TAV Vacuum Furnaces

Dual Chamber Vacuum Furnaces vs. Single Chamber Vacuum Furnaces — An Energy Perspective

The need to understand how certain furnace designs operate comes at a time when heat treaters are weighing each energy cost and benefit of their systems and processes. Read on for a quick summary on how dual chamber furnaces preserve energy.


On April 17-19, 2024, TAV VACUUM FURNACES provided a speaker at the 4th MCHTSE (Mediterranean Conference on Heat Treatment and Surface Engineering). The speech focused on the energy aspects of vacuum heat treatment, a subject towards which all of us within the industry need to pay attention for reducing the carbon emissions aiming at a zero net emissions future.

We have already analyzed the essential role that vacuum furnaces will play in this transition, with a focus on the optimization of energy consumption in our previous article. With this new presentation, we wanted to emphasize how selecting the right vacuum furnace configuration for specific processes may impact the energy required to perform such process. For doing so, we compared two different furnace designs — single chamber vs. dual chamber vacuum furnaces — detailing all of the components’ energy consumption for a specific process.

TAV DC4, dual chamber vacuum furnace for low pressure carburizing and gas quenching
Source: TAV VACUUM FURNACES

As a sneak peek into our presentation, we will summarize below how the main features of the two vacuum furnaces design are affecting their energy performance.

Let’s start by introducing the protagonist of our comparison: a single chamber, graphite insulated vacuum furnace, model TAV H4, and a dual chamber furnace TAV DC4, both having useful volume 400 x 400 x 600 mm (16” x 16” x 24”) (w x h x d).

In a single chamber vacuum furnace, like the TAV H4, the entire process is carried out with the load inside the furnace hot zone. This represents a highly flexible configuration that can perform complex heat treatment recipes with a multiple sequence of heating and cooling stages and to precisely control the temperature gradients at each stage.

Configuration of the TAV DC4 dual chamber vacuum furnace
Source: TAV VACUUM FURNACES

Alternatively, a dual chamber vacuum furnace, like the TAV DC4, is equipped with a cold chamber, separated from the hot zone, dedicated for quenching. Despite the greater complexity of this type of vacuum furnace, the dual chamber configuration allows for several benefits.

First, in dual chamber furnaces, the graphite insulated hot chamber is never exposed to ambient air during loading and unloading of the furnace; for this reason, the hot chamber may be pre-heated at the treatment temperature (or at a lower temperature, to control the heating gradient). But in single chamber vacuum furnaces, the hot zone must always be loaded and unloaded at room temperature to avoid damages due to heat exposure of graphite to oxygen.

Because dual chamber furnaces have more controlled heating, this will result in both faster heating cycles and lower energy consumption, as a substantial amount of energy is required to heat up the furnace hot zone. This advantage obviously will be more relevant in terms of energy savings the shorter the time is between subsequent heat treatments.

View of the cold chamber of the TAV DC4 dual chamber vacuum furnace
Source: TAV VACUUM FURNACES

Secondly, since the quenching phase is performed in a separated chamber, the hot zone insulation can be improved in dual chamber vacuum furnaces by increasing the thickness of the graphite board without compromising cooling performance. This translates into a significantly lower heat dissipation, to the extent that at 2012°F (1100°C) the power dissipation per surface unit (kW/m2) is reduced by 25% compared to an equivalent single chamber vacuum furnace.

Additionally, quenching in a dedicated cold chamber allows to obtain higher heat transfer coefficients and higher cooling rates compared to a single chamber vacuum furnace. Since the cold chamber is dedicated solely to the quenching phase, it can be designed for optimizing the cooling gas flow only without the need to accommodate all the components required for heating. All things considered, the heat transfer coefficient achievable in the TAV DC4 can be, all other things being equal, even 50% higher compared to a single chamber vacuum furnace. Secondly, since the cold chamber remains at room temperature throughout the whole process, only the load and loading fixtures need to be cooled down; as a result, the amount of heat that needs to be dissipated is significantly less compared to the single chamber counterpart.

CFD simulation showing a study on the cooling gas speed in a section of the cooling chamber for the TAV DC4 dual chamber vacuum furnace
Source: TAV VACUUM FURNACES

For heat treatments requiring high cooling rates, it is possible to process significantly higher loads on the dual chamber furnace compared to the single chamber model; translated into numbers, the dual chamber model can effectively quench as much as double processable in a single chamber furnace, depending on the alloy grade, load configuration and overall process. The savings in terms of energy consumption per unit load (kWh/kg) achievable in the dual chamber furnace for such processes can be as high as 50% compared to the single chamber furnace.

