Technical Tuesday

Selecting the Right Vacuum Pump Oil Starts with Knowing Your Pump

 

 

Source: VAC AERO International

 

Vacuum furnace heat treaters know that one of the most critical parts of their system is the pump oil, but it may be a bit overwhelming trying to determine which is the right kind of oil is needed. Selecting the correct vacuum pump oil starts with knowing your pump.

“‘Oil’ is a bit of a misnomer because modern pump oil technology has evolved well beyond the original distilled petroleum products. There are now double- and triple-distilled oils available, as well as hydro-treated oils, low sulfur oils, silicone-based synthetic oils, and flushing oils used to clean the pump. Due to the wide variety of formulations available, these are often now referred to as pump ‘fluids’ rather than pump ‘oils’.” — VAC AERO International

“Different pump oil formulations are specifically designed for different pumps and different vacuum applications,” notes VAC AERO, and a key factor in learning how to select the correct pump oil is the understanding of vapor pressure, viscosity, and distillation methods, as well as solvent refining, hydrotreating, synthetic oil (Perfluoropolyether), flushing oil for vacuum pumps, and diffusion pump oils.

 

 

Figure 1 | Viscosities of various liquids

 

Read more: “Vacuum Pump Oil”

 

 

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Before Normalizing, Pause to Assess Materials

 

Source: BluewaterThermal.com

 

When there is a need to provide a uniform, pearlitic structure at a microscopic level, many heat treaters turn to normalizing to increase or restore metal strength, but experts at Bluewater Thermal Solutions note the need to assess all aspects of the material before choosing this process.

“It is possible with given alloys and metals that the process may also cause a decrease in overall strength.” 

Read more: “The Advantages of Normalizing Heat Treatment of Parts” as well as “Normalizing Services for Metal and Metal Components”

 

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How to Know Which Softening Process to Use in Your Heat Treatment

 

 

Source: Metlab Heat Treat

 

When steel needs to be softened to alter ductility, toughness, or properties, or to produce a specific microstructure, a heat treater can turn to any one or combination of processes to suit the material or the application.

Metlab Heat Treat’s primer series includes a short explanation of the options available, whether it is

  • annealing, which “removes the internal stresses, which build up as a result of cold working and other fabrication processes;”
  • protective atmosphere normalizing, which “refines the grain size and enhances the uniformity of the microstructure;” or
  • spheroidize annealing, which “is generally done on parts which have been work hardened, to allow them to be further worked, either rolled in the case of coils, or drawn for wire.”

 

Read more: “Annealing, Protective Atmosphere Normalizing, Spheroidize Annealing”

 

Photo credit: Metlab Heat Treat

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What’s Going on Inside Your Heat Treated Part?

 

Source: Gear Technology

 

It’s no secret to heat treaters that not all methods work well on all parts and specifications. It’s also a hard fact that false readings can result when applying hardness measuring systems, therefore, says Charles D. Schulz of Gear Technology, “critical service parts often require a few ‘sacrificial lambs’ to be processed along with the production parts.”

“I cannot emphasize enough that if you are not cutting up parts or coupons you do not know what is really happening during your thermal processing.” — Charles D. Schulz

 

Read more: “Gear Materials: More Inside Heat Treating Trivia”

Photo credit: Gear Technology

 

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Tool Steel Potential Dependent Upon Heat Treating

 

Source: L&L Special Furnace

 

With its unique ability to be used in the shaping of other materials, tool steel, which includes a variety of carbon and alloy steels, is a particularly valuable property for tool manufacturers as well as manufacturers of components and parts that require the same degree of distinctive hardness, resistance to abrasion and deformation, and ability to hold a cutting edge at elevated temperatures.

The three-phase process of heat treating tool steel — annealed, austenite, and martensite — ensures the tool retains these qualities, achieves intended functionality, and meets performance specifications. In addition,

 

“The phases that define the process of heat treating tool steel alter the microstructure of the steel itself. Observable under a microscope, heat treatment rearranges the atoms of the iron, carbon, and any other metal components, which serves to give the final material specifically desired properties.” —  L&L Special Furnace

 

Multiple factors can influence the final product, including the appropriate hardening and tempering temperatures depending on the type of steel.

This table provides general recommendations for the appropriate hardening and tempering temperatures based on steel type, as well as the recommended type of quench process. — L&L Special Furnace

 

“Heat treating tool steel does more than adding significant value to the treated material—it makes the use of the tool steel possible. Without properly applied heat treating, tools simply wouldn’t work or couldn’t even be made. Modern metallurgical engineering is essential to the production and manufacturing of tool steel and all of its applications.” —  L&L Special Furnace

 

Read more: “The Critical Aspects of Preparing Tool Steels Through Heat Treatment”

 

Photo credit (main image): Youtube.com  and caption: “Visual indication of tool steel phase change to austenite when heat treating. Small pools of iron are forced from the steel as the volumetric change takes place and small amounts of carbon are burned off.”

