was extremely important to us that the equipment for upgrading our mint represented the highest quality."
Vector Vacuum Furnace by SECO/WARWICK
The Vector® vacuum furnace with 15 bar high-pressure gas quenching -- a product sold by North American SECO/VACUUM Technologies, which is the sister company to vacuum furnace supplier SECO/WARWICK -- is equipment that fits the operating performance requirements of mints. Furnaces with a graphite round heating chamber can be used for a majority of standard hardening, tempering, annealing, solution heat treating and brazing processes.
In the mint industry, these vacuum furnaces are popular as they ensure powerful, uniform gas cooling, which guarantees the high hardness and durability of mint tools. The perfect quality of mint punches and other products is ensured by the very high purity vacuum atmosphere. The parameters of the equipment purchased by the Egyptian Mint are very similar to the solutions delivered by SECO/WARWICK last year to the Mint of Poland — one of the most technologically advanced mints in the world. Some of the equipment installed by the Polish supplier has been operated by this customer for over 9 years.
Maciej Korecki Vice President of the Vacuum Furnace Segment SECO/WARWICK (source: SECO/WARWICK)
"Mints are very demanding customers. They manufacture high quality products that requires perfect details and production repeatability. Collectors, who are the customers of mints, expect the highest care, durability and quality of the finished products," said Maciej Korecki, Vice-President, Vacuum Furnace Segment, SECO/WARWICK Group. "This makes us even more happy that our flagship product — the Vector vacuum furnace — will be installed in another national mint."
Worldwide, there are 70 national mints and several dozen privately-owned mints, manufacturing almost 800 various coin denominations. The oldest mint in the world that has been continuously operated since 864 and the eighth oldest company in the world is Monnaie de Paris in France. The British Royal Mint is the tenth oldest company in the world, established in 886. National Mints provide the official currency for their home countries. They need to comply with rigorous standards that guarantees the weight, purity, and face value of the bullion they produce. This guarantee enables the bullion products manufactured by the state to enjoy a global reputation as the ideal source for investment in high-quality noble metals.
One of the world’s largest producers of high volume, specialty automotive fasteners based in Italy has awarded two contracts to Canadian heat treat supplier in order to expand their manufacturing capabilities with a mesh belt fastener heat treatment system.
The two systems being supplied represent CAN-ENG Furnaces International Ltd. (CAN-ENG) high-capacity line of mesh belt fastener heat treatment systems.
The client returned to the furnace manufacturer in order to receive a furnace with proven low energy consumption, reduced part mixing, reduced part damage potential, and high uptime productivity when compared to conventional cast link furnace designs.
The system will include: computerized vibratory loading system, rotary phosphate removal washer, mesh belt hardening furnace, oil quench system, post quench wash system, mesh belt temper furnace, soluble oil, and part containerization system.
CAN-ENG Furnaces International Ltd. (CAN-ENG) high-capacity mesh belt fastener heat treatment system
These fully integrated systems will feature CAN-ENG’s Process Enhancement Technology – PET™ System (Supervisory Control and Data Acquisition System) which provides the client with complete product traceability through the critical thermal process, process data collection, historical event archiving, process variable trend monitoring, scheduling optimization, and energy consumption features which are unique to CAN-ENG systems.
These new systems will be commissioned to the EU in early 2022.
Heat TreatToday publisher Doug Glenn discusses hot isostatic pressing with Cliff Orcutt of American Isostatic Presses, Inc. Learn about the revolution that is occurring in the heat treat industry and how it is being used across various manufacturing industries
Below, you can either listen to the podcast by clicking on the audio play button, or you can read an edited transcript.
The following transcript has been edited for your reading enjoyment.
Doug Glenn (DG): First off, Cliff, I want to just welcome you to Heat Treat Radio. Welcome!
Cliff Orcutt (CO): Thank you.
DG: If you don't mind, let's give our listeners just a brief background about you.
CO: It's been 43 quick years in the industry. I, actually, did start as a child. My father was one of the original people at Battelle where it was patented in the '50s, so, I grew up under that. Right out of school, I went to work for his company, after he and another gentleman left Battelle, Mike Conaway, and they formed Conaway Pressure Systems. By the time I was 20, I had already installed 10 HIP units around the world and helped design and build the Mini Hipper.
I was involved in 1978 in moving the world's largest HIP unit from Battelle to Crucible Steel in Pittsburgh, which is now ATI. Also, in 1979/80, we installed the very large system for Babcock and Wilcox at the Naval Nuclear Fuel Division in Lynchburg, VA. Both of those units, 40 years later, are still running.
I'm also past president of the Advanced Materials Powder Association, part of MPIF, and I was also a director of their Isostatic Pressing Association. I am currently the chairman of the International HIP Committee. We put on the triennial HIP conference every 3 years.
DG: Is that part of APMI?
CO: It's actually its own group. It was formed by all of the people in HIP around the world, in Europe and Japan and the United States back in, maybe, 1983 or so.
DG: What's the name of the organization?
CO: It's called the International HIP Committee. It's kind of a loose organization which the only thing that we do is put on this conference and we bring in speakers from around the world and promote HIP technology, basically. Our last one was in Sydney, Australia in 2017. We were supposed to have one in October 2020 and now it's pushed until September of 2021.
DG: Where will that be?
CO: It's going to be in Columbus, Ohio because that was the original founding city. Every other conference, we move to the United States, Europe or Japan. So, it's coming back to the US. I'm in charge of it. We have some other good people on the board, including Mike Conaway, who was one of the original Battelle people. Victor Samarov is on the board helping us with the meeting, programming and so forth. People can visit www.hip2020.org to see information on that.
DG: I got you a little distracted on that. Keep going with your background.