In the end, the aim of the speech was to highlight how the energy efficiency of vacuum furnaces is highly dependent on the machine-process combination. Choosing the right vacuum furnace configuration for a specific application, instead of relying solely on standardised solutions, will improve significantly the energy efficiency of the heat treatment process and drive the return on investment.

About the Author

Giorgio Valseccchi
R&D Manager
TAV VACUUM FURNACES

Giogio Valsecchi has been with the company TAV VACUUM FURNACES for nearly 4 years, after having studied mechanical engineering at Politecnico di Milano. 

For more information: Contact Giorgio at info@tav-vacuumfurnaces.com.


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Sintering Considerations: Vacuum vs. HIP

Source: TAV Vacuum Furnaces

When processing cemented carbide, there are a few considerations you need to understand to use the proper sintering equipment. One of the biggest factors is the actual material; what is the colbalt content level of the processed material?

In this best of the web article, walk through the steps of dewaxing, sintering for appropriate densification, and the processing temperatures that are required for sintering cemented carbide.

An Excerpt:

“Other than mechanical stresses due to the differential pressure between inside and ambient pressure outside the furnace, operating at relatively high temperatures with high pressure of gas would lead to significant dissipations of heat to the external environment. This is not only anti-economic from an efficiency point of view, but could also compromise the structural integrity of the water-cooled steel vessel of the furnace by overheating it.”

Read the entire article from TAV Vacuum Furnaces, written by Giorgio Valsecchi, by clicking here: “SINTERING OF CEMENTED CARBIDE: A USER-FRIENDLY OVERVIEW – PT.2


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An Overview of Cemented Carbide Sintering

Source: TAV Vacuum Furnaces

Cemented carbide is often used interchangeably with other terms in the industry to describe a popular material for tool production. However, the specifics of what makes up a cemented carbide, and how this material can be processed, are not so widely discussed.

In this best of the web article, discover the composition, applications, and processes involved in sintering cemented carbide, as well as how vacuum furnaces play an essential role for this material. You will encounter helpful diagrams and resourceful images depicting each step of the process.

An Excerpt:

“Hard metal, or cemented carbide, refers to a class of materials consisting in carbide particles dispersed inside a metal matrix. In most cases, the carbide of choice is tungsten carbide but others carbide forming element can be added, such as tantalum (in the form of TaC) or titanium (in the form of TiC).
The metal matrix, often referred as ‘binder’ (not to be confused with wax and polymers typically used in powder metallurgy) is usually cobalt, but nickel and chromium are also used. This matrix is acting as a ‘cement,’ keeping together the carbide particles (hence the ‘cemented carbide’ definition).”

Read the entire article from TAV Vacuum Furnaces, written by Giorgio Valsecchi, by clicking here: Sintering of Cemented Carbide: A User-Friendly Overview- Pt. 1


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This Week in Heat Treat Social Media


Welcome to Heat Treat Today's This Week in Heat Treat Social Media. You know and we know that there is too much content available on the web, so it’s next to impossible to sift through all of the articles and posts that flood our inboxes and notifications on a daily basis. Today, Heat Treat Today brings you another hot take of the latest compelling, inspiring, and entertaining heat treat chatter from the world of social media.

We're looking at microscopic images, some in-depth heat treat content, a recap of networking opportunities, plus much more!

If you have content that everyone has to see, please send the link to editor@heattreattoday.com.


1. Art or Science?

Through heat treatment, austempered ductile iron (ADI) becomes incredibly strong. For ADI, the material has been austempered such that the matrix is transformed into ausferrite, or a mixture of acicular ferrite and austenite. The image below has been elevated to art-gallery quality with the use of selective color etching.

Images of weld metal, microstructure of coarse-grain zone, microstructure of fine-grain zone, and base material. See how the crystal orientation changes in different zones.


2. All That Chatter

Check out some of the chatter that everyone has been posting on heat treat topics over the last few months.

 

May the 4th

 

Congratulation on the New Role!

Time Will Tell
________________________________________________________
You Will Be Missed!

3.  Bumping Shoulders with Heat Treaters

It's great to connect with other folks in the industry. This past week has been an amazing opportunity to forge new relationships and strengthen old ones at trade shows and expos.

 

Rapid + TCT

 

Ceramics Expo

 

ACT Expo

 

SAMPE 2023


4. The Reading (and Podcast) Corner

Time to take your afternoon coffee and read a few technical articles from around the industry. Got too many things to do? Put on an episode of Heat Treat Radio to enjoy on your commute. Maybe you'll find some "continuing education" time this weekend!

