Mark Hemsath

14 News Chatter to Keep You Current

Heat Treat Today offers News Chatter, a feature highlighting representative moves, transactions, and kudos from around the industry. Enjoy these 14 news items, including Haynes International Inc.‘s new hydraulic radial forging line to boost production of high-performance nickel- and cobalt-based alloys, the acquisition of JSA/Metalline by Hubbard-Hall Inc. to expand metal finishing service capabilities across the Midwest, Bodycote‘s achievement of independent validation from Bureau Veritas for its carbon footprint calculator tools, and more!


Equipment

1. A major U.S. bearing manufacturer has ordered two advanced SECO/WARWICK USA vacuum heat treat furnaces, reinforcing its commitment to precision manufacturing and capacity growth. The investment supports rising demand across the bearing industry, where consistent metallurgical performance is critical for industrial and aerospace applications.

2. Haynes International Inc. has commissioned SMS Group to supply a new hydraulic radial forging line to increase its production of nickel- and cobalt-based alloys, serving markets such as aerospace and chemical processing in the United States. The integrated plant investment, which includes a forging machine, reheating and annealing systems, and automated material handling, is expected to improve production efficiency, metallurgical quality, and responsiveness to global demand while supporting growth in high-performance alloy manufacturing. 

3. Hertwich Engineering GmbH has delivered a customized rolling ingot foundry — including an Ecomelt PS120 preheat-shaft melting furnace, holding furnace, and vertical casting machine — to  Remi Claeys Aluminium N.V. The new facility, set to begin operations in spring 2026, will enhance process stability and efficiency for processing contaminated aluminium scrap, strengthening competitiveness and sustainability in the aluminium  manufacturing sector.  

4. Marle Group has purchased and will install an additional vacuum heat treating furnace at its Marle Nowak facility in Pancé, France, expanding in-house capacity for heat treating cobalt-alloy orthopedic implants and surgical instruments. Supplied by SECO/WARWICK, the new furnace responds to the Marle Group’s need for rapid cooling of large loads while supporting efforts to improve production control and delivery times for medical device manufacturing. 

5. SMS group is supplying an isothermal forging module to the Institute of Forming Technology and Machines (IFUM) at Leibniz University Hannover to be integrated into their existing press as part of the EU and Lower Saxony-funded “High-performance materials of the future – oWZu” research project. This advanced vacuum forging system will expand research and development of high performance materials for aerospace, medical technology, and industrial applications, accelerating technology transfer and setting new standards in forming reactive superalloys. 

6. Researchers at the Korea Institute of Energy Research (KIER) have developed an electrified heat treatment technology for the annealing stage in galvanized steel strip production that cuts greenhouse gas emissions by over 98% compared with traditional combustion furnaces. The breakthrough replaces fossil fuel burners with electric heating elements while maintaining product quality and productivity, and could significantly reduce equipment costs and support decarbonization in the automotive and appliance steel supply chain. This innovation advances industrial heat treating processes toward carbon-free operation, helping manufacturers meet tightening environmental standards and global decarbonization goals.  

7. SECO/WARWICK has been selected by Brazil’s Isoflama to supply a customized horizontal retort furnace for high-temperature tempering and ZeroFlow nitriding at its heat treatment plant. This new furnace will integrate with Isoflama’s production control system and support processing of large, heavy components, enhancing efficiency and precision to continue serving the automotive, aerospace, and machinery industries in South America.

8. Brugola has implemented CODIAC monitoring technology to ensure reliable tracking and analysis of furnace processes on AICHELIN cast link belt furnaces at its facility. This upgrade enhances real-time oversight of thermal processing parameters, supporting consistent quality and operational efficiency. 

Company & Personnel

9. Hubbard-Hall Inc. has acquired the assets of JSA/Metalline, bringing JSA’s customer-facing team into Hubbard-Hall’s organization to expand sales coverage, technical support, and response times for manufacturers serving the plating and general metal finishing industries across the Upper Midwest/Midwest. The move strengthens regional service capabilities, giving manufacturers more direct access to supplier expertise, streamlined single-source ordering, and stronger technical support for critical surface finishing processes. 

10. AECO Corp. has promoted Maryann Remner to president, effective immediately, where she will lead the company and its three operating subsidiaries — Alloy Engineering, Mach3 Machining, and Thermcraft — which serve high-temperature fabrication, precision machining, and thermal processing equipment markets. 

11. Castings Technology, a UK manufacturer of titanium and steel castings, has announced the creation of twenty new jobs as it expands capacity to meet growing aerospace demand, reinforcing its role in supplying cast components for the sector.

12. WINGENS CONSULTANTS has appointed Mark Hemsath as Executive Consultant – Heat Treat & Advanced Furnace Specialist. Hemsath brings over 30 years of aerospace heat treating experience, with deep knowledge in vacuum systems, nitriding processes, and advanced furnace technologies.

Kudos

13. Bodycote has achieved independent validation from Bureau Veritas for its proprietary carbon footprint calculator tools covering nine core heat treatment processes, enabling customers to request ISO-assured carbon data for thermal processing methods such as vacuum and low-pressure carburizing. This validation enhances transparency and helps manufacturers measure and compare emissions, supporting the selection of lower-carbon heat treatment options. 

14. Ipsen recognized six service technicians — Todd Jones, Casey Guinn, Craig Monaghan, Eric Gould, Alfredo Mendoza, and Dom Wirthlin — for completing its 14-week Field Service Engineer Academy, an intensive hands-on training program for vacuum furnace specialists combining classroom instruction with mentored field experience.

14 News Chatter to Keep You Current Read More »

2 Large Scale Furnaces for Automotive and Marine Propulsion

Two intensive furnace projects are poised to bring heat treating to the automotive brake rotor and marine propulsion systems industries. An FNC furnace has been completed which will process approximately 600,000 brake rotors per year for the automotive industry. An additional pit nitriding furnace has a capacity of 80,000 lb. and will be utilized for the production of large marine gears.

Brake Rotor Furnace

Mark Hemsath
President
Nitrex/UPC-Marathon
Source: Linkedin

“In August our Team received Final Acceptance on two of the most difficult projects in Nitrex history…Our most sophisticated brake rotor semi-continuous FNC furnace is installed at a subsidiary of a major auto maker in Europe. Again, our team worked tirelessly to meet customer demands. I am so proud of our team and what they accomplished,” remarked Mark Hemsath, president of Nitrex/UPC Marathon.

The scale of the brake rotor furnace highlights its uniqueness. The furnace processes approximately 600,000 rotors per year, or about 1.6 metric tons per hour. If run continuously, output could approach nearly a million rotors annually.

The brake rotor furnace integrates a post-oxidation (ONC®) process, allowing control over both the color and oxide layer. This feature sets it apart from furnaces currently in use for brake rotors.

The standard load size of the brake rotor furnace is: 1200 mm x 1200 mm x 1800 mm, with a gross load capacity of up to 4 metric tons. Nitrex was able to offer an extended charge size to 2400 mm deep, which could raise throughput to about 2 metric tons per hour.

Brake rotor furnace
Source: Nitrex

Pit Furnace

Nitrex’s largest pit nitriding furnace
Source: Nitrex

The pit furnace represented another leap forward with a capacity of 80,000 lbs. Engineering efforts centered on maximizing productivity while maintaining the precision nitrided layers expected from smaller systems.

This furnace presented significant logistical challenges due to its sheer size and complexity in transport and installation.

Mark Hemsath remarked: “I am so proud of the effort our entire team exerted to meet schedules, quality demands and design improvements. Our largest ever precision Nitrider (4.5 meter diameter!) for deep-case nitriding of large gears was built on-site with no prior testing.”

The pit furnace is built to handle extremely large gears, typically for marine propulsion systems in very large ships where double-helix gears are standard. These gears, which can weigh 20,000 lb., require 12 days to nitride, not including heating or cooling — a stark contrast to the two-hour cycle time of the afore mentioned semi-continuous rotor furnace, which is for high volumes in automotive settings.

The furnace stands at 4.5 meters (177 inches / 14.75 feet) in diameter and 3.5 meters deep (11.48 feet), marking one of the largest precision nitriding capacities ever built with a retort lining.