CO: Personally, in these 43 years, I've installed over 200 units, hands on. I've flown about 5 million miles, I've been to 38 countries; you name it, I've been there, good ones and bad ones. In my early years, when my father started this company, they pulled about 6 people out of Battelle and they were, basically, my teachers. So, instead of going to educational school, I went to HIP school. We had some of the top people: Roger Pinney, Hugh Hanes, Don Woesner, Gary Felton and another gentleman, Bob Tavnner, all came out of there.
In 1979, my father passed away, and his company then sold to ASEA who then became ABB who then became ABB Flow and then they became Quintus now. That's how they have a location in Columbus, as well.
A couple of people, including Bob Tavnner, left and formed International Pressure Service. That was in 1983. They hired me as operations manager, and we grew to be a force to be reckoned with and the Japanese then bought us. At that time, Rajendra Persaud, or Reggie we call him, left and formed AIP (American Isostatic Presses) and I said, “Hey, Reggie, let's have a two person company again rather than two one-person companies.” That was 1992 and so, 28 years later, now we're a force to be reckoned with again.
DG: Tell us a little about AIP.
CO: American Isostatic Presses, when the Japanese bought us, we had a lot of technology and a lot of good people. Then they hired a new CEO and he decided he didn't want to continue building HIP units, he wanted to do something else. So, Reggie formed AIP and I joined him and we pulled 5 other people back from ITS. We sold our first big job in 1994 to Horus in Singapore, a multimillion dollar job, and took off from there and haven't looked back. We started on a shoestring, no venture capitalists, no dollars, and now we have 4 buildings and locations around the globe.
"We're just a high tech blacksmith, that's all it is. Instead of hitting something with a hammer, we're using gas pressure to squeeze on it."
DG: How many units do you think you guys have installed since 1994?
CO: As AIP, around 150. It's snowballing. In the last 5 years, we've sold 5 big units. Up until that time we were mainly mid and small. We had orders for some big ones but, unfortunately, we couldn't get export licenses for them. The technology that grew out of Battelle was based on nuclear fuel rods for the submarines. Admiral Rickover wanted to extend the life of the sub, so it was protected for quite some time. And then they also had missile nose cone technologies it was used for and that's still what they're protecting it for is missile nose cones.
We had some orders in the late '90s early 2000 through China for large equipment and we were denied. Then we were denied in India, so we kind of just got stuck with the smaller to mid-size units. Here recently, it's starting to expand. Things are loosening up a little bit.
DG: AIP today is selling not only in North America, obviously, but you're pretty much selling around the world, anywhere where it is legal to sell, you'll do it.
CO: Yes, if we can get an export license, we will put it in. Some of the rules have relaxed a little bit, and, with some countries, we're more friendly with them now.
DG: I think a lot of our listeners are probably not going to be as familiar with HIPing, hot isostatic pressing, as other more common “heat treat operations” like carburizing, hardening, annealing and that type of thing. Take us back, class 101: What is HIPing?
CO: We're just a high tech blacksmith, that's all it is. Instead of hitting something with a hammer, we're using gas pressure to squeeze on it. We heat it up hot, we put pressure on it, and we're basically densifying it, making it more dense, and getting rid of imperfections in the metal.
A lot of what's done is castings. When you have a casting, the metal is hot, so it's expanded. When it cools, it cools from the outside in, so it freezes on the outside first and then the center starts to shrink. It creates internal porosity. Most of that porosity is thermal shrinking which is a void. So, you put it back in our heat treatment, apply pressure to it and you get rid of the voids that are left. You make the casting dense and better grain structure and more homogenous. It increases fatigue in property strength. That's the number one use of it right now.
Second is probably powder metallurgy where you take powder metals and you can blend powders and you can start with different grain sizes and different materials. You put them in a container because the gas would go through the container if you didn't have something around it. So, you squeeze on the container and it densifies whatever is inside of it and you make a solid part. For example, a lot of powder metallurgy billets which are then used for extruding into other products or rolls and different things. We do a lot of pump bodies and valves for deep sea work, extruder barrels, you can bond things; there are a whole lot of applications.
DG: The two things I understand with HIPing are high temperature and high pressure. Give us a sense of high temperature. What does that mean? Is it hotter than a typical heat treat operation? And how about the pressures? Give us a sense of what the pressures are looking like.
CO: A lot of people are familiar with sintering. That's where you just take the metal up, you sinter it and the grains merge together by melding and attractive forces. What we're doing is: we're not taking it up to those high temperatures to where the part actually is molten or melting, we're taking them up below that and applying pressure. Because of the pressure, we're basically pressurize sintering; we're adding force to make it sinter faster or better or at lower temperatures.
Usually, it's about 150 C degree less than sintering temperature. Again, it depends on the process of what we're trying to do with it. Typically, most parts are done around 15,000, some parts 30,000. Here, at AIP, we actually have test units up to 60,000 PSI and we've actually built 100,000 PSI HIP units. You're above the yield strength of some of the metals you're using. Most of the majority, again, in like castings, titaniums around 970, steels around 1225, but we go up to 2200 C for some things, even higher for like half-in carbide with people pushing it to 2300. It's pretty hot, a lot of pressure. Unfortunately, high temperature and high pressure costs money. You want to use the lowest pressure and the lowest temperature you can get by with, but sometimes you can't.
DG: It's harder, I would imagine. The way I've always heard it said is that the hotter it is, the more difficult it is to keep, let's say, that cylinder container that you're talking about. If it becomes hotter, it's harder to keep it together. I would guess you're right, when you've got higher temperatures, things tend to blow apart easier?
CO: Not so much. The temperature is contained in the middle of the pressure vessel, so you've got plenty of insulation around it and you keep your container cool. The goal there, in a HIP unit, because it's the expensive piece of item, you want maximize your work zone, that's where you have to have good engineering to make sure you do keep the container cool.
DG: Are most of those units water cooled jackets, or are they cold wall?
CO: They're almost all hot wall, but some of them are cooled internally and some of them are cooled externally. You still have loss to the metal, whether it's internal or external cooled, but internal gives you faster cooling than the external.