Is there room for creativity in the heat treat shop?

Listen to an interview with Gary Sharp about ion nitriding. Topics include the history of and applications for this particular kind of nitriding.
Dig in a little deeper. Read more about ion nitriding. Hone in on TMS 80 micro alloyed steel with Dr. Rolinski.

Review of quench basics. Click to watch the video below!


5. Sleep Deprived

The excitement of nitriding keeping you awake at night?!

 

Have a great weekend!


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19 Quick Heat Treat News Chatter Items To Keep You Current

Heat Treat Today offers News Chatter, a feature highlighting representative moves, transactions, and kudos from around the industry. Enjoy these 19 news bites that will help you stay up to date on all things heat treat.

Equipment Chatter

  1. Global commodities group, Anglo American, and thyssenkrupp Steel have signed a memorandum of understanding to collaborate on developing new pathways for the decarbonization of steelmaking. The collaboration will focus on joint research to accelerate the development of high-quality input stock for lower carbon steel production, using both conventional blast furnace and direct reduction iron.
  2. SECO/WARWICK delivered additional CAB lines to SUZHOU RETEK in China.
  3. Tenova was contracted by Sinova Global to supply the basic engineering of a new silicon metal plant in Tennessee. The site will be North America’s most modern and efficient silicon metal plant, a greenfield development for Sinova Global.


Company and Personnel Chatter

  1. Brighton Science and Hubbard-Hall partner to provide the Infinity Surface Cleaning Intelligence Program, which is designed to aid manufacturers to prepare surfaces and prevent problems.
  2. Thermal-Vac Technology, Inc. announced the completion of a new microgrid from Verdant Microgrid, LLC. Collaboration with the following companies ensured the completion: Eos Energy Enterprises of Edison, NJ; Stronghold Engineering, Inc. of Perris, CA; and GridSwitch Asset Management Services of Moon, PA.
  3. Bryan Stern has joined Gasbarre as the product development manager for Gasbarre Thermal Processing Systems. Bryan’s experience, knowledge, and forward-thinking will allow him to support existing clients and advance the company’s growing footprint in the vacuum furnace market.
  4. Ipsen recently launched a new website with the goal of providing a better user experience for customers worldwide. IpsenGlobal.com now incorporates all Ipsen locations, products, and services under one domain.
  5. Furnaces North America 2022, the premier trade show and technical conference in the North American heat treating industry, attracted over 1,200 attendees from around the world. The show produced by the Metal Treating Institute in partnership with its media partner, Heat Treat Today.


Kudos Chatter

  1. Doug Peters, CEO of Peters’ Heat Treating, received the Winslow Award, an honor that is given to an individual or business that has made valuable economic improvements.
  2. A two chamber vacuum oil quench furnace has received Nadcap accreditation. Solar Manufacturing designed the furnace for Solar Atmospheres of Western PA.
  3. Ayla Busch was honored with the German Leadership Award 2022. This award was presented at the annual alumni convention of the Collège des Ingénieurs and is an award for innovative corporate leadership in the German economy.
  4. Texas Heat Treating, Inc. announces that both Round Rock and Texas Heat Treating Worth just completed ISO 17025 lab audits. The audits came back with no findings.
  5. Representatives from TAV VACUUM gave a speech during the first day of the 27th IFHTSE Congress & European Conference on Heat Treatment 2022. The talk was about the heat treatment of titanium alloys, specifically, “Vacuum heat treatment of Ti6Al4V alloy produced via SLM additive manufacturing.”
  6. RETECH, a SECO/WARWICK Group company, was acknowledged as “The Most Innovative Metallurgical Equipment Specialist in 2022 for the USA” by Acquisition International Magazine. Additionally, Earl Good, its managing director, has been honored by The Corporate Magazine in the “Top 20 Most Dynamic Business Leaders of 2022.″
  7. Nitrex Metal, Inc. announced that it was selected for the “American Dream” series airing on Bloomberg and Amazon Prime. The series explores the entrepreneurial stories of men and women who founded and built incredible companies from the ground up.
  8. Jim Oakes, president of Super Systems, has been awarded the first ever Furnaces North America (FNA) Industry Award at the trade show’s opening night kickoff reception.
  9. At the recent 2022 MTI fall meeting held in Indianapolis, IN, the Metal Treating Institute recognized Roy Adkins, director of Corporate Quality, with the MTI Award of Industry Merit. This award is given in recognition of current and ongoing commitment to the betterment of the commercial heat treating industry with one or more significant accomplishments.
  10. Hubbard-Hall has been awarded the Top Workplaces 2022 honor by Hearst Media Services in Connecticut. The award is based solely on employee feedback gathered through a third-party survey that is administered by employee engagement technology partner Energage LLC.
  11. Pelican Wire Calibration Laboratory received “ISO/IEC 17025:2017” accreditation from ANSI National Accreditation Board.

