CARBURIZING TECHNICAL CONTENT

Temperature Monitoring and Surveying Solutions for Carburizing Auto Components: Introduction

This is the first in a 4-part series by Dr. Steve Offley (“Dr. O”), Product Marketing Manager at PhoenixTM, on the technical challenges of monitoring low-pressure carburizing (LPC) furnaces. This introductory article explains the LPC process and general monitoring needs and challenges. 


Carburizing Process

Dr. Steve Offley (“Dr. O”), Product Marketing Manager PhoenixTM

Carburizing has rapidly become one of the most critical heat treatment processes employed in the manufacture of automotive components. Also referred to as case hardening, it provides necessary surface resistance to wear while maintaining toughness and core strength essential for hardworking automotive parts.

The carburizing heat treatment process is commonly applied to low carbon steel parts after machining, as well as high alloy steel bearings, gears, and other components. Being critical to product performance, monitoring and controlling the product temperature in the heat treatment process is essential.

The carburizing process is achieved by heat treating the product in a carbon-rich environment, typically at a temperature of 900 – 1050 °C / 1652 – 1922 °F. The temperature and process time significantly influences the depth of carbon diffusion and associated surface characteristics. It is critical to the process that, following diffusion, a rapid quenching of the product is performed in which the temperature is rapidly decreased. This generates the microstructure giving the enhanced surface hardness while maintaining a soft and tough product core.

Increasing in popularity in the carburizing market is the use of batch or semi-continuous batch low-pressure carburizing furnaces. New furnace technology employs the dissociation of acetylene (or propane) to produce carbon in an oxygen-free low-pressure vacuum environment, which diffuses to a controlled depth in the steel surface. Following the diffusion, the product is transferred to a high-pressure gas quench chamber where it is rapidly gas cooled using typical N2 or Helium up to 20 bar.

An alternative to gas quenching is the use of an oil quench, used commonly in continuous carburizing furnaces where the products are plunged into an oil bath.

 

Fig 1: Schematics of the LPC Carburizing process showing the Temperature and Pressure steps

Temperature Monitoring Challenges in Low-Pressure Carburizing

As already stated, the success of the carburizing process is governed by careful control of both the process temperature and duration in the heating and quench stages. Obviously, when considering temperature, we are interested in the product temperature, not the furnace. Measuring product temperature through a carburizing process, although possible using trailing thermocouples, as performed historically, is neither easy nor safe, and it disrupts production for lengthy periods.

PhoenixTM provides a superior solution with the use of a “thru-process” temperature monitoring system. As the name suggests, the PhoenixTM temperature profiling system is designed to travel through the thermal process, measuring the product and or furnace environment from start to finish. The system can be incorporated into a standard production run so does not compromise productivity. A high accuracy, multi-channel data logger records temperature from thermocouple inputs, located at points of interest on, in, or around the product being thermally treated. To protect the data logger as it travels through the hostile furnace, a thermal barrier is employed to keep the logger at a safe working temperature to prevent damage and ensure accuracy of measurement. The barrier also obviously needs to protect during the quench, whether that be against high pressure or oil ingress if the quench can’t be avoided.

Employing the PhoenixTM system a complete thermal record of the product throughout the entire process can be collected. A popular enhancement to the system is the use of 2-way RF telemetry, providing real-time process monitoring directly from the furnace, useful for either profiling or performing a live Temperature Uniformity Survey (TUS). The product temperature can be viewed live and downloaded at any point in the furnace. Raw temperature data collected from the process can be converted into useful information using one of the custom-designed PhoenixTM Thermal View Software packages available. The thermal graph can be reviewed and analyzed to give a traceable, certified record of the process performance. Such information is critical to satisfying CQI-9, AMS2750, and other regulatory demands. Fully TUS-compliant reports can be produced in moments from the simple and intuitive software, making accurate TUS a simple and quick task. Information can be used to not only prove product quality but provide the means to confidently change process characteristics to improve productivity and process efficiency (Optimize Diffusion, Soak and Quench).

Temperature Monitoring and Surveying Solutions for Carburizing Auto Components: Introduction Read More »

Novel Carburizing Method with Endocarb System Has Patent Awarded

On January 10, 2017, the United States Patent and Trademark Office awarded patent number 9,540,721 to George Barbour, President of Heavy Carbon Company for a Method of Carburizing which allows a carburizing process in a furnace at high temperatures in a protective atmosphere.  The primary function of this carburizing method  is soot control with an atmosphere flow providing a constant low CH4 to produce a strong reaction for a high quality atmosphere regardless of carbon potential set point.

This new method carburizes at a carbon potential well into the soot range while maintaining a controllable carbon potential with a stable CH4.  This stability maintains a constant reaction, cracking an air/gas mix in a self heated retort to a temperature of 1825f before entry into the furnace.  The high carbon potential penetrates the steel surface at a rate up to 30% faster saving time and money while producing higher quality parts.

In addition to the speed at a higher carbon potential at high temperatures, the atmosphere will also penetrate lower grade steels at lower temperatures without using ammonia to raise the HRC.  The air/gas mix is cracked in a retort outside the furnace to form the atmosphere and is heated at the same high temperature of 1825f before entry into the furnace.  In this manner, the low furnace temperature does not hinder the reaction that must take place in the furnace.

Soot control takes place simultaneously while the carburizing cycle is in operation therefore no time is lost to clean soot from the furnace, instead of using furnace time to remove soot and clean the furnace, loads can be run instead.  Time is money and soot burn out takes time.  Because less time is required per load less gas and power is used resulting in more cost savings.

The Heavy Carbon Company manufactures the patented system which is known as the Endocarb System.  The Endocarb System can be added to existing furnaces or built into a furnace at the time of manufacture.

Novel Carburizing Method with Endocarb System Has Patent Awarded Read More »

Carburizing vs Nitriding: Treatment Modeling

BOTW-50w  Source:  Thermal Processing Magazine

The finite element method can provide insights needed by engineers to calibrate thermal processes, whether it’s carburizing or nitriding, and maximize the benefits of the heat treatment.

Carburizing and nitriding treatments have the same goal: increase hardness on the surface while keeping the core ductility. Carburizing is a process where the part is placed in a confined environment regulated by its carbon content. By adjusting the parameters such as temperature and time, the carbon will diffuse into the part to a certain thickness. While the carbon content (%C) is fairly known at the locations where the carbon has diffused, it is harder to anticipate how far the carbon has diffused. The nitriding process uses the same concept but with nitrogen instead of carbon. The simulation of this process is helpful for the engineer to optimize the process. This article presents two examples to illustrate the carburizing and nitriding heat treatment processes.

Read more: Carburizing and Nitriding Treatment Modeling by Nicolas Poulain

 

Carburizing vs Nitriding: Treatment Modeling Read More »