Grammer Vacuum Technologies

Getting to the “Hearth” of It: 5 Hearth Tips

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Want a free tip? Read some of the top 101 Heat Treat Tips that heat treating professionals submitted over the last few years. These handy technical words of wisdom will keep your furnaces in optimum operation and keep you in compliance. If you want more, search for "101 heat treat tips" on the website! This selection features 5 tips all about the hearth of your furnace!

Also, check out Heat Treat Resources in the September 2021 magazine to check it out yourself!


Hacksaw Your Hearth!

When loading parts, carefully place the workload on the center of the hearth (front-to-back and side-to-side). Make sure it is stable and no part of the load is close to or touching the heating elements. This can create arcing and damage your parts.

Tip: Once the load is in place, mark the hearth posts with a hacksaw to quickly find the front and back measurements each time.

(Ipsen USA)


TZM Moly Grids

A very commonly observed failure mechanism with a moly post hearth assembly is bending of the moly posts. They will stay fairly straight at the center of the hearth area, but they can distort badly toward the outer sides of the work zone. The outer rows of vertical posts end up leaning away from each other. This is due to the very high linear thermal expansion coefficient of nickel-iron alloy grids (usually 330 SS or Inconel). With a high load on the nickel alloy grid, it is not able to slide on the perpendicular hearth beams as the temperature rises. The outer hearth post rows are forced in an outward direction. The quenching of the furnace load does not reverse all of this effect and over time results in the severe bending of the hearth posts.

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By replacing the stainless steel or nickel alloy grids with a moly or TZM alloy moly grid, which exhibits very low thermal expansion, the hearth life can be increased. For comparison, the figure shows the coefficients of linear thermal expansion for commonly used grid materials. For example, a 36” wide 330 SS grid at 70°F grows to 36.6” wide at 2200°F.

Another significant benefit of TZM moly grids is use at higher furnace process temperatures without the problem of a softened, sagging grid that cannot support the load properly.

(Grammer Vacuum Technologies, Inc.)


How to make thru-process temperature monitoring robot friendly!

In modern rotary hearth furnaces, temperature profiling using trailing thermocouples is impossible as the cables would wind up in the furnace transfer mechanism.

Due to the central robot loading and unloading and elimination of charging racks/baskets the use of a conventional thru-process system would also be a challenge.

Faced with such loading restrictions it is necessary to fit the thermal barrier inside the cavity of the product (engine block shown) and allow automated loading of the complete combined monitoring system and product.

To allow miniaturization of the thermal barrier to fit, but also provide sufficient thermal protection, the use of phased evaporation technology is critical. Such a system allowed BSN Thermoprozesstechnik GmbH in Germany to commission such a furnace accurately and efficiently and thereby optimize settings to not only achieve product quality but ensure energy efficient, cost effective production.

(PhoenixTM)


Hearth Height Adjustment

The available width and height of the work zone in a vacuum furnace with a round hot zone is determined by the elevation placement of the top of the furnace hearth. This distance is determined by the length of the vertical hearth support posts. By having spare, interchangeable hearth post sets of varying lengths, one can extend the work zone width or height as needed. The figure shows a variety of work zone dimensions that are possible with a standard 36” wide x 36” tall typical work zone as an example. The important thing in choosing your work zone shape is to maintain an (approximately) 3” clearance between the elements and the work zone to avoid part to element contact.

Note: With the symmetric shapes of modern, round hot zones there is good reason to expect good temperature uniformity anywhere within the 3” clearance ring shown in Figure 1. If you can build a survey fixture capable of surveying all the space you want to use, you theoretically could use more than just the rectangular space shown in the examples. Getting an auditor to accept the survey is a separate task.

(Grammer Vacuum Technologies, Inc.)


TZM Moly Hearths

In the case of furnaces with all-molybdenum hearths or of graphite hearths with molybdenum (“moly”) support posts, a direct replacement of those moly posts with TZM alloy moly posts will both increase strength of the hearth assembly and eliminate problems with recrystallization-induced embrittlement of the posts. (For an all-moly hearth, replacement of the horizontal load beams with TZM would have a similar benefit.) The comparative strengths vs. temperature of TZM alloy and pure moly are shown in the graph. Whereas at room temperature the strengths are very similar (around 110KSI-120KSI), once you exceed the 2000F recrystallization temperature of pure moly, the difference becomes dramatic. At 2000F the pure moly is about 40% of the strength of TZM alloy. By the time it reaches 2300F the pure moly is only about 25% of the strength of TZM alloy.