The big advantage of HIPing is, like with some materials like titanium, you can eliminate a lot of machining. Making chip that you can't really reuse real easy makes a lot of economic sense. Titanium is a very high melting temperature, so you can't take those chips and melt them cheaply. Aluminum, you can. A lot of aluminum, people can't afford to HIP it because you can just recast it.
HIP is an expense process. The equipment is expense. It uses argon gas. Swinging a hammer is cheap, but using gas pressure, it's so compressible, that you have to put a lot in. You can reclaim some, but the cost is still high. You're talking medical, aerospace and military, basically. Forty years ago, I thought every car would have HIP pistons. It's just not going to happen. They can't afford it. I do see Edelbrock and Trickflow both have HIPed aluminum race heads, though. If you get into where you have the economy of doing something like that, you can apply it. You're definitely going to get a better product, it's just price versus performance.
Watch an "oldie but goodie" on what HIP is.
DG: As far as why people want to do the HIPing, I guess, primarily, it's an elimination of, let's say, defects or inclusions or whatever, either cast parts or powder metal parts, you're increasing fatigue strength, and things of that sort.
Are there any other major reasons why people want to HIP?
CO: Well, there are some things you can't make other ways. In other words, it's like water and oil, you can't mix them very well and some metals you can't melt them and just make a molten bucket and pour it. In HIP, since you're starting with powders that are solid, you can blend things like graphite powder and steel. You couldn't blend them very well in a molten state, but in here, you can. And, you can squeeze it to solid, you can get interlocking and bonding and diffusion bonding materials that you couldn't otherwise. So, you can make things you couldn't make any other way.
Also, you can eliminate machining. For instance, you're making a titanium fitting that has a lot of holes on the inside, it might even be curved and really hard to drill, but you can lay it up and do powder metallurgy around it and make shapes that you couldn't make otherwise. A lot of parts are pressed and sintered for years, for instance, for transmissions. Something like that is real easy because it's a small disc and it's not very long. But, if you're trying to make a real long part that is a strange shape, you can't just press and sinter it. You can do it from HIPing. You can do big shapes that you couldn't get enough force on or you can't fit into a press dye. You can do big shapes that you couldn't get enough force on or you can't fit into a press dye. It opens up a lot of options. A missile nose cone, for instance. There is just almost no way to press and sinter a cone, but with HIPing you can make that shape and you can make it very uniform. There's really no other way to do it.
DG: I think that is one of the benefits of HIPing, from what I understand, it is absolutely equal pressure on all parts when you increase the pressure. It's not like you're only pushing on one part, like with a forge press, or something like that – equal pressure all round.
CO: Yes. And it gives you uniform density throughout the part, which is very difficult.
DG: HIPing is primarily used on castings, powder metal and things of that sort, helps us get a very clean part, if you will, to eliminate inclusions, and minimize the porosity.
You may have mentioned this before, but the actual history of HIPing. It started at Battelle?
CO: It started at Battelle [Memorial Institute], I think in '55 or '56. Again, for the nuclear fuel rods for cladding of the fuel rod. Four people were involved in the patent, two of them, Ed Hodge and Stan Paprocki, "the two others on the patent were Henry Saller and Russell Dayton" I worked for both of them over my years. It grew out of Battelle and then in 1975 is when my father and Mike Conaway left and formed Conaway Pressure Systems. That was kind of like the beginning of the commercialization of it. There were some other companies, like Autoclave Engineers, that were building high pressure equipment, but they weren't really offering packaged HIP units. Conaway Pressure, CPSI we called it, was really the origination of commercial HIPs as we know it.
DG: You hit on this a little bit, but I want to make sure that we're clear on it. You mentioned the industries that are using it, but let's just review that real quickly, and maybe if you can give any example of parts. You said, they've got to be higher value parts because the process is expensive, so we're looking at aerospace, medical and that type of thing. What primarily, at least in those two industries, and other industries if you want to list, are the parts being run?
We’re seeing a lot of application now in ceramics. We see pump plungers and ceramic bearings. Here, at AIP, we do a lot of military work for armor, boron carbides, spinell (21:03), things that are really hard, ceramics. . . You want them perfect because if they have a defect in it, that’s a starting point for a crack. A lot of brakes for jets and fighter jets.
CO: A lot of extruder barrels. What happens is you can use a solid steel chunk of metal for the barrel portion but then you can HIP or diffusion-bond powders on the inside of that barrel that might be very expensive. If you're doing something like a crane or something where the teeth are outside, you can weld on. A lot of times they'll weld on hard brittle materials that help you dig things with a digger. But on an extruder barrel, it's on the inside, it's internal; it's very hard to coat down on the inside. So, we can actually bond those powders to the inside of extruder barrels.
Another big application is sputtering targets. I don't know if you're familiar with sputtering targets, but they're basically sacrificial material that you plate onto other materials. The target is just something that is being hit with an electron beam inside a vacuum furnace. It creates a vapor and by charging the different particles you can attract them and plate things out. All of your mirrored windows, all of your hard drives, all of your CDs and DVDs, when you see that mirrored finish on there, that is a sputtered coating and those coatings come from these things we call targets. What happens is, if say, you're doing a chromium target, at the end, if you try to molten cast it, if you had a bath or a melt of chromium, it would get oxides in it and be terrible. But, you can make very pure powders. That's one of the good things about HIPing is they can make very pure powders by blowing argon through a stream and it makes nice pure powder. Then, we can put it in and squeeze it into a solid billet and make a target which then can be evaporated in the vacuum chamber for coating.
We're seeing a lot of application now in ceramics. We see pump plungers and ceramic bearings. Here, at AIP, we do a lot of military work for armor, boron carbides, spinell (21:03), things that are really hard, ceramics. . . You want them perfect because if they have a defect in it, that's a starting point for a crack. A lot of brakes for jets and fighter jets.
