BULK GASES & SYSTEMS TECHNICAL CONTENT

Heat Treat Tips: How to Install an Ammonia System

During the day-to-day operation of heat treat departments, many habits are formed and procedures followed that sometimes are done simply because that’s the way they’ve always been done. One of the great benefits of having a community of heat treaters is to challenge those habits and look at new ways of doing things. Heat Treat Today101 Heat Treat Tips, tips and tricks that come from some of the industry’s foremost experts, were initially published in the FNA 2018 Special Print Edition, as a way to make the benefits of that community available to as many people as possible. This special edition is available in a digital format here.

In today’s Technical Tuesday, we continue an intermittent series of posts drawn from the 101 tips. The category for this post is Industrial Gases, and today’s tip #39 comes from Dan Herring, “The Heat Treat Doctor®”, of The Herring Group. 


Heat Treat Tip #39

How to Install an Ammonia System

Dan Herring,  “The Heat Treat Doctor®”, of The Herring Group

One of the keys to any successful ammonia system installation in the heat treat shop is to find a supplier who is capable of providing premium grade (also known as metallurgical grade) anhydrous ammonia. This product has little or no water, which could contaminate your process. Look for a specification of 99.995% ammonia.

Once you have picked a supplier, there are several choices when it comes to ammonia storage. For the lowest product price, you should consider a tank of at least 10,000 gallons (43,000 pounds of ammonia.) This allows you to purchase full 38,000-pound tanker trucks of ammonia to reduce your supply costs. One pound of ammonia yields 22.5 cubic feet of vapor or 45 cubic feet of dissociated ammonia (75% H2, 25% N2).

In most states, you must comply with these standards if you have more than 10,000 pounds of anhydrous ammonia on site. So, you need to make sure you comply with OSHA’s Process Safety Management (PSM) and EPA’s Risk Management Plan (RMP).

The second option is to keep below the 10,000-pound threshold by installing a 1,000 gallon (4,400-pound capacity) or a 2,000 gallon (8,800-pound capacity) storage tank. Pricing for ammonia into these tanks runs about 50% higher in the smaller quantities. Even with the lower inventory, you will need to comply with OSHA 1910.111 and any applicable state, city, or county laws. It is critical to check with local agencies to make sure you are in full compliance with these regulations.

Another option for smaller usages are ammonia cylinders, but if stored inside the factory, special containment cabinets are required. Check with your ammonia supplier for the details.

With regard to the installation, in most cases, you need to pour a foundation for the tank, provide electricity to the tank for a sidearm vaporizer (used to maintain pressure in the tank since you will be withdrawing ammonia vapor to the process) and provide piping from the tank to your process. Most suppliers can lease the tank and valves/attachments for a nominal monthly fee depending on your ammonia consumption. You can also add a telemetry unit that allows your supplier to monitor your tank level via an Internet site. You will need to install a water shower near the tank and have gas masks close to the tank. It is a good idea to provide a fence around the tank if your company does not have security. Your supplier should provide hazardous awareness training for ammonia.

You can expect relatively trouble-free operation from a properly installed and well-maintained ammonia supply. Maintenance problems, other than an occasional paint job, are usually minimal but good inspection (including all valving) and frequent leak checks are mandatory. The tank should be visually inspected yearly, probably by your supplier, and the pressure relief valves should be changed every five years.

Submitted by The Herring Group

Photo credit: Video Stock Footage from QuickStock.com


If you have any questions, feel free to contact the expert who submitted the Tip or contact Heat Treat Today directly. If you have a heat treat tip that you’d like to share, please send to the editor, and we’ll put it in the queue for our next Heat Treat Tips issue. 

Heat Treat Tips: How to Install an Ammonia System Read More »

Furnace Gas Composition Controlled with CO and CO2

 

Source: AZO Sensors

 

 

Many heat treat processes require protective or process gases. These gases often require careful monitoring. One of the protective and/or process gases used in many heat treat applications is an endothermic atmosphere which is made up largely of CO, CO2, H2, and N2. This article is about the creation and proper monitoring of endothermic atmospheres.