Not only is the TZM alloy much stronger than pure moly at temperature, but it also does not suffer from the same embrittlement problems. Pure moly, once it has recrystallized, forms very brittle grain boundaries in its microstructure. Its behavior begins to resemble that of glass. This is the primary mode of failure of moly components in vacuum furnaces – breakage due to intermetallic grain boundary embrittlement. TZM’s recrystallization temperature is around 2500F, and even when it does recrystallize, it forms very fine new grains that still have decent ductility. Hence, we recommend TZM alloy as a replacement for pure moly in all structural applications for vacuum furnaces. It is the “right stuff.”

Note that all metals used in a vacuum furnace, moly and TZM alloy included, will suffer from distortion due to the numerous thermal cycles they experience. Moly hearth beams are a good example. Once distorted moly hearth beams can be very difficult if not impossible to straighten without breaking them. To have any chance at all they must be heated to forging temperatures. TZM hearth beams however, due to their good ductility can often be heated to forging temperatures and successfully straightened. Most heat treating shops scrap out the moly hearth beams rather than even trying to straighten and re-use them. With a TZM hearth the hearth components can typically be re-used with a newly re-lined hot zone saving a large additional expense.

(Grammer Vacuum Technologies, Inc.)


Check out these magazines to see where these tips were first featured:

 

 

 

 

 

 

 


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Getting to the “Hearth” of It: 5 Hearth Tips Read More »

Tips for Your Vacuum Furnace

One of the great benefits of a community of heat treaters is the opportunity to challenge old habits and look at new ways of doing things. Heat Treat Today’s 101 Heat Treat Tips is another opportunity to learn the tips, tricks, and hacks shared by some of the industry’s foremost experts.

For Heat Treat Today’s latest round of 101 Heat Treat Tipsclick here for the digital edition of the 2020 Heat Treat Today fall issue (also featuring the popular 40 Under 40).

Today’s tips come to us from Grammer Vacuum Technologies, Inc. and are all about that clean, bright equipment solution: vacuum furnaces.


Heat Treat Tip #8

TZM Moly Hearths

In the case of furnaces with all-molybdenum hearths or of graphite hearths with molybdenum (“moly”) support posts, a direct replacement of those moly posts with TZM alloy moly posts will both increase strength of the hearth assembly and eliminate problems with recrystallization-induced embrittlement of the posts. (For an all-moly hearth, replacement of the horizontal load beams with TZM would have a similar benefit.) The comparative strengths vs. temperature of TZM alloy and pure moly are shown in the graph. Whereas at room temperature the strengths are very similar (around 110KSI-120KSI), once you exceed the 2000F recrystallization temperature of pure moly, the difference becomes dramatic. At 2000F the pure moly is about 40% of the strength of TZM alloy. By the time it reaches 2300F the pure moly is only about 25% of the strength of TZM alloy.

Not only is the TZM alloy much stronger than pure moly at temperature, but it also does not suffer from the same embrittlement problems. Pure moly, once it has recrystallized, forms very brittle grain boundaries in its microstructure. Its behavior begins to resemble that of glass. This is the primary mode of failure of moly components in vacuum furnaces – breakage due to intermetallic grain boundary embrittlement. TZM’s recrystallization temperature is around 2500F, and even when it does recrystallize, it forms very fine new grains that still have decent ductility. Hence, we recommend TZM alloy as a replacement for pure moly in all structural applications for vacuum furnaces. It is the “right stuff."

Note that all metals used in a vacuum furnace, moly and TZM alloy included, will suffer from distortion due to the numerous thermal cycles they experience. Moly hearth beams are a good example. Once distorted moly hearth beams can be very difficult if not impossible to straighten without breaking them. To have any chance at all they must be heated to forging temperatures. TZM hearth beams however, due to their good ductility can often be heated to forging temperatures and successfully straightened. Most heat treating shops scrap out the moly hearth beams rather than even trying to straighten and re-use them. With a TZM hearth the hearth components can typically be re-used with a newly re-lined hot zone saving a large additional expense.

(Grammer Vacuum Technologies, Inc.)


Heat Treat Tip #18

Hearth Height Adjustment

The available width and height of the work zone in a vacuum furnace with a round hot zone is determined by the elevation placement of the top of the furnace hearth. This distance is determined by the length of the vertical hearth support posts. By having spare, interchangeable hearth post sets of varying lengths, one can extend the work zone width or height as needed. The figure shows a variety of work zone dimensions that are possible with a standard 36” wide x 36” tall typical work zone as an example. The important thing in choosing your work zone shape is to maintain an (approximately) 3” clearance between the elements and the work zone to avoid part to element contact.

Note: With the symmetric shapes of modern, round hot zones there is good reason to expect good temperature uniformity anywhere within the 3” clearance ring shown in Figure 1. If you can build a survey fixture capable of surveying all the space you want to use, you theoretically could use more than just the rectangular space shown in the examples. Getting an auditor to accept the survey is a separate task.