Project Highlights

These projects were collaborative, drawing expertise from across the organization.

In Canada, Janusz Szymborski came out of retirement to contribute design enhancements. Lead Designer Kamil Szczudlo and Chief Engineer Marcin Doroszko from Nitrex’s Poland facility drove the design, automation, and gas flow systems, while plant manager Robert Sokolinski coordinated production and logistics. Karl Michael Winter, vice president of Engineering in Germany, worked on advanced brake rotor layer formation.

Heat Treat Today original press release, last updated on 01/21/2026 at 12:22pm.



2 Large Scale Furnaces for Automotive and Marine Propulsion Read More »

Aerospace Manufacturer Expands with 7th Vacuum Furnace

A major North American aerospace manufacturer has placed an order for a seventh vacuum furnace to expand capacity. This furnace is specifically designed for the heat treatment of high-performance engine components and is built to support rigorous production schedules.

Mark Hemsath
President
Nitrex Turnkey Systems

The vertical, large-precision vacuum furnace, built by G-M Enterprises, a Nitrex Vacuum company, is engineered to meet the aerospace company’s growing production needs and its demand for critical engine components. Six VVF series vacuum furnaces have previously been installed for the manufacturer to produce aircraft engine parts across a range of aerospace applications. The latest furnace order includes a 60” x 60” (1,524 mm x 1,524 mm) chamber with bottom loading, capable of handling loads up to 3,000 lbs (1,360 kg).

“The customer’s decision to expand with Nitrex reflects G-M Enterprises’ proven track record in furnace reliability,” said Mark Hemsath, president of Nitrex Turnkey Systems. “Our commitment to quality has anchored this partnership for over three decades.”

Jay Jefsen
Regional Sales Manager
Nitrex Vacuum

“Our long-standing relationship with this aerospace customer underscores Nitrex’s commitment to providing durable equipment backed by robust technical support,” said Jay Jefsen, regional sales manager for Nitrex Vacuum. “We are proud to contribute to their ongoing success and look forward to supporting their production goals with this latest addition.”

The furnace is scheduled for commissioning in April 2025.

The press release is available in its original form here.



Aerospace Manufacturer Expands with 7th Vacuum Furnace Read More »

Heat Treat Radio Series for Spring

OC

The days are getting a little longer, you've saved up some vacation hours, it's time for a break this spring!

Make use of some down time to listen in on a couple of Heat Treat Radio series. Putting in some driving miles, relaxing in the sand, or enjoying a staycation all mean some time to peacefully enjoy some heat treat topics. We've put together an original content piece that lets you listen in on a 3-part series on thermocouples, and a back-to-basics series on heat treat hardening. It's nice to know that there is plenty to listen to; you can just click to play each episode!


Thermocouples 101 with Ed Valykeo and John Niggle

This series gives the opportunity to learn from an expert all about thermocouples. The first episode digs into thermocouple history, types, vocabulary, and other basics. Hear from Ed Valykeo, as he gives some of his own history and then dives into all things thermocouple.

1. Heat Treat Radio #61

Contact us with your Reader Feedback!

The second episode covers thermocouple accuracy and classification. Ed Valykeo continues to review and explain necessary information on how thermocouples are calibrated and used.

2. Heat Treat Radio #62

The final episode in this series gets into discussion with John Niggle about thermocouple insulation types. His review towards the beginning of the episode is helpful, and his discussion of insulation reminds readers that job specifications and requirements are crucial.

3. Heat Treat Radio #64

Metal Hardening 101 

Mark Hemsath sits down with Heat Treat Radio to provide an overview of metal hardening basics. In the first part of the series he provides explanation of what it is, what materials can be hardened, why it has to be done, and more.

1. Heat Treat Radio #49

For the second episode, Mark Hemsath explains five hardening processes: carburizing, nitriding, carbonitriding, ferritic nitrocarburizing, and low pressure carburizing.

2. Heat Treat Radio #54

In this final episode for the metal hardening series, a discussion is presented on newer advances in metal hardening. A call is even put out for new ideas and engineers willing to experiment with some of these advance.

3. Heat Treat Radio #56

As you can see above, this resource provides two series -- each with three parts -- that give a comprehensive look at two fundamental components in the heat treat industry. Both the discussion of thermocouples and the investigation of metal hardening provide educational listening with something for everyone in the form of review as well as maybe some basics that have been neglected or forgotten.


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Heat Treat Future with AM and 3D Printing

OC

All the buzz in our industry seems to indicate that additive manufacturing (AM) and 3D printing are the next hot topics in heat treat, particularly in vacuum heat treat. Heat Treat Today decided to find out how these new technologies are shaping the industry. Read what five heat treat industry leaders had to say about how their companies are preparing for the next generation of AM and 3D printing.

This Technical Tuesday article bringing together the responses from these five companies was first published in Heat Treat Today‘s November 2022 Vacuum print edition.


What changes have you made to accommodate the AM/3D printing marketplace?

Dennis Beauchesne
General Manager
ECM USA, Inc.

The most important changes relate to the build plate size and how it connects to our standard size systems. Build plates are ever-changing, it seems, as customers have new applications and mostly larger build plates are being requested. In addition, the process parameters – such as temperature and time at temperature and quantity of material – are important. These two items have the most to do with reconfiguring equipment for the AM market. We have also been able to implement our wide range of automation and robotics skills into this equipment as the market scales up for high production.

How will your products and/or services change to accommodate this marketplace?

We are/will be introducing equipment that is in line with standard-build plate dimensions along with reducing operating costs.

Share how 3D printing or AM products/services help heat treaters.

Contact us with your Reader Feedback!

Recent debind and sinter applications have involved, as previously mentioned, complete robotics to handle parts after printing, to debind, to sinter, and then to process specialized by ECM, such as low-pressure carburizing. ECM has also provided equipment to provide all three processes in the same furnace without moving the load or requiring the furnace to cool and reheat. This reduces work processing time along with less handling and less utility cost.

What changes have you made to accommodate the AM/3D printing marketplace?

Mark Hemsath
Vice President
of Sales, Americas
Nitrex Heat
Treating Services

Nitrex Vacuum Furnaces, through its GM Enterprises acquisition, has moved heavily into additive manufacturing via large production MIM furnaces, which are able to both remove large amounts of powder binders and sinter the parts in the same process. We are in the process of installing and/or starting up five furnaces for these markets, and we have recently employed even more advanced concepts on high volume wax removal. A further trend is on higher value materials, like nickel and cobalt alloys and titanium, necessitating diffusion vacuum levels for processing. Nitrex Vacuum has had this experience already for many years, so moving to smaller scale 3D designs comes with years of experience.

How might your products and/or services change to accommodate this marketplace?

Smaller units are a trend to keep an eye on. We have over a decade of learning from the large units we offer, and this will allow us to compete in these lower volume markets (i.e., 3D) via our proven expertise. Several facts/ideas that we are keeping top of mind are:

  • Large potential in the future (whole new market starting to evolve)
  • Redesign the product to meet the new needs
  • Good for rapid prototyping and quick low volume parts

Furnaces need to be available with fast delivery 3D printing is finding a tremendous niche in fast part production, sourced internally or sourced quickly. These parts may cost more per piece, but having them fast is often more important, and 3D offers this ability to cut weeks or months off of supply chain sourcing.

Share how 3D printing or AM products/services help heat treaters.

The AM sector is still in growth mode. How we help is to give a full-service solution to those customers who want to really increase their volume yet use vacuum in the process. Vacuum helps to transport the binder vapors away from the parts and into the traps for removal. Full binder removal adds to the quality of the parts, as does vacuum sintering of the final parts. We have supplied a few systems over the years with higher, diffusion vacuum levels. As powder materials evolve to higher value materials, there is more interest in diffusion vacuum, and we recently supplied such a system.

What do readers need to know about AM/3D to make decisions today?

Vacuum is the proper way to debind and sinter. Additionally, 3D printing started slow and there were many technologies evolving. Now, it has started to really grow, and the need for smaller furnaces that can offer the same quality as MIM parts produced in high volumes will be a need for 3D part makers, in medium to low volume parts. This may involve furnaces for sinter only, debind and sinter, or even sinter and heat treat. We can see the need to both sinter 3D parts in a small furnace and also heat treat them with special added processes and surface treatments.