In an atmosphere furnace, the proper mix of these gases can help facilitate changes in the metal such as proper hardness and strength, resistance to temperature, or improved tensile strength to mention a few. Without careful control of temperature, time and atmosphere, metals can experience unwanted changes in properties such as hydrogen embrittlement, surface bluing, soot formation, oxidation, and decarburization. With such critical outcomes in the balance, it is necessary to control the endothermic gas.

An excerpt:

“In order for the required metal treatment to be a success, you must control and monitor the gas composition with extreme care. The concentrations of gases, CO₂, H₂O, CH₄, N₂, H₂ and CO, that make up the endothermic gas atmosphere should be measured in order to aid the prevention of unwanted reactions and ensure that the endogas generator and the furnace are operating normally.”

 

Read more: “CO and CO2 Control of Endothermic Gas in Heat Treatment Furnaces”

Furnace Gas Composition Controlled with CO and CO2 Read More »

Off-Gas Process Control, Water Detection Technologies Ordered by Indiana Steel Producer

 

A global company providing steel plant and metals industry equipment and services, including heat treating, was recently selected by an Indiana-based steel producer to install and implement its proprietary off-gas process control and water detection technologies.

 Steel Dynamics Inc., at Pittsboro, Indiana, is the second SDI plant to place an order for Tenova’s combined technologies. With this order, SDI Pittsboro will install Tenova’s hybrid extractive/laser NextGen® off-gas analysis system, iEAF® dynamic process control system and Water Detection Technology® (WDT®) as a fully integrated solution on the plant’s 100 ton AC EAF, providing SDI Pittsboro with the world’s most comprehensive technology package of off-gas based EAF process control technology.

Tenova’s technological package combines EAF process automation, thermodynamic models, process hardware, innovative temperature/velocity sensor technology, and water detection.

NextGen® is a hybrid laser/extractive off-gas analysis hardware system that delivers faster analytical response times, requires minimal maintenance and reduces hardware and installation costs.  NextGen® enables the operator to monitor and control furnace conditions helping to mitigate operational risk.

iEAF® Modules 1, 2 and 3 use NextGen off-gas analysis plus Tenova’s proprietary optical off-gas temperature & flow sensors, a link to the plant’s PLC network and a real-time mass & energy balance to dynamically control and optimize chemical energy & electricity consumption  and improve endpoint control to maximize operating cost savings, reduce electrode consumption, increase yield and reduce power on time.  .

 

Off-Gas Process Control, Water Detection Technologies Ordered by Indiana Steel Producer Read More »

Matching Gases with Vacuum Heat Treatment Operations

 

Source: VAC AERO International

 

Relative Gas Supply Cost Notes: [a] Based on a minimum usage of 2830 cubic meters (100,000 cubic feet) per month. [b] All gases compared to nitrogen whose relative cost is unity. [c] Based on liquid supply.
Heat treaters use a variety of gases with vacuum furnaces during the processing cycle in partial pressure operation, for backfilling to atmospheric pressure at the end of the processing cycle, and for cooling/quenching. In this article, VAC AERO describes the most common of these gases — (in order of frequency of use) nitrogen, argon, hydrogen and helium — as well as other common gases such as various hydrocarbons and ammonia (for vacuum carburizing/carbonitriding) and specialty gases such as neon (for certain electronics applications), and analyzes their uses and value in various vacuum heat treating processes. In addition, their relative cost per 100,000 cubic feet, the liquid properties and physical properties of common backfill gases, and the conversion between common pressure and vacuum units are explored.

Read more: “Types of Backfill, Partial Pressure, and Cooling Gases for Vacuum Heat Treatment”

 

Matching Gases with Vacuum Heat Treatment Operations Read More »

Skip to content