We have a process inside the HIP that we call carbon-carbon impregnation. We take pressure and we push the carbon into the 3D woven graphite fibers and make brakes and nose cones. Other materials like beryllium, it's very hard to make beryllium and machine it because it's kind of dangerous, and so forth. Again, they take powders and the HIP the beryllium to make things like space mirrors and other jet parts.
Now, we've got into more things like teeth and braces are being done with ceramics- new transparent braces made out of aluminum and different materials, zirconia caps for your teeth. Again, if you don't HIP them and they've got a defect in it, it will be like a plate when you drop it. But, if you get rid of that defect, now you've got something harder than steel. On the other end we're doing jewelry such as gold and platinum rings. The benefit there is you don't have porosity. If you have porosity, it's like trying to sand a sponge and you can never find a nice perfect surface. But if you've got rid of that and the sponge is now hard, then you can polish it and you're not taking off any material.
It hasn't really happened too much, but we're seeing rumblings on phone cases. A lot of those have been metal in the past, but now they want to do the magnetic charging and it doesn't work real well.
DG: It's got to be glass of some sort, right?
CO: Yes. We're competing with Gorilla Glass. Some companies are looking at transferring that to zirconia. The iPhone watch, or iWatch, they were making it in zirconia, and that's one of the applications and things like that. Ceramic rings, ceramic knives, ceramic scissors – they're all being HIPed.
On the diffusion front, like the vacuum plates for the fusion reactor, like ITER, they can bond copper to tungsten and different things. You couldn't really weld them, because if you try to weld tungsten, it gets real brittle and cracks, but you can diffusion bond materials and you can do things you couldn't do otherwise.
DG: Those are great examples, and I think that gives folks enough. Are there any other examples that jump to your mind that you think people ought to know about, or is that it?
CO: The big one right now is 3-D printing. There is a lot of interest in 3-D body parts, titanium, stents, spines, implants for teeth and screws. Just about anything you can put in 3-D, they're trying to print. The problem with 3-D is, it's not perfect yet. Maybe in 10 years it will be perfect, but they're making imperfect parts when they print them. If you put them in the HIP and squeeze on it, not you've got a pretty much perfect dense part that's bonded better, stronger, improved properties.
It also allows you to print faster, so maybe you'll want to print an imperfect part, but you can just print twice as fast, so you increase the range between the particle and speed up your process. Again, price versus performance. You look at what the benefits of the two ways are.
DG: I've got a question. In heat treating, a lot of times after heating, you have to worry about dimensional change of the part, right? So, I'm thinking to myself, you've got a cast part with some innate porosity and you put it in a HIPing unit. Do you have to compensate, or do you have to be careful about dimensional change, most notably, I would think, with pressure shrinkage of the part?
CO: Very little because it's isostatic and we're talking about micro macro small porosity. If you had a 1 inch hole in the center and you were squeezing that out, you might give it up, but microscopic particle size is really not that much. Now, in the powder metallurgy, we say it's isostatic but then you do have some of the stresses in the container that you put around it. You might see some distortion at the corners where you welded a container, and so forth. But, there's good software out there, there's good programming and things and a lot of empirical data. People can pretty much design to shape within a couple millimeters.
DG: You mentioned this earlier, but the gas that's used is predominantly argon, because it's a heavy gas?
CO: The reason we use argon is the furnaces we use can't run in air or oxygen. We have a choice of nitrogen or argon, the two commercial grade gases. Nitrogen also embrittles materials like molybdenum. It tears up our furnaces, so argon is the preferred choice. Also, it has poor thermal conductivity which is good for the insulating portion of the HIP unit and when you get it dense enough then it does conduct good enough that it works for the part. It's the all around cleanest, best gas but it's an inexpensive gas. We do use nitrogen on some things. A lot of ceramics like silicon nitride we'll use nitrogen, for different reasons.
One of the biggest issues right now is we see a lot of interest in oxide ceramics. I've got many customers that want us to build a real high temperature oxygen furnace and we're real close to issuing that. What it will allow is to actually sinter in the HIP unit at high temperatures under partial oxygen which hasn't been done yet.
DG: Let's change gears just a little bit. You actually have two sister companies. I want to ask you two questions and you can incorporate information about those sister companies with this: One, why would a company want to outsource a HIPing process? And, two, on the flip side of that, why would a company want to purchase their own HIPing equipment and do it in-house? Maybe you can address both of those, because you've got experience on both sides, based on your sister companies.
CO: The outsourcing is really easy. If you've only got one part to HIP, you're not going to buy a HIPing unit. It's quantity versus can you support the operation of the HIP unit. And, you've got to do it profitably. You've got to do everything profitably or you're not going to do anything. You've got to look at the capital equipment cost and the space. Maybe you don't have space in your building or you don't want to build a new building, or, maybe you just don't have the people that have the knowledge in HIPing and you don't want to hire and train a maintenance crew, and so forth. Even some big companies like Pratt &Whitney and Wyam-Gordon both owned massive HIP units at one time and they decided it was cheaper to sell the HIP unit to Bodycote and then outsource it.
Sometimes economics may play in there, but sometimes maybe you want to have in-house sourcing. Maybe your part is so heavy, you can't afford to ship it. Then, you look at that and say you might want to have your own HIP for that reason, or you've got so many parts, you just can't afford to box them all, ship them out and bring them back. So, there are reasons why you'd want to own your own HIP unit.
DG: You've got sister companies that do the service, right? AIP, American Isostatic Presses, the company that you're with specifically, they build the units. But you've got sister company that actually does the service. Tell us about them a little bit.