What changes have you made to accommodate the AM/3D printing marketplace?

Phil Harris
Marketing Manager
Paulo

Adding a hot isostatic press has been the most notable change Paulo has made to serve the growing AM market. It goes a step further than that though; heat treatment of AM parts has rapidly evolved, and the desire for custom cycles and more data has caused us to make instrumentation changes and do more R&D type work. Understanding the full production path of the parts and doing our part to reduce the time parts are spending in post-processing steps, including offering stress relief, HIP, EDM, and vacuum heat treatment in a one-stop-shop.

How might your products and/or services change to accommodate this marketplace?

As trials continue and boundaries are pushed for both additive and the accompanying thermal processing, we’re constantly keeping an eye on what’s next. Investing in equipment that’s capable while maintaining and instrumenting it to provide the data and reliability the market needs is the name of the game. Of course, open communication with additive manufacturers and printer designers makes this far easier. We value communication with printer manufacturers as it helps us understand demand for our services in terms of build plate size, since, as we all know, furnaces and HIP vessels aren’t one size fits all!

Share how 3D printing or AM products/services help heat treaters.

Additive parts have become commonplace and we’re now regularly providing HIP, stress relief, and solution treating for them. A more interesting example is for parts printed in Inconel 718; we’ve developed a combined HIP and heat treat (or High Pressure Heat Treat) cycle which was able meet material properties specifications when the traditional processing techniques were not. This is where we feel the real cutting edge is when it comes to heat treatment of additive parts; the slow cooling HIP cycles developed for casting decades ago aren’t always optimal for today’s additive parts.

What changes have you made to accommodate the AM/3D printing marketplace?

Trevor Jones
President
Solar Manufacturing, Inc.
Source: Solar Manufacturing, Inc.

There are several methods for 3D printing and we as heat treaters and vacuum furnace manufacturers generally classify those methods into two basic groups: those that use liquid binding polymers and those that do not.

For the group who does not use liquid binding polymers, there are no changes thus far to the design of the vacuum furnace that must be made. One significant caution is insuring there is no loose powder on the surface or cavities of the parts. Residual powder on or in the parts could have adverse effects on the parts themselves and to the vacuum furnace. The loose powder can liberate from the part during the heat treat or quench steps during the process and contaminate the vacuum furnace. The powder in the furnace is then considered FOD (foreign object debris) for subsequent heat treatments processed in that furnace. The powder could also accumulate over time and cause an electrical ground the heating elements or the quench motor, clog the heat exchanger, contaminate vacuum gauges and hot zone insulation, among other issues.

For the group that does contain liquid binding polymers, in addition to the comments about avoiding loose powder on or in the parts, care must also be taken to accommodate for the vaporization of the binder that occurs during heating of the parts. The binder, in its vapor form, will condense at cooler areas in the vacuum furnace. The condensed areas are potential contamination points and could have all the same issues and concerns of loose powder as described above. The binder collection locations, whether at intentional or non-intentional places, will also have to be routinely cleaned to maintain ideal binder collection, optimum vacuum pumping, and overall furnace performance.

How might your products and/or services change to accommodate this marketplace?

With the growth of 3D printing using liquid binder polymers, Solar Manufacturing has taken what was learned from the furnace modified at Solar Atmospheres of Western PA for MIM and AM processing and applied it to a new furnace product line specific for the debind and sinter applications. Solar Manufacturing collaborated with our affiliate company, Solar Atmospheres of Western PA, in modifying an existing vacuum furnace to accommodate the debind and sintering processes. A modified hot zone was installed, and a dedicated binder pumping port was added that helps minimize and target the condensation of detrimental binders evaporating out of parts containing binders. The modified Solar Atmospheres furnace is extremely valuable in gaining knowledge about various aspects of the process and learning what works, and what does not work, in furnace and recipe design. Combining the knowledge and experience of process development of Solar Atmospheres with the advanced Engineering Design Team at Solar Manufacturing, we believe we have a furnace design that modernizes and simplifies the debinding process while minimizing traditional maintenance issues.

Share how 3D printing or AM products/services help heat treaters.

We developed a process of debinding and sintering stainless steel parts with our affiliate company Solar Atmospheres in Souderton PA. The project started out with our Research and Development group to develop the process for the client’s parts. As the trials scaled up, test coupons became test parts, eventually full-size loads. There are always challenges to scaling up from test parts to production loads and we were able to provide the support the customer needed through that transition. The R&D eff orts were successful, and the client ended up purchasing multiple furnaces, which was the end goal for both parties.

Additionally, Solar Atmospheres is currently vacuum stress relieving a 3D component for a major U.S.-based aerospace company that is in use in aircraft today. Also, numerous large-scale components destined for deep space.

What do readers need to know about AM/3D to make decisions today?

Bob Hill, president of Solar Atmospheres of Western PA, reminded us to “realize and acknowledge that AM is still in its infancy stage. Therefore, many metallurgical uncertainties still exist for the multiple printing processes that exist. Understanding this new kind of metallurgy for each printing process, while developing standards and specifications unique to additive manufacturing, is still a huge obstacle. Until this is accomplished, AM will not be the ‘disruptive’ technology that all the experts predict it will be.” If your business is printing parts with liquid polymer binders, you should seriously consider how you plan on debinding and sintering the parts ahead of time. Printed parts in the “Green” or even “Brown” state are fragile and if you are going to ship the parts somewhere else for the debind and sinter steps, extreme care must be taken to prevent the parts from fracturing during transit. Although the shipping can be safely and successfully accomplished, ideally a furnace is available at the print shop to immediately perform the debind and sinter process to avoid those potential shipping difficulties. The other forms of 3D printing that do not contain liquid polymers generally do have this issue.

What changes have you made to accommodate the AM/3D printing marketplace?

Ben Gasbarre
Executive Vice President
Sales & Marketing
Gasbarre Thermal Processing Systems

From our inception, Gasbarre has had expertise in the powder metallurgy industry, which requires debind and sinter applications similar to that in the AM and 3D printing markets. Our ability to supply equipment for both powder and parts producers has set us up for quick adoption into this market. While considerations need to be made specific to AM, our focus has been on technical support and helping the market grow to higher volume applications.

How might your products and/or services change to accommodate this marketplace?

As adoption of these technologies grow, the volume at which parts need to be produced will grow. Our line of continuous processing equipment in both vacuum and atmosphere applications are well suited. Whether it be debind and sinter, annealing, or stress relieving, we have equipment and expertise that can grow from early production to high volumes.

Share how 3D printing or AM products/services help heat treaters.

Overall, Gasbarre is here to be a resource and support the growth of the additive market. Whether that be through new equipment, servicing existing equipment, or involvement in the industry organizations, we have the expertise to drive success today and into the future!

What do readers need to know about AM/3D to make decisions today?

Additive manufacturing is such a dynamic technology, it is difficult to state one specific item. There is the potential for significant growth opportunities for new applications, but also the potential replacement of traditional manufacturing methods. We also know there is substantial backing for the technology by both private industry and government entities. Like other emerging technologies in the automotive and energies sectors, additive manufacturing isn’t a matter of if, but when it’ll achieve wide scale adoption and high-volume applications.

It is amazing how the list of materials being utilized with this technology is growing. While metals and alloys have not been the majority of the market, it is rapidly growing. With that growth, there is a wide variety of applications and thermal processing requirements for those materials. As well, the different additive and 3D printing processing methods (i.e., binder jetting, powder bed fusion, etc.) leads to a similar diversity in thermal processing requirements.

For more information, contact the leaders:


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Heat Treat Future with AM and 3D Printing Read More »

Aerospace Manufacturer Awaits Heat Treat Vacuum Furnace

HTD Size-PR Logo

Mark Hemsath
Vice President
of Sales, Americas
Nitrex Heat
Treating Services

An aircraft provider of small and large commercial and military jet engines will receive a new vertical vacuum furnace, measuring 84" x 84" with a 6,000 lb. load capacity and operating temperatures up to 2500°F, which will be used for heavy and large-cross section parts and processing high-stacked loads, such as tall engine components.

