Mercury Marine’s Vacuum Carburizing and Closed-System Cleaning: A Case Study
What are the ways to improve the cleaning process of component parts and reduce smoke from residue and environmental impact? Mercury Marine faced this challenge head on with a new system. Learn more about their solution in today’s Technical Tuesday case study written by Chris Tivnan the sales manager for North America at SAFECHEM North America Inc.
This informative piece was first released in Heat Treat Today’s August’s 2025 Annual Automotive Heat Treating print edition.
Mercury Marine’s Need for Clean
Mercury Marine is a world leading manufacturer of marine propulsion systems headquartered in Fond du Lac, Wisconsin. A subsidiary of Brunswick Corporation, Mercury Marine designs, manufactures, and distributes engines, services, and parts for recreational, commercial, and government marine applications.
Mercury Marine has an in-house heat treatment facility for the components they manufacture. These components include gear case parts, such as propeller shafts, pinions, forward and reserve gears, and clutches. The parts undergo typical manufacturing steps like turning, milling, or gear tooth generation. Some machines allow for dry cutting, while others involve hydraulic oil. In total, more than 170 distinct metal parts require cleaning before undergoing vacuum carburizing, hardening, tempering, and/or cryogenic treatments.
Carburizing with Closed-Vacuum Solvent Cleaning
But vacuum carburizing has not always been the technology of choice for Mercury Maine. Prior to 2023, parts and components underwent initial cleaning in an aqueous washer before proceeding to atmospheric carburizing. Then, they were quenched in oil and then underwent another round of cleaning with a water-based cleaner.

Mercury Marine made the strategic decision to transition from atmospheric carburizing to vacuum carburizing in 2023. The shift was motivated by concerns related to smoke and environmental impact, particularly the evaporation of oil residuals during tempering. The desire for an overall environmentally friendlier process further fueled this change.
Vacuum carburizing benefits from more stringent cleanliness requirements on parts whereby all residue oils, greases, and debris must be removed entirely to prevent contamination of the furnace and the vacuum pump system. As a result of these considerations, Mercury Marine replaced their existing aqueous cleaning process with solvent-based cleaning, convinced that this solution provided superior and consistently reliable cleaning results.

Source: ECM USA
Their furnace equipment manufacturer ECM recommended a closed-vacuum solvent-based cleaning machine (Model: SOLVACS 3S) from the manufacturer HEMO. This design could be seamlessly integrated into their NANO vacuum carburizing system.
The vacuum cleaning machine runs on the modified alcohol solvent DOWCLENE™* 1601. Because of its lipophilic and hydrophilic properties, DOWCLENE 1601 can remove oils and greases just as effectively as certain polar contaminants like cooling emulsions or solids (e.g., particles and abrasives). The solvent also has low toxicity and good biodegradability.
Enabling High Environmental and Safety Standards
The switch from aqueous to solvent cleaning initially raised some safety concerns within Mercury Marine’s environmental safety committee. However, these concerns were swiftly addressed once the committee understood the operation of a closed vacuum cleaning machine and how it contributes to the highest safety and sustainability standards.
First, the airtight design of the machine virtually eliminates air emissions. The hermetically sealed construction means there is minimal risk of contaminating groundwater. Additionally, full machine automation removes operator handling and minimizes chemical contact.

Second, the machine’s built-in distillation unit enables continuous solvent recovery — as high as 95% in Mercury Marine’s case — thereby significantly reducing chemical consumption and waste while lowering overall cleaning costs. Distillation ensures that parts are consistently cleaned in fresh solvent. The effective cleaning result is further warranted by the high solvent quality in the rinsing step, followed by vapor degreasing as the last cleaning step, which is highly effective due to high temperature difference between parts and vapor. With the drying process below 0.1 psi, a perfect drying of the parts is guaranteed.
Additionally, unlike aqueous cleaning, solvent cleaning does not consume significant water, nor does it require wastewater treatment, providing a considerable cost and environmental advantage.
Using a simple test kit, solvent conditions can be easily monitored on a regular basis. Solvent lifespan can also be extended by adding stabilizers, reducing the need for frequent bath exchanges. Due to the high stability of the cleaner, only minimal stabilizer additions have been required since the machine was first put into operation.
Leveraging CFC for Solvent Cleaning
Another crucial factor supporting solvent cleaning is the use of carbon fiber composite (CFC) workload trays and fixturing of the heat treat batch in the cleaning machine. After cleaning the parts, the CFC fixtures are directly transferred into the vacuum furnace. This streamlined workflow eliminates the need to transfer parts between different fixtures, minimizing part damage or contamination while saving time. The durability and thermal stability of CFC fixtures make them ideal for such demanding applications.

Since CFC is a highly absorbent material, it can soak up liquids during the cleaning process. Any remaining residue in CFC fixtures can be released during a vacuum heat treatment process, contaminating the oven, which will impact the process and cause improper heat treatment outcomes. Unlike aqueous cleaning, which leaves some liquids behind, solvent cleaning under vacuum conditions effectively removes these absorbed residues.
Additionally, CFC fixtures must be properly dried and moisture-free before entering the vacuum furnace. Moisture can lead to contamination, inefficient carburizing, oxidation, or vacuum system problems. Solvents dry much faster than water, mitigating the risk of water vapor migration into the vacuum carburizing system.
Superior Controllability and Quality Results
Since transitioning from atmospheric to vacuum carburizing, Mercury Marine has experienced many benefits due to a significantly more consistent and repeatable heat treatment process.
It is known that residual oxygen within the furnace atmosphere can react with alloying elements on the component’s surface. This interaction can lead to the formation of an oxidation layer, potentially affecting the compressive stress profile. Such layers need to be ground off. However, with vacuum carburization, these intergranular oxidations (IGO) no longer occur.
The vacuum carburizing process follows a precise “boost and diffuse” cycle, where the presence of carbon is transferred via acetylene. This approach provides superior controllability compared to atmospheric carburizing, where natural gas is used. Additionally, the absence of open flames and the energy-efficient design contribute to reduced greenhouse gas emissions.
In the past, Mercury Marine faced cleaning challenges following oil quenching. While maintaining clean quench oil is essential, frequent oil changes can be costly. When the quench oil was not cleaned frequently enough, deposits adhered to parts, especially drive shafts with spiral oil grooves for passage. Despite attempts at aqueous cleaning, such debris could persist, and additional blasting was needed to remove them.
Vacuum carburizing has eliminated this problem as the parts now undergo gas quenching instead of oil quenching, removing the aqueous cleaning step altogether.
The investment in a new furnace system, along with the integrated closed vacuum solvent cleaning machine, has proven highly beneficial. The fully automated system ensures that technicians are not manually handling baskets, while parts are cleaned to the highest standard, enabling a seamless vacuum carburizing process. Mercury Marine has expressed great satisfaction with the results, recognizing the system as a valuable addition to their manufacturing operations.
About The Author:

Sales Manager North America
SAFECHEM North America Inc.
With two decades of experience in the chemical industry, Chris assists manufacturers in determining the right choice of cleaning agent and their parts cleaning operation. He also manages relationships with regional distributors as well as local OEMs/OEAs.
For more information: Contact Chris Tivnan at c.tivnan@safechem.com.
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