CO: When we started out, we were just going to build HIP units and we were selling to a lot of the toll companies and we still do. But, around 2004, after the economic downturn of 2001, we decided we would get into building our own pressure vessels. We hired an engineer, Dan Taylor from Hydropack, and started building pressure vessels because we thought we could do it better. Then we were looking at toll. A lot of people would come to use and say they were not happy with turnaround or other things and they asked if we could help them toll HIP? We kind of got drug into it. We didn't, again, want to step on our customer's toes, so we came out with a different name and sort of hid behind that a little bit and didn't really even market it for a long time. But then again we kept getting dragged in, so we opened another plant and now, this last year, we opened another one. I've never seen a toll HIP company go out of business yet or lose money. Equipment building is up and down, you're riding the waves. It helped us flatten the curve a little bit. It flattened out the cash flow curve and it helped us a lot. Our competitors weren't doing it. They still aren't really doing it like we're doing it. The original name was Isostatic Pressing Services (IPS), then when we did our plant in Oregon, we called it ITS, Isostatic Toll Services. The family wanted to have different names and different people involved and there are different investors. It's AIP, basically, but there are other family members in the Persaud family. In Spain, the big one we opened last year, it kept the ITS name, but there are five players in that one, so we're one of the players.
DG: So, the sister companies have Toll Services, I know one in Oregon. And one in Ohio?
CO: The other is in Mississippi and then one in Spain. The Ohio one is under the AIP name. Basically, what we do in Ohio is we do more research. We, again, are expanding here in Columbus. We are getting ready to build again and we'll start heading a little more into the production toll. We've got a couple customers that are, again, pulling us that way. But, right now, Columbus has 5 HIP units, up to abut 500 mm in diameter. Most of it is high temperature. In Columbus, we concentrate on 2000 C. All of our other plants are doing production work which is medical implants and turbine type parts and those are all 1225 C roughly.
DG: Let's talk about some of the more latest advances, some of the newer things that are coming onto the scene. You mentioned one, I know, and that was the ceramic oxides. Let's talk about that a little bit more, and also, are there any other advances in the HIPing world that we should know about.
CO: I've been in it from almost day one, and it hasn't changed much. If you look at HIP from 40 years ago and today, they'd look the same. We still use the same valves and fittings. The big thing that has changed is computer control. AIP was one of the very first, I won't say the first because, again, back at Battelle in 1973, they had a Foxboro PDP that was in the whole room and had tape reels in it. I remember seeing it run a HIP unit, you'd type in STOP and START. It was like a movie.
Around '93 or '94, AIP branched into computer control pretty hard and we've kind of led since then. It allows us to do a lot of things, number one is that we can run it remotely. So, in Mississippi, we actually run our plant from Columbus. They load it and we take it over here. Our guys here in Columbus, they run our units all night by staying at home and watching them. Computers really help us there. As for service, we were able to get on the computer and look at a piece of gear in Singapore and fix it. That's the thing that really helped us.
"Where we're advancing things is in furnace technology for high temperatures, getting these furnaces to last longer, making them more reliable. . . We're trying to hit the everyday guy and make him profitable, get parts in and parts out."
Where we're advancing things is in furnace technology for high temperatures, getting these furnaces to last longer, making them more reliable. That's kind of one of the keys because, again, with costs and the economics of HIP is you want not to have to be repairing it and replacing things all the time. That's what we concentrate on. We don't try to push the edge. I think some of our competitors really try to push the edge and do things that may or may not be beneficial or even needed, but they're just trying to push the edge of things. We're not. We're trying to hit the everyday guy and make him profitable, get parts in and parts out.
As far as the oxygen, that's because ceramics has been coming for a long time and it's still coming. It's just never really taken off yet, but sooner or later it has to because they're higher temperature, stronger materials in steels, it's just we are competing against forgings and we re competing against casting companies. That's kind of the whole thing with all the HIP companies. There are basically only four main players in the world. We are all kind of small. We all kind of try to work together as much as we can and we all make good equipment to try to advance HIPing technology. More than beating up on each other, we try to beat up on the forging companies and the casting companies. We want to take their business.
In the research here, a lot of what we're doing is trying to work on the higher temperatures and higher pressures. If you can go to higher pressure, you can drop the temperature which then minimizes grain growth. In many materials, that improves either clarity of the material, if it's a transparent ceramic, or it can improve the strength of a steel because you have better interlocking between small particles. We're trying to do a lot more in high pressure, high temperature than some of the other companies. A lot of the companies are just in the metals only; they really focus on that. We're doing some really odd things here. We do stuff that nobody else wants to fool with.
DG: And you have fun while you do it! I'm curious, just from my own purposes. I envision these things as kind of like bell furnaces, a cylinder. Is that true? And, how big, on average, is a HIP unit? What's the work zone dimensions, let's say?
CO: They start with our smallest one which is about the size of a desk and it has a work zone of about 3 inches x 4 inches. We can build a little bit smaller, but economy-wise, we just built that one small model and that is the smallest that anyone uses. It's the size you need for a tensile bar. Just about every university and lab has an AIP small unit. Then, they can go up to massive units. The large one in Japan that Quintus built is 82 inch hot zone. That's a big diameter. They're talking about a 100 inch or 110 inch hot zone.
DG: That's diameter. How tall was it?
CO: 3 meters. Some people are looking at 4 meters or even longer. I've been told that the Army said if you can put a whole tank in one, they'd do it. One of the drivers there is turbine blades. As the blades get bigger, like on jet engines, your turbo fan is the outer blades and so forth, those big shrouds as they get bigger, the gas economy gets better, so they would like to build massive engines and they would like some of those parts HIPed. They want really big HIP units. Another one is in nuclear reactors for small modular nuclear power. They'd like to replace some forgings and if they could do it with powder metallurgy lids, and so forth, and those need a 3mm diameter HIP unit. The majority of the work is in the 1 meter range.
Fives, an international industrial engineering group for silicon steel processing lines, will receive high efficiency burners with low emissions. This will help the company as they fulfill recent orders involving the supply of annealing and pickling lines as well as annealing and coating lines to Chinese steelmakers.