(Grammer Vacuum Technologies, Inc.)

Tips for Your Vacuum Furnace Read More »

Heat Treat Tips: Vacuum Furnace, Cooling

Heat Treat 2019 was just a month ago, and one of the great benefits of gathering with a community of heat treaters is the opportunity to challenge old habits and look at new ways of doing things. Heat Treat Today’s 101 Heat Treat Tips is another opportunity to learn the tips, tricks, and hacks shared by some of the industry’s foremost experts.

For Heat Treat Today’s latest round of 101 Heat Treat Tipsclick here for the digital edition of the 2019 Heat Treat Today fall issue (also featuring the popular 40 Under 40).

Today’s Technical Tuesday features tips from Grammer Vacuum Technologies covering Vacuum Furnace and Cooilng.

If you have a heat treat-related tip that would benefit your industry colleagues, you can submit your tip(s) to doug@heattreattoday.com or editor@heattreattoday.com.

 


Heat Treat Tip #59

Oxygen Contamination Sources

A common source of oxygen contamination to vacuum furnace systems is in the inert gas delivery system. After installation of the delivery lines, as a minimum, the lines should be pressurized and then soap-bubble tested for leaks. But even better for critical applications is to attach a vacuum pump and helium leak detector to these lines with all valves securely closed, pull a good vacuum, and helium leak check the delivery line system. Helium is a much smaller molecule than oxygen and a helium-tight line is an air-tight line. Also, NEVER use quick disconnect fittings on your inert gas delivery system to pull off inert gas for other applications unless you first install tight shut-off valves before the quick disconnect. When the quick disconnect is not in use, these valves should be kept closed at all times. (Though the line is under pressure, when you open a back-fill valve to a large chamber, the line can briefly go negative pressure and pull in air through a one-way sealing quick disconnect valve.)


Air-cooled vacuum furnace cooling system (from Dry Coolers)

Heat Treat Tip #80

Closed-Loop Water Cooling Systems

Modern water cooling systems for vacuum furnaces are typically closed-loop. (By this we mean that air never comes in contact with the water that goes through your vacuum furnace.  The expansion tank would be pressurized with dry nitrogen, in this case, to prevent oxygen pick-up by the water.) Sometimes after maintenance work, the expansion tank or sump is left open to air. As a result, air/oxygen, dirt, and organic materials can get into the water system and eventually cause both corrosion and plugging of your chamber. A plugged chamber can overheat and explode or implode causing serious injury or death. Replacement chambers are very expensive. A recirculating water system that allows air to contact the water entering your furnace can dramatically decrease the life of your vacuum chamber.


Heat Treat Tip #89

Lanthanated Moly Alloy Strip Increases Element Longevity

Moly and TZM moly grids can double or triple vacuum furnace throughput by using a two-tier or three-tier fixture to utilize unused work zone space.

Pure molybdenum vacuum furnace heating elements distort with time in service due to growth and contraction during thermal cycling. You can often see this distortion beginning just a month or two into service of new elements. Eventually, these will contact either the insulation/shield wall— or worse yet, your parts—and cause electrical arcing. So they need to be replaced before this happens. By making a direct replacement of these pure moly strips with a lanthanated moly alloy strip, the life of the elements can be significantly increased. We have seen a rough doubling of the element life by making this change. Many new OEM vacuum furnaces are now supplied with lanthanated elements at the start. OEM and aftermarket hot zone re-builders are frequently making this change as well to get longer life out of their hot zone elements.


Heat Treat Tip #101

TZM Moly Alloy for Structural Vacuum Furnace Components

For over 30 years, there has been a molybdenum alloy called TZM (Moly-0.5%Ti-0.1%Zr) which is far superior to pure molybdenum in vacuum furnace structural applications. TZM is slightly more expensive than pure moly, so OEM furnace companies use pure moly to keep their costs down for competitive reasons. But they could be offering it as an option for their buyers. Pure molybdenum metal undergoes recrystallization at temperatures as low as 2000°F. The recrystallized structure is very brittle at the grain boundaries, resulting in a structural component that also is very brittle. If you have a vacuum furnace with moly components, you have undoubtedly seen this with older parts. TZM alloy, however, does not recrystallize until around 2500°F, and even then it does not exhibit the brittle behavior of pure moly, because the recrystallized grain size is still very fine. TZM is also stronger than pure moly, as much as 3 to 4 times the strength at temperatures above 2000°F. For a 10-15% premium in cost, you can dramatically extend the life of your moly structural components in your furnaces.

Heat Treat Tips: Vacuum Furnace, Cooling Read More »

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