Nitrex Vacuum Furnaces will deliver the vertical vacuum furnace to this major engine maintenance, repair, and overhaul company in South America. The manufacturer will use the furnace to heat treat many aerospace components with processes including annealing and stress relief. “Shipment of this furnace system, after a number of COVID-related delays, was a milestone for Nitrex,” Mark Hemsath, vice president of Sales and acting general manager at Nitrex Heat Treating Services, Americas said.


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Aerospace Manufacturer Awaits Heat Treat Vacuum Furnace Read More »

Paging Through Heat Treat Today’s Technical Files

OCWe're flipping through Heat Treat Today's technical articles today to highlight four heat treat-related processes: hardening, ferritic nitrocarburizing, titanium processing, and stress relieving. Read our top picks of technical articles from these categories that include a back pocket resource, a podcast episode, and a review of past and future innovations.


HARDENING: Heat Treat Radio: Metal Hardening 101 with Mark Hemsath, Part 1 of 3

Sometimes, the best technical advice comes out in a conversation. Mark Hemsath and Doug Glenn took three Heat Treat Radio episodes to talk about the basics of metal hardening. Listen to or read the transcript of the first episode in this series to get a leg up on metal hardness.

"I think the most important thing is that with metals, you’re trying to get certain features that allow it not to wear over time.  At the same time, you want the part to last.  You don’t want it to break, you don’t want it to chip, you don’t want it to seize up, so there are a lot of different things you can do with the parts to give them certain wear characteristics and hardness."

 

FERRITIC NITROCARBURIZING: Nitriding vs. FNC

How is nitriding different from ferritic nitrocarburizing? Temperature? Materials processed? Costs? Industries? This article is a resource: a table that compares these two processes against the other.

"Skim this straight forward data that has been assembled from information provided by four heat treat experts: Jason Orosz and Mark Hemsath at Nitrex, Thomas Wingens at WINGENS LLC – International Industry Consultancy, and Dan Herring, The Heat Treat Doctor at The HERRING GROUP, Inc."

 

TITANIUM PROCESSING: Titanium: A Fascinating History & Future

Titanium is its own animal, so its sometimes helpful to take a moment to identify what it is and how processing this metal might change in the future. Check out this article to learn more.

"The recycling of titanium is of a different magnitude than other metals due to its value. It took a shortage of titanium in the 1980s–and some innovative metallurgy–to transform valuable titanium scrap back into a qualified ingot. To do this, metallurgists used the reactivity of the metal to their advantage."

 

STRESS RELIEVING: Indentation Plastometry

It's not as flashy as a huge furnace, but understanding stress relieving is key to heat treat parts correctly. Plastometrex is a new technology to advance what we know and how we test stress on projects. Read all about.

"The oxidized layer was then removed and the Hardox steel samples were indented in the locations that are shown in Figure 5a. The indentation data were analyzed and converted into stress-strain curves using the SEMPID software. Two are shown in Figure 5b, where it is apparent that the high temperature brazing process has affected the strength characteristics of the material in that location."


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Celebrate January 6th: National Technology Day!

OCWhat’s new in heat treat? A LOT.

Over the past year, we’ve seen numerous new technologies in the way of research, new partnerships, and conversations throughout the industry. So in honor of today being #NationalTechnologyDay, we’re sharing an original content article about just several of these new technologies that are changing the work of heat treaters across North America.


Research

Using HIP to Advance Oregon Manufacturing Innovation Center Programming “‘Today’s globally competitive manufacturing industry demands rapid innovations in advanced manufacturing technologies to produce complex, high-performance products at low cost,’ observes Dr. Mostafa Saber, associate professor of Manufacturing & Mechanical Engineering Technology at Oregon Tech.”

College Students Implement a NEW Heat Treat Solution with Induction? “‘We were in shock,’ Dennis admitted, ‘because we didn’t expect it to [work].’ The expectation, Dennis continued, was that something would go wrong, like the lid would not be able to clamp down, or the container would leak.”

The Age of Robotics with Penna Flame Industries“The computerized robotic surface hardening systems have revolutionized the surface hardening industry. These advanced robots, coupled with programmable index tables, provide an automation system that helps decrease production time while maintaining the highest quality in precision surface hardening.”

New Partnerships

Captive Extrusion Die Maker Levels Up With 11 New Furnaces Heat treaters are leaning into the benefits of nitriding and vacuum technology.

Auto Partner Enters Agreement for New Nitriding Technology As nitriding technology becomes more popular, heat treaters are brushing up on their understanding of case hardening processes across the board. (Read this article comparing 5 common case hardening processes.)

Vacuum Heat Treat Supplier Partners with Neota to Advance MIM Technology Learn how this partnership produced solid and strong metallic parts with near 100% density.

Conversations in the Industry

Heat Treat Radio: Five experts (plus Doug Glenn) discuss hydrogen combustion in this episode. An easily digestible excerpt of the transcript circulated by Furnaces International here and is available to watch/listen/read in full for free here.

Heat Treat Radio: Get on-the-ground projections of what technologies Piotr Zawistowski believes will be bringing in the future. Watch/listen/read in full here

Heat Treat Radio: HIP. The Revolution of Manufacturing, that is, according to Cliff Orcutt. Watch/listen/read in full here

Heat Treat Radio: Will indentation plastometry find its way into North America? If you’ve been listening to James Dean, it seems like it already has. Watch/listen/read in full here

Heat Treat Radio: Fluxless inert atmosphere induction brazing. That’s a mouthful! But what is it? Watch/listen/read in full here

Learn More About New Tech!

Everything You Need to Know About HIPing eBook

Metal Hardening with Mark Hemsath Podcast

Stories About Heat Treaters Implementing New Hardening Methods Article

 

 

Celebrate January 6th: National Technology Day! Read More »

Looking to a Future with FNC or Nitriding?

OCWhat's the future of ferritic nitrocarburizing and how does it compare to other hardening processes? When it comes to metal hardening, there are many variations on central processes, including recent innovations in how to apply hardening processes.

This Technical Tuesday brings you a quick overview of how hardness technologies differ, specifically nitriding and FNC, and how certain heat treaters have developed these specific hardness technologies.


Understanding the Various Hardening Processes

If you want to know the future, the best you can do is understand the past and present. Let’s begin with looking at the most common hardening processing methods. Here are a few excerpts from “Elevate Your Knowledge: 5 Need-to-Know Case Hardening Processes” by Mike Harrison, engineering manager of Industrial Furnace Systems Division at Gasbarre Thermal Processing Systems:

Read more about these 5 processes in Mike Harrison's article. Click to read.

Carburizing: “Gas carburizing is a process where carbon is added to the material’s surface. The process is typically performed between 1550-1750°F, with carburizing times commonly between 2-8 hours [this spec is disputed, and times may run up to 24 hours]; of course, these values can vary depending on the material, process, and equipment. The most common atmosphere used for atmosphere gas carburizing is endothermic gas with additions of either natural gas or propane to increase the carbon potential of the furnace atmosphere.”

Nitriding: “Gas nitriding is a process where nitrogen is added to the material surface. The process is typically performed between 925-1050°F; cycle times can be quite long as the diffusion of the nitrogen is slow at these temperatures, with nitriding times typically ranging from 16 – 96 hours or more depending on the material and case depth required. Nitriding can be performed in either a single or two-stage process and has the potential to produce two types of case, the first being a nitrogen-rich compound layer (or “white layer”) at the surface that is extremely hard and wear-resistant but also very brittle.”

Carbonitriding: “Despite its name, carbonitriding is more closely related to carburizing than it is to nitriding. Carbonitriding is a process where both carbon and nitrogen are added to the material surface. This process is typically performed in a range of 1450-1600°F [this spec is disputed, and temperatures may go up to 1650°F] and generally produces a shallower case depth than carburizing.”