The burners were designed and supplied by WS Wärmeprozesstechnik, and with their FLOX® process, Fives will be able to manufacture using the strictest emission values without SCR (selective catalytic reduction) treatment for their furnaces for silicon steel. This was necessary as China’s steelmakers have been demanding combustion technology with lowest NOx emissions in order to meet climate-related goals.
Dr.-Ing. Joachim G. Wünning President WS Wärmeprozesstechnik GmbH
The silicon strip line with FLOX® burners from WS (pictured above) will assist Fives in their current orders as well as their continued design and supply of machines, process equipment, and production lines in various sectors. These sectors include steel, aerospace and special machining, aluminum, automotive and manufacturing industries, cement, energy, logistics and glass.
"It is our ambition at WS," states Dr.-Ing Joaching G. Wünning, president of WS Wärmeprozesstechnik GmbH, "to provide solutions for all continuously operated strip lines which can reliably attain NOx emissions well below 100 mg/Nm³, with simultaneously high combustion efficiency over 80% and which are, already today, suited for a future with green combustion gases."
Heat TreatRadio is a podcast where Doug Glenn, publisher of Heat TreatToday discusses cutting-edge topics with industry-leading personalities. Among many cutting-edge interviews and conversations on the latest technologies and commercial happenings in the industry are topics like AMS2750F, ferritic nitrocarburizing, and supply chain options.
You can subscribe to Heat TreatRadioon iTunes or SoundCloud, and even listen to these episodes on PodBean, iHeart Radio, and ListenNotes. Check out some of the top heat treat topics from the list of episodes below.
1 - The World of Ferritic Nitrocarburizing with Thomas Wingens
"A big part of the success of FNC is the combination with post oxidation. That is a big part because the combination of ferritic nitrocarburizing with post oxidation leads not only to a mechanical strong surface with compressive stresses, it also has a very high corrosion resistance."
"One of the things I always had in my mind when I first got involved with the specification was that the specifications were written by the aerospace 'primes,' but that’s not the case; it involves people, such as myself, who are end-users of this specification. I’m an end-user, so I’m able give my input and say, 'Hey, this doesn’t make sense. What you want to add into the spec is not real world.' It’s nice that people such as us get involved with these specifications."
3 - Rethinking Heat Treating for the 21st Century with Joe Powell (Part 1 of 4)
"I am a commercial heat treater who believes that part design should be integrated for heat treating by the part-maker. It’s a nuance, but what it really boils down to is that sometimes commercial heat treaters do it best, but sometimes the part-maker can do it better."
4 - Metal Hardening 101 with Mark Hemsath, Part 3 of 3
"[Nitriding], and really its cousin FNC (ferritic nitrocarburizing), are actually fairly inexpensive treatments and they can be performed on final dimension parts. There is no post machining and there is minimal distortion. That’s kind of my opinion of why it has done well.”
"Who wouldn't want to have a smoother operation? Not have to schedule people, pay overtime, justify it. We're three years into the project and I think we have a very viable tool for heat treaters to see what they currently cannot see."
6 - James Jan & Andrew Martin on Development of Modeling Software
"We model what happens with FIRE CFD code, we model what is happening at the transition of the interface between the metal component and the water. Because when something that hot gets plunged into water, it is quite an interesting thing that happens—it is called the Leidenfrost Effect. Initially, what happens is the component is so hot, it forms a film around the outside of it, a vapor film, and perversely that vapor film then insulates the component from the water. That film slowly breaks down then you get into nucleate boiling and things like that, and that becomes a lot more aggressive and the cooling happens much faster until you eventually get a single phase. But actually modeling the boiling process is what the CFD code does. That is the secret sauce that we’re bringing to the party here."
7 - A Discussion with Carl Nicolia, PSNergy President
"Their recovery cycle was reduced by 25%. Now, a recovery cycle is from the time I close the door to the time I start my controlled cycle. 25% reduction. And in that total cycle, they dropped gas consumption 5% which eventually led to an increase in output of that furnace by 10%. What we love about this, and this is kind of the theme of the article really, is that the total cost to implement this was less than $10,000. This is a perfect example of high value solution. I hate to say ‘low cost’ because cost is relative, but this is high value. If I can deliver 25% improvement with less than $10,000, or if I can deliver 10% double-digit output increases for less than $10,000, that’s a high value solution."
"The other one I think that’s going to emerge is most probably making more and more parts by powder metallurgy from metal powder which are 100% free alloyed. In other words, all the elements are in each metal powdered particle. In other words, you’re starting with a micro ingot as opposed to a big ingot that you normally use to make bars, and then from bars you cut pieces, and then from those pieces you do hard forging or machining."
9 - Justin Rydzewski on CQI-9 Rev.4 (Part 1 of 4) – Pyrometry
"Perhaps the most significant change within the temperature uniformity survey section is to the alternative temperature uniformity survey testing methods. In instances when I can’t perform a survey with sensors being trailed in, or I can’t send a data pack sort of unit or a PhoenixTM unit through that furnace system itself to collect the data, for systems like that, in the third edition, there were three or four paragraphs of information about what you could do."
"The interesting thing is that there is a phenomena precipitation hardening that goes on in aluminum and titanium. But it also goes on in these high alloy steels. It is a secondary hardening mechanism. We’ve been working on that and we feel that once we can handle secondary hardening in steel, then the jump to aluminum and titanium should be pretty straightforward."
The 31st Heat Treating Society Conference and Exposition (Heat Treat 2021) is scheduled for September 14-16 in St. Louis. This bi-annual, can’t-miss event provides an excellent opportunity for the heat treating community to meet, exchange information, and conduct business.
Eric Hutton President, ASM Heat Treating Society Vice President Operations Aerospace, Defense and, Energy Bodycote
In addition to our standing colocation with AGMA’s Motion & Power Technology Expo (MPTE), we are excited to also be co-locating with ASM’s NEW Annual Meeting, “International Materials, Applications, and Technologies (IMAT)” Conference and Expo. Heat Treat conference registration includes full access to IMAT 2021. Co-locating with IMAT 2021 will provide access to additional exhibitors and more than 400 technical presentations on a wide variety of materials-related topics.