 


Heat Treat Today is pleased to join in the announcements of growth and achievement throughout the industry by highlighting them here on our News Chatter page. Please send any information you feel may be of interest to manufacturers with in-house heat treat departments especially in the aerospace, automotive, medical, and energy sectors to sarah@heattreattoday.com.


 

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Sintering and Binder Jetting With Vacuum Furnaces

Source: TAV Vacuum Furnaces

Ever heard of binder jetting (BJT)? It's an evolving technology that is quickly catching up to metal injection molding (MIM). Compared to MIM, BJT has a lower cost per part rate, produces larger parts, and, because BJT is a cold process, it does not introduce residual stress inside the part.

Even though BJT is a cold process, sintering is a key step in BJT. Read this best of the web article to learn the ins-and-outs of sintering with binder jetting.

An excerpt:

"Vacuum sintering furnaces are usually the go-to choice for sintering of [binder jetting] parts, thanks to the ability to provide bright and shiny sintered parts, the tight process parameters control and the possibility to work with different debinding and sintering atmospheres."

Read more at "Binder Jetting and Vacuum Furnaces: Everything You Need To Know"


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“The Die is Cast”: What’s NADCA 207?

Source: TAV VACUUM FURNACES

When "the die is cast," heat treaters should make sure that they're using NADCA 207 standards. Prepared by the North American Die Casting Association (NADCA) for its members, they provide recommendations on how to produce dies for die casting to optimize thermal tool life in terms of thermal fatigue.

In today's best of the web article, check out what some of the essential requirements are and how this standard could help in "maximizing the resistance of tools to the occurrence of cracks from thermal fatigue."

An excerpt:

However, the content of this specification is so well processed that it is valid not only for the production of die casting dies and for thermal fatigue, but also for many other applications, and is the best information material for commercial vacuum heat treatment plants, tool shops and die casting foundries, enabling the elimination of fundamental errors in the tool making process.

Read more at "DO YOU KNOW WHAT NADCA 207 IS?"

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AMS2750F Review: Calibration Process Instrumentation

Source: TAV Vacuum Furnaces

Heat treat specifications can be tiresome to stay up-to-date on. So it’s great when we find digestible content on AMS2750F to share with you.

In today’s best of the web article, you’ll be able to review the 4 new requirements for process instrumentation and what 18 pieces of information must always be reported in the calibration certificate.

An excerpt:

“The recording tools used on heat treatment plants should not be used to record TUS or SAT sensor temperatures unless it can be demonstrated that the recording channels of the TUS and/or SAT sensors of an integrated system are separated from the recording system of the heat treatment furnace and also meet the requirements of the field test instrument.”

Read more: “AMS2750F Pyrometric Requirements for Heat Treatments: Calibration Process Instrumentation

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Can You Choose the Right Sintering Atmosphere?

Source: TAV VACUUM FURNACES

How do sintering parameters, especially the sintering atmosphere, affect the quality achievable from parts? Do you know what your three gas options are? Find out this and more, including an evaluation of some interesting solutions for your heat treating needs.

An excerpt:

"However vacuum furnaces operating with hydrogen require additional safety measures. For this reason, specific design solutions (such as double seals on all the furnace flanges) and software safeties are adopted. Despite the increased degree of complexity of the equipment and the higher process costs, vacuum furnaces operating with hydrogen over-pressure bring several advantages. . ."

Read more at: "Vacuum Sintering of Stainless Steels: How to Choose the Right Sintering Atmosphere"

Can You Choose the Right Sintering Atmosphere? Read More »

How are Vacuum Furnaces Used for Minting Coins?

Source: TAV VACUUM FURNACES

How does coin production benefit from vacuum heat treating? Is hardening, tempering, and machining required?

In this Best of the Web, take a look at what it takes to create “the master die” and the importance of vacuum heat treating in the minting process. The article offers a few contextualizing points around the topics of green energy and maintaining a safe workplace.

An excerpt:

[blockquote author=”TAV VACUUM FURNACES” style=”1″]The master die is then hardened and tempered to produce a positive tool called hob. Note that the master die is not used to produce coins. What do we need to produce our first coin?[/blockquote]

 

Read more at “Minting Industry: The Importance of Vacuum Heat Treatments

 

 

 

 

 

All images sourced from TAV VACUUM TECHNOLOGIES.

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