Ferritic Nitrocarburizing (FNC): “In the author’s opinion, just like with carbonitriding, ferritic nitrocarburizing (FNC) is named incorrectly as it is more closely related to nitriding than it is with carburizing. FNC is a process that is still mostly nitrogen-based but with a slight carbon addition as well. The added carbon helps promote compound layer formation, particularly in plain carbon and low alloy steels that do not contain significant nitride-forming alloys. This process is typically performed in a range of 1025-1125°F with cycle times much shorter than nitriding, typically 1-4 hours.”

Low Pressure Carburizing (LPC): “Low-pressure carburizing (LPC), or vacuum carburizing, is a variation of carburizing performed in a vacuum furnace. Instead of the atmospheres mentioned previously, a partial pressure of hydrocarbon gas (such as acetylene or propane) is used that directly dissociates at the part surface to provide carbon for diffusion. After LPC, the workload is transferred to a quench system that could use oil or high-pressure gas, typically nitrogen.”

Nitriding

Learn more about the basics of hardening at Heat Treat Radio. Click to listen,

Gas nitriding, a process over 100 years old, is a hardening process that involves diffusing nitrogen into the surface of steel to create a hard, wear-resistant case. Among many benefits, the part will have enhanced fatigue properties, anti-galling properties under load, and a resistance to softening at elevated temperature. This makes it an excellent choice for the aerospace industry.

There is some recent history regarding problems related to the “white layer”. In a typical microstructure, the “white layer” is a nitrogen-rich surface layer and the diffusion layer exists beneath it.1 It is essential that the surface layer be controlled to avoid an overly brittle part. Mark Hemsath the vice president of Sales – Americas for Nitrex Heat Treating Services, elaborated on this in a Heat Treat Radio episode:

"Doug Glenn: I assume, with all the modern day technology and whatnot, we're able to control that white layer and/or depth of nitriding layer through your process controls and things of that sort."

"Mark Hemsath: Yes. Nitriding has been around a long time, but one of the problems that they had was controlling the white layer. Because they basically would just subject it to ammonia and you kind of got what you got. Then they learned that if you diluted it, you could control it. That's with gas nitriding. Then plasma nitriding came around and plasma nitriding is a low nitriding potential process. What that means is it does not tend to want to create white layer as much. It's much easier to control when the process itself is not prone to creating a lot of white layer, unlike gas. Now, in the last 10 – 15 years, people have gotten really good at controlling ammonia concentrations. They've really learned to understand that."

Recently, SECO/WARWICK shared their nitriding technological developments in their product, ZeroFlow.

"ZeroFlow nitriding is ammonia-based gas nitriding," commented Dr. Maciej Korecki, PhD Eng., vice president of the Vacuum Furnace Segment at SECO/WARWICK Group. "It is distinguished by the fact that the nitrogen potential is controlled by introducing the right portion of ammonia at the right time and only ammonia, instead of a continuous flow of a mixture of ammonia and diluent gas."

"Consequently, the ZeroFlow method uses the minimum amount of ammonia needed to achieve the required nitrogen potential and replenish the nitrogen in the atmosphere, taking into account the situation where no ammonia is supplied to the furnace at all, no flow, hence the suggestive name of the solution," he continued. "Using ammonia alone in the nitriding process, we are dealing with a stoichiometric reaction (as opposed to some traditional methods), that is, one that is uniquely defined and predictable based on the monitoring of a single component of the atmosphere. Therefore, the ZeroFlow process controls very precisely through the analyzer only one gas, obtaining an improvement in the quality and repeatability of the results compared to various traditional methods."

According to Dr. Korecki, the process is about going back to the basics of nitriding: "The inventor of the method is Prof. Leszek Maldzinski of the Poznan University of Technology, who developed the theoretical basis and confirmed it with research. Then, more than 10 years ago, a partnership between SECO/WARWICK and the Poznan University of Technology initiated a project to develop and build the first industrial furnace designed to perform the ZeroFlow nitriding processes. The furnace was launched at SECO/WARWICK's research and development department (SECO/LAB®), where the method has been implemented and validated on dozens of industrial-scale processes."

Ferritic Nitrocarburizing

This nitrogen-based process can produce a deeper compound layer than nitriding, which is great for industrial machinery applications where this deep layer is needed for increased wear resistance and the critical strengthening of a deep case depth is not essential.

FNC has gone through a technical evolution with different heat treaters in the industry developing their own unique applications with method in mind. We'll look at two recent examples: AHT's Super Ultra Ox and Bodycote's Corr-I-Dur.

Edward Rolinski
Senior Scientist
Advanced Heat Treat, Corp.
(Source: https://www.ahtcorp.com/)

According to experts at Advanced Heat Treat Corp. (AHT), Edward Rolinski (Dr. "Glow"), Jeff Machcinski, Vasko Popovski and Mikel Woods, "Thermochemical surface engineering of ferrous alloys has become a very important part of manufacturing. Specifically, nitriding and nitrocarburizing (FNC) processes are used since their low temperature allows for treatment of finished components. They are applied to enhance the tribological and corrosion properties of component surfaces.2 In many situations, nitriding replaces carburizing even if the nitrided layer is not as thick.3 A post-oxidizing step, applied at the end of FNC, leads to significant enhancement of corrosion properties by formation of a magnetite layer (Fe3O4).

"AHT’s newly developed process, UltraOx® Hyper, results in superior wear and corrosion resistance and allows for good control of the parts’ blackness. The latter is very important when the treatment is used for firearms. While the parts’ corrosion resistance improves with nitriding alone, the additional steps in UltraOx® Hyper significantly extend corrosion resistance. AHT is committed to achieving its customers’ desired metallurgical and cosmetic results through R&D and investing in state-of-the-art equipment. These innovations allow for flexibility in these areas."

In recent news, wave energy pioneer CorPower Ocean will be using Bodycote's thermochemical treatment, Corr-I-Dur®, for CorPower’s high-efficiency WECs.
Image Source: www.waterpowermagazine.com

From Bodycote, they say that their proprietary Bodycote thermochemical treatment “Corr-I-Dur® is a combination of various low temperature thermochemical process steps, mainly gaseous nitrocarburising and oxidising.”

They explain, "In the process, a boundary layer consisting of three zones is produced. The diffusion layer forms the transition to the substrate and consists of interstitially dissolved nitrogen and nitride precipitations which increase the hardness and the fatigue strength of the component. Towards the surface it is followed by the compound layer, a carbonitride mainly of the hexagonal epsilon phase. The Fe3O4 iron oxide (magnetite) in the outer zone takes the effect of a passive layer comparable to the chromium-oxides on corrosion resistant steels.

"Due to the less metallic character of oxide and compound layer and the high hardness abrasion, adhesion and seizing wear can be distinctly reduced. Corr-I-Dur® has very little effect on distortion and dimensional changes of components compared to higher temperature case hardening processes."

How to Implement?

We’ve seen a lot of development in way of nitriding and ferritic nitrocarburizing (FNC), but for many heat treaters, you inherit specific processes and traditions of accomplishing heat treatment and do not have the chance to understand how to implement each process. Read the full 21 point comparative resource at FNC vs. Nitriding

Conclusion

The more informed you are, the better decisions you can make. For example, knowing these recent developments in metal treating and hardening is sure to help you decide whether to shift directions in how you company process parts for electric vehicles, or if you are ready to expand your offerings for your aerospace clients. It is clear that each of these processes have a future all-their-own. It’s up to you to decide whether that future should be yours, too.

For more information on the basics of hardness, listen to the what, why, and how of hardening with Mark Hemsath, an expert on metal hardness and vice president of Sales – Americas for Nitrex Heat Treating Services, on this Heat Treat Radio episode with Doug Glenn, publisher of Heat Treat Today. You can also review the resources below that were referenced in today’s article.

 

References

1 Daniel H. Herring, “The Heat Treat Doctor”, “Case Hardening of Steel, Part Three: Gas Nitriding,” PowerPoint Presentation, © 2004 – 2010 The HERRING GROUP, Inc.

2 “Thermochemical Surface Engineering of Steels”, Woodhead Publishing Series in Metals and Surface Engineering: Number 62, Ed. Eric J. Mittemeijer and Marcel A. J. Somers, Elsevier, 2015, pp.1-769.