This year’s Heat Treat organizing committee did an excellent job of ensuring that the latest research and development is included for a high level of technical content on a wide variety of important topics, including Atmosphere Technology, Additive Manufacturing, Internet of Things, Nitriding, Vacuum Technology, Applied Technology, Quenching and Cooling, etc.
The Heat Treat Expo, co-located with IMAT and MPTE, is the place to be, featuring more than 500 companies. Activities on the show floor include a VIP guided industry tour on Tuesday, Solutions Center presentations, welcome reception with exhibitors, the Fluxtrol Student Research Competition, and the HTS Strong Bar Competition.
We hope attendees will join us during our premiere networking event, “The Heat is On,” at the Anheuser Busch Biergarten, scheduled for Wednesday, September 15. This special evening will feature live music, a tempting array of locally inspired food, craft beer, and a few “hot surprises.” Attendees will have the opportunity to network with Heat Treat, IMAT, and MPTE attendees.
We know that things might look a little different this year, but, rest assured that your health and safety are always our top priorities, and the ASM team continues to closely monitor all federal, state, and local guidelines. We are confident that we can safely come together and are taking all appropriate measures to ensure a healthy and successful in-person conference and expo.
Let’s get back to business! I hope you will join me at Heat Treat 2021, a great location to reconnect, make new contacts, share information, and collaborate with attendees and exhibitors from around the world in the global heat treating industry. We look forward to seeing you in St. Louis in September.
A Canadian leader in the coating industry will expand their heat treat capabilities with a floor-standing box furnace used for ceramic coating applications for parts in the aerospace industry.
The L&L Special Furnace Company Inc. model XLE214 is used for curing and bonding ceramic coatings to various steel bodies. This process provides extra strength to aerospace parts that are subject to various heats and stresses under normal operating conditions.
The furnace has an effective work zone of 22" wide by 16" high by 20" deep. A horizontal door with ceramic hearth and support bricks is included to incorporate the customer’s loading system. Nickle chrome elements are used in the furnace that are resistant to any potential contamination the process may cause. Heat shields provide a safe-to-touch case temperature under operating conditions.
Model XLE MDS from L&L Special Furnace Company, Inc.
The model XLE214 is controlled by a Eurotherm program control with overtemperature protection, chart recorder with jack panel, solid-state relays, and zone controls for balance of temperature gradients. Thermocouples, fusing and electrical interconnections are included. The furnace control circuit is completely tested to ensure proper operation prior to shipping.
The furnace case is sealed for use with inert atmosphere to help reduce oxygen impregnation with the parts. The furnace has a manual inert flow panel to control the inert gas flow into the oven.
The model XLE214 also includes a high-convection fan for uniformity of ±10°F/5.5°C above 500°F/260°C to 1,875°F/1,023°C. There is a 4" diameter venturi with a variable frequency drive to evacuate outgassing that occurs during the curing of the ceramics to the steel part. The system is completely automated through the program control logic.
Global leader in industrial cleaning products based in North America acquires a Canadian chemical division, expanding its offerings to include molten salt for the heat treat market.
Kolene Corporation has acquired the chemical division of Park Thermal International Corporation. The president of Park Thermal, Jay Mistry, will work with Kolene going forward to assure the transition of all Park Thermal standard and proprietary heat treat chemical blends, as well as providing customer support.
Peter Shoemaker Vice President of Purchasing Kolene Source: PRNewsWire
"We are very excited to broaden our molten salt offerings into the heat treat market and utilize Jay’s extensive chemical knowledge and excellent technical customer support to do so," says Peter Shoemaker, VP of purchasing at Kolene. "It’s great to have Jay as a partner with Kolene as we relaunch the industry trusted Iso-Therm product line."
"We were challenged with the Covid downturn in our business," stated Jay Mistry, "and we were looking for a strong partner to continue supporting our established customer base. I am glad to have found the Kolene team, a trusted and competent North American partner who has the technical and commercial bandwidth to carry our heat treat salt business into the next phase."
Kolene Corporation has been a trusted brand for both ferrous and non-ferrous metal cleaning products for 82 years and is also known for their ferritic nitrocarburizing (FNC) salts.
Park Thermal International Corporation of Georgetown, Ontario, Canada, was founded in 1938. Jay Mistry started as chemist at Park Thermal in 1989 and bought out the company from Brian Reid in 2017. Since then, Park Thermal has developed chemical blends for special client demands.
Today's shared content is provided by the global information partnership between leading European heat treat news provider heatprocessing and the team at Heat TreatToday.
What's next in heat treating carbon materials? In this best of the web feature from our European industry partner, heatprocessing, take a moment to see how computer modelling demonstrates the technical feasibility and the efficiency of this dynamic combination of induction heating and radiation heat transfer. Could this method be a practical integration in your heat treating process needs? Would adopting this method save you energy? Take a read and let us know!
An excerpt:
"This dynamic combination of induction heating and radiation during the baking process improves greatly the energy efficiency and permits a very precise control of the temperature profile in the carbon."
While we typically try to send our readers to free content, this article requires a nominal fee to access. We hope that you will find this content beneficial.
Last month we began the discussion about the relationship between combustion safety and uptime, highlighting how combustion safety, reliability, emissions, and efficiency are inseparable. This month, we will explore the subject in greater detail and outline a path that can both reduce the risk of an incident and protect the bottom line.
This article written by John Clarke, technical director at Helios Electric Corporation, appears in the annual Heat TreatToday 2021 Buyer's Guide June print edition. Return to our digital editions archive on Monday June 21, 2021 to access the entire print edition online!