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Clarity and Accuracy in Heat Treat Specifications Ensures Quality Processing

 

Source: Paulo Learning Center

 

Heat treaters strive to deliver parts that meet industry and manufacturers’ specifications with precision, but too often the information they get from customers is inadequate, unclear or incorrect. This article from Paulo’s Learning Center provides 7 points of data that will help a metallurgist treat parts to stand up to the manufacturer’s intended application, including:

  • making sure materials are clearly identified
  • specifying the process required
  • noting prescribed hardness tolerance
  • identifying case depth tolerance
  • sharing the right amount of information
  • providing correct hardness scales
  • identifying inspection points

 

Read more: “Understanding Heat Treatment Specifications”

 

Photo credit: Paulo Learning Center

 

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Binder Removal in Vacuum Sintering

 

Source: TAV: The Vacuum Furnaces Blog

 

Andrea Alborghetti, Technical Manager of TAV Vacuum Furnaces

Heat Treat Today previously posted Parts 1 and 2 of this series on vacuum sintering. Part 1 focused on the two processing steps of debinding and sintering. Part 2 addressed primarily the vacuum sintering furnace itself. This installment analyzes the process and variables involved with binder removal.

Andrea Alborghetti, technical manager of TAV Vacuum Furnaces and contributor to the company’s blog, provides an analysis of burning vs capturing binders, addressing advantages as well as problems that may arise and how to execute control in the process, as in this example:

“One thing that is worth clarifying is that the flames usually seen on the outlet of kilns that use combustible gases (hydrogen, for example) as the process gas, were not originally designed to burn the binder disassociation residues to reduce emissions to the legal limits. Rather, it is solely for disposing of the emitted hydrogen safely, thus avoiding hazardous, potentially explosive atmospheric concentrations being created outside of the kiln.”

Read more for further analysis of binder removal, including discerning the type of residue found with your process: “Perfect Vacuum Sintering Step by Step #3”

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Seven Types of Annealing, and Why Bearing Manufacturers Should Turn to Spheroidization

Sources: Machine Manufacturing; Knergize.com

Heat treating more often than not includes the process of annealing in order to induce precise softness; to alter ductility, strength, or properties; or to produce a definite microstructure. Because of the wide variety of steels and metal alloys, it is important for heat treaters to match the correct annealing process with the steel grade and to the application of the parts being treated.

Machine Manufacturing has provided a summary of the annealing process and listed seven types of annealing, describing the process and the objectives for each. Included in the list are:

  1. Complete Annealing
  2. Isothermal Annealing
  3. Incomplete Annealing
  4. Spherification Annealing
  5. Diffusion, or Uniform, Annealing
  6. Stress Relief Annealing
  7. Recrystalization Annealing

Read more: "What Is Annealing and 7 Types of Annealing Process"

 

Dr. S.B. Sarkar

And to take the analysis into more specific types of annealing, over at Knergize.com, Dr. S.B. Sarkar discusses Spheroidized Annealing and its benefit to bearing manufacturers, describing the metallurgical science behind the process, noting the need to adhere to international standards and specifications, and addressing equipment management and quality control of the process.

Read more: "Why Spheroidised Annealing of Bearing Steel Is Important for Manufacturing Good Quality Bearings"

 

Photo credit

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Feasibility Studies for Aerospace Applications Should Review Heat Treatment

 

Source: Precipart

 

When designing for manufacturability (DFM) for aerospace applications, should a design team commission a comprehensive feasibility study? In this article from Precipart, which designs and manufactures high precision custom gears and mechanical components for the medical technology, aerospace and industrial sectors, read about application-specific requirements, concerns with production tooling, and tolerance of materials for post-fabrication processes, including heat treatment:

  • key specifications of a gear or motion control system
  • potential design issues that may occur throughout the life of a device; for example, how heat treatment, among other post-fabrication processes,
  • recommendations to address performance issues in various environments and conditions

Read more: “What Are the Benefits of an Aerospace Gear Feasibility Study?”

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The Pros and Cons of Gas and Ion (Plasma) Nitriding

 

Source: AHTcorp.com

 

The compound zone acts as a ceramic skin protecting the metal underneath from corrosion. (Photo credit: Advanced Heat Treat Corp)

Engineers considering the advantages and disadvantages of surface treatments typically have a usable lifespan, surface hardness, and fatigue strength in mind. As a process, both gas and ion (plasma) nitriding avoid the issues involved with coatings and achieve similar metallurgical properties, and the compound zone increases corrosion resistance. But what are other areas in which the two processes can be compared, and what are their differences? It’s good to know, particularly since the latter could significantly make a direct impact on the end product.

Jacob McCann, a process metallurgist with AHT Corp., provides a specific list of pros and cons of gas nitriding and ion (plasma) nitriding in our Technical Tuesday feature for today.

 

Read more: “Gas and Ion (Plasma) Nitriding: What’s the Difference?”

Photo credit: Advanced Heat Treat Corp

 

 

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