3 J. Senatorski, et. al, Tribology of Nitrided and Nitrocarburized Steels”, ASM Handbook Vol 18, Friction, Lubrication and Wear Technology, ed. G. Totten ASM International, 2017, pp. 638-652.

 

Resources

  1. Herring, “Case Hardening of Steel, Part Three: Gas Nitriding,” PowerPoint Presentation, © 2004 – 2010 The HERRING GROUP, Inc.
  2. Harrison, “Elevate Your Knowledge: 5 Need-to-Know Case Hardening Processes,” Heat Treat Today, https://www.heattreattoday.com/processes/hardening/hardening-technical-content/comparative-study-of-5-case-hardening-processes/.
  3. Hemsath and D. Glenn, “Heat Treat Radio: Metal Hardening 101, Part 2 of 3,” Podcast and Transcript, Heat Treat Today, https://www.heattreattoday.com/media-category/heat-treat-radio/heat-treat-radio-metal-hardening-101-with-mark-hemsath-part-2-of-3/.
  4. Orosz, T. Wingens, and D. Herring, “Nitriding vs. FNC,” Heat Treat Today, https://www.heattreattoday.com/processes/nitrocarburizing/nitrocarburizing-technical-content/integrated-nitriding-and-fnc/.
  5. Senatorski, J. Tacikowski, E. Rolinski and S. Lampman, “Tribology of Nitrided and Nitrocarburized Steels”, ASM Handbook Vol 18, Friction, Lubrication and Wear Technology, ed. G. Totten ASM International, 2017.
  6. “Thermochemical Surface Engineering of Steels”, Woodhead Publishing Series in Metals and Surface Engineering: Number 62, Ed. Eric J. Mittemeijer and Marcel A. J. Somers, Elsevier, 2015, pp.1-769.

Looking to a Future with FNC or Nitriding? Read More »

Parts Cleaning: What the Experts Are Saying

OCIn the past, the topic of parts cleaning was not one that garnered much attention in the heat treating industry, but today, things have changed. Interest in parts cleaning is at an all-time high and that makes the need for parts cleaning discussion of vital importance in all types of heat treatment processes.

This article appears in Heat Treat Today's 2021 Automotive August print edition. Go to our digital editions archive to access the entire print edition online!


Heat Treat Today wanted to discover why parts washing is such an important step in the heat treat process and about its growing value, so we contacted respected industry experts for an in-depth analysis of the growing popularity of this important step in heat treating.

The following experts contributed to this analysis: Fred Hamizadeh, American Axle & Manufacturing (AAM); Mark Hemsath, Nitrex Heat Treating Services (HTS); Tyler Wheeler, Ecoclean; Experts at Lindberg/MPH; Andreas Fritz, HEMO GmbH; Richard Ott, LINAMAR GEAR; and Professor Rick Sisson, Center for Heat Treating Excellence (CHTE) at Worchester Polytechnic Institute (WPI).

Heat Treat Today asked 13 questions regarding parts washing and encouraged the experts to answer as many as they wished. The following article is a compilation of their experienced insight.

What role does parts cleaning play in the heat treat process and component quality? What is the cost or consequence for heat treating when cleaning is not done correctly? Any anecdotes you can share with us?

Fred Hamizadeh
Director of
Heat Treat & Facilities Process
American Axle & Manufacturing

Fred Hamizadeh, the director of Heat Treat & Facilities Process at American Axle & Manufacturing (AAM), says, “As a captive heat treater (supplying parts that are used in a final assembly), cleanliness of parts is of paramount importance to the longevity and durability of the final product. Parts that are completely unclean prior to heat treating can cause non-uniform case; and uncleaned parts after quenching can cause a multitude of issues, from failure in post-heat treat operations to higher cost of tooling due to contaminated surface, to fi res in temper furnaces from burn-off of the remnant oils on the surface of parts.”

Mark Hemsath
Vice President
of Sales, Americas
Nitrex Heat
Treating Services

Mark Hemsath, the vice president of Sales, Americas, at Nitrex Heat Treating Services replies, “For many surface engineering treatments like gas nitriding and ferritic nitrocarburizing, surface cleanliness is very important. Various oils and organic substances can impede—selectively or broadly—diffusion and surface activity. Some surface contaminants will bake on or ‘varnish’. Some can be removed with slow heating and purging or vacuum, or even surface activation, but it is not a reliable science. Either way, by positively cleaning them beforehand, problems are avoided. The issues occur when the composition and/or concentration of surface contaminants are not well known or preannounced. Pre-washing and cleaning take time, cost money, and must be studied and discussed with customers prior to any start of production. When parts are promised ‘clean', but arrive coated in an unknown rust preventative or cutting/forming oils, they need to be cleaned.”

Tyler Wheeler
Product Line Manager
Ecoclean

Ecoclean’s Tyler Wheeler, a product line manager, shares, “Cleaning plays a critical role that will directly affect the success of the heat treating process. While sometimes looked at as a nonvalue-added process, the consequences of not cleaning correctly are many and can be costly. Depending on the method of heat treating, quality issues may range from staining, discoloration, inconsistent properties, and even damage severe enough to scrap entire batches. Not only are there consequences for the workpieces themselves, but these problems may extend to damaging the heat treating equipment itself, leading to downtime and expensive repairs.”

The experts at Lindberg/MPH report there are several benefits to cleaning parts prior to any heat treating. They say: “By washing the parts prior to heat treating, it assures that the furnace chamber will remain conditioned and free from vapors, resins, binders, or solvents that could attack the refractory lining or heating elements and cause pre-mature failure of those items.”

What about the cost or consequences when the cleaning is not done correctly? “Washing parts prior to any thermal process, removes any layer of machine or cutting oils etc., which can be baked on and require additional and costly processes such as grit blasting, machining, or grinding to remove the unwanted layer on the surface of the parts.”

The Lindberg/MPH experts had an interesting anecdote to share about the importance of parts cleaning: “A customer was using a simple spray washer to clean small sun gears with an inner spline. The parts were to be carburized afterwards. The spray washer didn’t remove the machine oil used in the broaching process. During the carburizing process, the machine oil acted as a shield and didn’t allow the carbon to penetrate the ID properly, thus causing part failure on the gears. Afterwards, a dunk washer with heated water and a dry-off was purchased to clean the parts.”

Andreas Fritz
CEO
HEMO GmbH

Andreas Fritz, CEO at HEMO GmbH, explains, “Cleaning has always played a role in heat treatment. The question was always, ‘How clean is enough to keep the cleaning process as cheap as possible?’ Nowadays, especially in LPC or nitriding processes, the cleaning quality is at least equal to the hardening quality, because heat treaters understand that these processes belong together. There are no good hardening results without good cleaning quality.”

Additionally, Fritz continues, “a cleaned surface lowers the risk of defective goods after heat treatment by helping to provide a very good hardening depth and compound layer.”

Fritz shares a company-altering anecdote: “In the mid-1990s, we sold the first machine to a Bosch automotive supplier which had a captive heat treatment department. They delivered the cleaned and then hardened goods to Bosch, and their QM sent the goods back stating they were not hardened.

“Our customer asked if they checked the hardening quality, and Bosch replied: no, because the parts were not black; therefore, coming to the conclusion that they had simply forgotten to harden them. The supplier invited them to see that the parts were cleaned in a new way with a solvent-based cleaning machine under full vacuum. Since they came out spot-free after cleaning, there was no oil left, which formerly cracked on the surface and left the black color. The result was that for a couple of years, Bosch wrote on drawings that the parts had to be HEMO-cleaned before hardening. This was our start in the heat treatment industry and today, we make 50% of our annual turnover there.”

LINAMAR GEAR’s Richard Ott, a senior process engineer, offers his perspective, “Pre-cleaning and post-washing are very important because all parts coming into our plant can’t have any contamination on them. After heat treating, all parts are washed and blown off before temper.”

Historically, cleaning has not received the attention it deserves in the heat treat process. Have you seen any positive changes in perception among heat treaters in recent years?