John B. Clarke Technical Director Helios Electrical Corporation Source: Helios Electrical Corporation
How many times have we heard the tale about the man with the leaky roof? He cannot fix his roof when it is raining, and the roof doesn’t need repaired when it is not. This story is also applicable to heating system maintenance, perhaps more so than other plant maintenance activities because it so seldom “rains.” Ovens and boilers tend to be very reliable. (This statement is true for equipment operating at low or moderate temperatures, less so for equipment operating above 1832°F (1000°C).) It is exactly when the machine is properly producing parts that the planning for combustion safety, availability, and performance must occur.
The first critical step we must take is to understand that combustion safety, routine maintenance, tuning, and calibration are parts of a larger work strategy. To focus solely on the annual inspection of safety components while ignoring system tuning will not only compromise tuning and efficiency, but also the safety. We have seen how managerial reactions to high profile incidents have caused some firms to dispatch teams to annually examine valves and pressure switches. This effort is highly compromised if it does not include all aspects of system maintenance as well as capturing what is learned each time to improve future inspections and equipment designs. There is data beyond pass and fail that is valuable if we wish to optimize the performance of our equipment
Let us assume it is a clear sunny day, and we are ready to invest some time in preparing to improve our combustion system starting with a deep dive examination of two pressure switches: the low fuel gas pressure switch (LFGPS) and high fuel gas pressure switch (HFGPS). These ubiquitous components are present on nearly every fuel train and are vital for safe operation. As their names imply, they monitor the fuel pressure and shut the safety valves if the fuel gas pressure is either too high or too low.
These switches must be listed for the service they provide by an agency independent of the manufacturer – UL, TUV, FM, etc. Simply looking for a stamp may not be enough; take the time to read the file or standard being applied by the agency and determine if it describes the application. Next, ask if the pressure switch carries the basic ratings expected, like the enclosure rating (Nema or IP). Is a Nema 1 switch operating in a Nema 12 area? Temperature ratings must be confirmed. All too often a component rated for 32°F (0°C) is applied in an outdoor environment in cold climates, or one with a maximum rating of 120°F (50°C) is applied next to the hot wall of a furnace. The component may operate out of specified environmental ranges for some time, but to apply a component in this manner is betting against the house – sooner are later we are going to lose. Ask the people of Texas if the bet against sustained cold temperatures in early 2021 was worth it.
"John Clarke, Technical Director, Helios Electrical The first critical step we must take is to understand that combustion safety, routine maintenance, tuning, and calibration are parts of a larger work strategy"
Next, let us look at the contact(s) rating of the switch and how it is applied to the burner management circuit. More often than not, these switches are in control circuits fused for more current than the contact rating. If the switch rating is too low, the electrical designer has an option to use an interposing relay to increase the current carrying capacity to this device. This relay is an added component, and as such, adds yet another possible point of failure. If the relay is interposed, is it dedicated to this one switch? Multiple devices being interposed by a single relay is prohibited by NFPA 86, for good reason. Is the relay designed to fail safely? That is, will a relay coil burn out or wiring fault close the critical safety valves? Is the wire gauge suitable for the current carried and protection device used?
Next, is the switch mounted in a safe location free from possible vibration or the foot of an eager furnace operator? If the switch must be changed, are clearances provided to perform this maintenance? What is the mean time to replace (MTTR) the component? Is the way the device is wired providing a path for combustible gas to enter the control enclosure and cause an explosion? Flexible conduit, without a means to seal the connection, is a very common error. Use a properly specified cord and consider using some type of connector to terminate the wiring at the switch. A simple 7/8-16 or DIN connector not only provides additional protection from combustion gas getting into the electrical conduit but is also a great benefit when changing the component in a rush and helps to isolate the component’s control circuit during testing and calibration.
Is the pressure switch suitably protected from bad “actors” in the fuel gas? Perhaps soot is present that could foul narrow passages or H2S that could result in corrosion. These are rare conditions, but coke oven gas may not be as clean as purchased natural gas. Do we need to specify stainless steel components? Would a filter make sense to protect the switch and increase the intervals between maintenance?
Finally, let’s discuss pressure ratings. Unfortunately, nomenclature varies by manufacturer. What is the maximum pressure the device can sustain and not fail, i.e., leak fuel gas into the environment? Many switches can experience a pressure surge without risk of leakage, but the high-pressure event will damage the switch internally. It is important when determining if this rating is adequate to consider possible failure modes that might expose the pressure switch to excessive pressure. As a rule of thumb, a pressure switch must be able to sustain a surge pressure delivered to the inlet of the pressure reducing regulator immediately upstream of the device. Think of it this way, if the upstream regulator experiences a failure, the full pressure delivered to this regulator will pass to the pressure switch in question.
Other obvious pressure ratings are the maximum and minimum set points. The pressure switch should be set to trip as close to the middle of the range as possible and should never be set close to either the minimum or maximum setpoint. Is the pressure switch manually or automatically reset after a trip? In general, it is best practice that the LFGPS resets automatically, and the HFGPS requires a reset by the operator. This recommendation is because LFGPS trips each time pressure is removed from the system, and it is generally understood that the system needs fuel to operate. On the other hand, a high-pressure event is exceedingly rare, and the operator should be made aware of this unusual event.
This article has discussed a lot about the simple pressure switch. It appears to be a heavy lift to perform this analysis on every pressure switch in a facility, but take comfort, once the exercise has been completed on the first system, it is much easier to replicate what has been learned to properly assess other systems. We should most definitely insist that our OEM provides this data, in detail, when new equipment is supplied. Why did we review all these specifications? Because I have been around for a while and have seen nearly every one of these errors in the application of pressure switches on operating combustion equipment.
Next month, we will expand on the pressure switch discussion to describe the tune/calibration and testing processes. I hope this deep and specific dive has been of value. If you have any questions or comments, please let me know.
About the Author:
John Clarke, with over 30 years in the heat processing area, is currently the technical director of Helios Corporation. John’s work includes system efficiency analysis, burner design as well as burner management systems. John was a former president of the Industrial Heating Equipment Association and vice president at Maxon Corporation.