Wheeler of Ecoclean addresses the perception of value: “Historically, the cleaning process has been looked at as a non-value-added necessity of manufacturing. However, this attitude is becoming a thing of the past for companies who invest in a quality cleaning process. As of late, customers have placed a greater focus on their cleaning processes both before and after heat treating as quality and production demands continue to increase. A proper cleaning process can eliminate scrap, increase uptime, and lead to a better-quality product for the end customer, which may translate into additional orders. When considering the holistic benefits of a proper and robust clean process, the old mentality is starting to change.”

The experts at Lindberg/MPH reply, “For many years washing parts before or after heat treating was considered an optional process and often bypassed. Today, most commercial and captive heat treaters are using parts cleaning as a necessity, particularly in the growing vacuum heat treating sector, where any contamination is detrimental to the hot zone and pumping systems.”

HEMO’s Fritz explains, “Commercial heat treaters specifically, changed their minds very early because they saw the chance to cover the various cleanliness demands of all hardening methods and processes with one single cleaning system. The hybrid cleaning system which made it possible to clean with solvent or with water or in combination in the same machine, made it possible for them to ensure hardening quality for any incoming good, no matter which residue was on it.

“They were able to cut down costs by using only one cleaning system and by increasing the income per ton due to increased quality and less defective parts.

“The captive heat treaters changed when they sent parts outside to commercial heat treaters while they did annual maintenance or when they didn’t have enough of their own capacity. The returned parts were of much better quality; and they started introducing this kind of cleaning system as well.”

Hemsath of Nitrex agrees about rising standards: “Similar to other areas of heat treatment, OEMs continue to raise their standards for part cleanliness. Sometimes these standards are rooted in functional requirements such as minimizing the number of foreign particles in a closed system in the finished product and other times the requirements are purely aesthetic. In either case, the result is that, in recent years, heat treaters have been required to devote more resources to improve their cleaning processes proactively during the quoting/process design stages, or reactively as a result of non-conformance. Many commercial heat treaters have come to understand that evaluating the cleaning needs of a part and implementing a robust cleaning process before production begins results in a better customer experience as well as improved long-term profitability.”

AAM’s Hamizadeh concurs with a positive change in perception: “Yes! As automotive industry reliability demands are increased, more and more attention is placed on all aspects of cleanliness, which includes heat treat washers.”

Ott, of LINAMAR GEAR, shares evidence of the rise in parts cleaning importance, saying, “Yes, our washers are checked twice a day for concentration and cleanliness.”

How can heat treaters determine their cleaning needs?

Rick Sisson
George F. Fuller
Professor and Director of the Center
for Heating Excellence (CHTE)
Worchester Polytechnic Institute

Rick Sisson, the George F. Fuller Professor and director of the Center for Heating Excellence (CHTE) at Worchester Polytechnic Institute (WPI), explains, “The incoming materials should be carefully examined visually to identify the type and quantity of surface contamination. Look for heavy oil, light oil, cutting fluids and/or rust, and scales. The cleaning process should be selected to remove the type of surface contamination identified. In general, a cleaning process should be included prior to heat treating to ensure a predictable response to the heat treating or surface modification process.”

Sisson continues, “The heat treater must confer with their customer to determine the post-heat treat cleaning requirements. If the part will be ground or machined after heat treat, then post-heat treat cleaning is not required. However, if the part is ready to be shipped, then the appearance is important. For medical applications, any discoloration may be a cause for rejection. The surface finish may be important and should be discussed with the customer.

“The pre-heat treat cleaning requirements are determined by the effects of cleanliness on the heat treat performance. For surface treating, a dirty surface may affect the carburization or nitriding performance. Nitriding is very sensitive to the surface cleanliness. A fingerprint can inhibit the nitrogen uptake and result in soft spots. Carburizing is less sensitive to oils and grease, but corrosion products may inhibit the surface reactions and cause soft spots. However, it is best practice to examine the preheat treat parts and clean away the oils and grease. Corrosion products (aka rust) and cutting fluids ensure a uniform response to the heat treating process,” Sisson concludes.

Hamizadeh of AAM states, “Most customers should have a specification. Start by reviewing the provided prints and follow up with the final customer to determine if parts are further washed with dedicated process washers prior to installation in the final product.”

He concludes, “Nevertheless, heat treaters must provide a part which is clean, uniform in color, and free of quench oil on surfaces and cavities. Parts must also not exhibit any markings from oxidized quench oil (tiger stripes), either.”

“We are in-house heat treaters. Our customers require spotless parts and if they’re not, then we need to clean them,” explains Ott of LINAMAR GEAR.

Fritz from HEMO shares his perspective: “Heat treaters usually have their own labs to check the hardening quality. If the quality is not stable, the cleaning could be the reason. Additionally, they could send parts outside to be cleaned in a different way. Then do the hardening in their shop to see if there is a difference. In most cases, their customers tell them if the quality is not good. We are then the ones to offer our experience and take them to the next level.”

Ecoclean’s Wheeler describes their process in determining cleaning needs: “When determining the needs of a cleaning system, it is essential to understand the incoming contaminants on the part. In addition, one needs to understand which upstream manufacturing processes were used, the requirements of the heat-treating process, and which type of heat-treating process is being used. Not all cleaning systems are created equally, and not all approaches work in every scenario. For example, phosphate-coated parts coming from a stamping process will require a different cleaning system than a machined part. Working together closely with your cleaning equipment supplier is the best way to ensure that the best cleaning process is implemented for your specific application.”

How do the requirements for cleaning differ between pre- and post-heat treating?

The experts at Lindberg/MPH explain: “Pre-washing parts ahead of heat treating is needed to remove any oils or solvents that can remain on the parts. Also, some parts can hold wash water and some residue that can be carried into the furnace, and those must be blown-off or dried before the next operation.”

They continue: “Post-washing parts, particularly after oil quenching, is needed to remove any oil that might be trapped—parts such as pistons, valves, and gears with recessed areas. Most of those batch washers are fitted with a dunk or oscillation feature where the load is completely submerged, then drained and dried before moving to the tempering process. For many years, a single washer was used for both pre- and post-washing, but that practice has largely stopped.”

Nitrex’s Hemsath states, “When oil quenching in vacuum oil quench furnaces or standard integral quench furnaces, the oil is known, and it must be removed prior to temper operations. Quench oils are often difficult to remove completely, especially in hot oil quenching applications. Tempering can help with further removal of the oils, or it can make the situation worse by baking on quench oil residues into tough, difficult-to-remove deposits. With post-cleaning, the contaminants are well known, and they do not impede the heat treatment or surface engineering.” Hemsath continues, “Contaminants on the part’s pre-heat treatment must be removed for vacuum furnace operations to protect the equipment and prevent carbon pickup on the parts. Pre-contaminants must also be removed to help with processes such as gas nitriding, FNC, and low-pressure carburizing (LPC). Since LPC is a vacuum process, precleaning is more critical than with gas atmosphere carburizing, where the hot hydrogen gas can be effective at assisting with pre-cleaning of parts. However, even in atmosphere heat treating, minimizing the number of foreign substances entering the furnace on each part will help ensure a more consistent process and extend quench oil life.”

Wheeler of Ecoclean states, “Different goals and objectives drive the requirements of the pre-and post-heat treat cleaning systems. A pre-heat treat cleaning process aims to remove all contaminants produced by the upstream manufacturing process that could negatively affect the heat treating process. Without a proper pre-cleaning process, the heat treating may not be effective, parts could be damaged, and even the heat treating equipment itself could face damage. The goal of the post-heat treat cleaning system is to ensure that the final product meets the quality demands of the customer or end-use application. The needs of these systems may be driven by strict specifications which limit the number of allowable particulates and even the maximum size of each particle.”

Hamizadeh of AAM agrees that the processes are in no way similar. He says, “Drastically different. Pre-wash is intended to clean the product from any upstream contaminants, cutting fluids to provide a clean, uniform surface for process. Additionally, pre-wash is used to protect the heat treat equipment from contamination from oils and chemicals, which will have an adverse effect on lining or internal alloy components of the furnaces.”

He further explains, “Post-washers are historically built to remove the bulk quench oil from the part. However, it is more common that parts have irregular shapes, hidden holes, and geometries that make it difficult to remove trapped oils.”

“In the case of pre-cleaning, we make a difference between organic and inorganic residues,” Fritz of HEMO contends. “An old chemical says, ‘Similar dissolves similar.’ Hence, it is important to identify the residues of parts before pre-cleaning.”

He continues, “Water-based coolant should be cleaned with water and detergent because solvent would leave white spots caused by salts.”

“Oil is organic and should be removed by solvents like hydrocarbon or modified alcohol because water and oil are not a good mixture,” explains Fritz. “Anybody who first cleans an oily pan before a glass in the same bath knows that. Sometimes the parts have both kinds of residues on them due to several production processes before heat treatment. Then a hybrid cleaning machine is the perfect solution, because it first takes away the organics with solvent and then the inorganic spots with water.”

He concludes, “In the case of post-cleaning, we mainly talk about cleaning after oil quenching. In this case, water is the worst solution because the cleaning quality is not good, and the amount of wastewater is immense. A pure solvent machine is the best option for this scenario.”

How does cleaning differ between commercial heat treat shops and in-house/captive heat treat departments?

Sisson of CHTE describes the difference this way: “The need for cleaning remains the same. Captive heat treaters will have the benefit of heat treating the same parts over time and should document the contamination identified and the cleaning methods used. Frequently the parts will be coming from a machining or surface finishing operation. A discussion with the machine shop will identify the contamination.

“Commercial shops will see a wide variety of parts and should develop an incoming materials evaluation process to determine the type and extent of surface contamination. As part of this incoming material evaluation process a cleaning process should be specified for each incoming part. The process to remove grease and oil is different from corrosion products.”

How clean is clean anyway? How can one determine cleanliness? How can heat treaters identify the right cleaning method for their applications? What should they pay attention to?

“Specifications based on design and final function of the part will determine the cleanliness requirement,” Hamizadeh of AAM points out. “It is imperative to determine the cleanliness requirements prior to processing the parts. This could be surface chemical, oil contamination, or particulate allowed on part in terms of grams allowed per part or number of particles of determined size per part. Pay attention to customer contractual requirements based on RFQ or part print, or customer specs as stated in part drawings.”

“When answering this question, we need to ask ourselves: ‘What is the end goal of the cleaning process and what contaminants am I removing?’” Wheeler of Ecoclean begins. “Not all contaminants are created equally, nor will they successfully be removed using the same approach. The types of equipment, process steps, machine parameters, and chemicals used for cleaning need to be chosen carefully to ensure a successful and robust process.”

He explains: “Cleaning prior to heat treating is focused on preparing the parts for a successful heat treat, which means we need a surface free of oils, coolants, and particulates. In addition to the cleaning aspect, it is also crucial to sufficiently dry the parts before treating them to prevent damage during the heat treating process. A simple test to check for cleanliness prior to heat treat is to perform a ‘water break test,’ where clean water is rinsed across the surface with a goal of seeing a continuous film of water running across the whole part without being interrupted. A more scientific approach involves measuring the surface energy of the piece by using a contact angle measurement tool or Dyne pens.”

Wheeler clarifies: “When asking how clean the parts need to be post-heat treatment, there may be drastic differences based on customer quality requirements and the end-use of the workpiece. These requirements can range from simple visual cleanliness checks to strict maximum residual particle size limitations. The evaluation for conformity to these high-end specifications will require the use of multiple pieces of lab equipment, including expensive particle measuring and counting microscopes.” CHTE’s Sisson illustrates, “As we have seen in old movies, the butler wears white gloves and after rubbing the surface any contamination can be seen. There is a limited number of types of surface contamination for heat treaters to identify: heavy oils, light oils, cutting fluids, and corrosion products (rust and scales). Knowledge of the part history will help identify the contamination and therefore the cleaning method.

“The largest impact will be on nitriding and ferritic nitrocarburizing (FNC) processes. Surface contamination inhibits the absorption of nitrogen by interfering with the decomposition of ammonia on the steel surface. Even the grease from fingerprints can cause soft spots,” he concludes.

HEMO’s Fritz shares, “Clean can be visually clean or when you wipe a cleaned part or when a part is not dirty after the hardening process because it was cleaned well before.”

In determining cleanliness, Fritz continues, “Optically, for example, use an ink pen that shows the surface tension. A high surface tension shows a well cleaned surface.”

And finally, identifying the right cleaning method and focus: “First thing is to always identify the residues which are on the parts. If this is identified the cleaning process can be selected accordingly.”

What might be the impact for furnaces if components are not cleaned thoroughly?

Fritz of HEMO answers, “The residues vaporize and crack on the furnace walls. The walls then must be stained new in short intervals. This can be prevented by using a better cleaning system.”

“Heat treating oily parts will cause the oils to burn and fill the room with smoke and oil vapors. These gases and the smoke will deposit in the furnace and reduce performance and furnace life,” shares Sisson of CHTE.

The experts at Lindberg/MPH explain, “For many years unwashed parts were placed in tempering furnaces to burn-off the machine oils rather than washing. Over time, all that machine oil saturated the furnace brickwork or coated the heating elements, which had to be replaced much sooner than needed. Today, due to some environmental issues, that ‘smokebomb’ has become a problem, and the washer has become a sound solution and a proven benefit.”

AAM’s Hamizadeh says, “I’ve seen carburizing furnaces become contaminated with chemicals from prewash. They glazed the hard refractory into a glass and caused adhesion between silicon carbide rails and alloy base trays.” He continues: “We’ve also seen excessive smoking from temper progress to an occasional, but rare fire in a temper furnace or a more probable fire in exhaust ducts due to oil film build up.”

What cleaning options are available? What are their pros and cons?

“Traditional batch or continuous spray washers with or without dunk is an absolute minimum,” states Hamizadeh of AAM. “Other equipment such as Aichelin’s Flexiclean Vacuum washer can do a fabulous job without the use of solvents. Today—as a minimum—prewash systems should have a 3-tank system of wash, rinse & rinse, and blowoff. Post-washers should have 4-stages: 2-wash, followed by 2-rinse, and blowoff dry stage. Conventional washers are very cost-effective. Newer technology washers, with the use of advanced skimmers, multistage filtration, and ultrasonics to get the best agitation possible, will improve the capability of the machine. Dedicated and custom designed line washers perform the best, but also cost the most.”

HEMO’s Fritz shares, “I think the inline water-based dip and spray cleaners with hot air or vacuum drying are still fine for 50% of all applications in heat treatment. Anything else would be too expensive and simply not necessary. But for higher demands, more sophisticated systems are necessary. There you find top or front-loading full vacuum machines which can run water with detergent, solvents, or both.”

“For most washers, added features such as skimmers, oil traps, and dual-can type filters are very popular,” point out Lindberg/MPH experts. “These options help in keeping the washing media cleaner and free from loose metal, chips, and free carbon. The cost of these items is minimal compared to dumping several hundred gallons of water and many chemicals on a regular basis.”

They conclude, “Most washers, especially those fitted with the dunk features, are built with stainless steel tanks and all structures that are submerged in the washing solution. The extra cost for stainless steel far outweighs the cost of replacing a mild steel-lined tank or coated tank, which both have a much shorter life than the stainless-steel units.”

Apart from technical cleanliness, are there other aspects that heat treaters should consider in their choice of the right cleaning solution? Do certain materials demand specific cleaning precautions? What cleaning methods will be particularly suited to specific types of soils?

LINAMAR GEAR’S Ott says, “Washer chemistry that will remove oil and other surface contaminants and possibly leave a protective coating on the parts may be worth developing, so that flash rusting will not occur before the tempering operation.”

AAM’s Hamizadeh explains, “For specific parts and materials, specific washers with specific chemicals are needed. All parts should be compared to detergents used, temperatures, and agitation/spray pressures they can endure.”

“They should consider the quality of the final product,” Fritz of HEMO details. “They should consider environmental issues like wastewater, amount of detergent, heating energy, etc. They should consider cycle time and the degree of cleanliness required. Altogether it will lead them to a total cost of operation consideration, and they will find out that a high investment doesn’t mean higher operating cost over the lifetime of the equipment.”

He shares that “Copper and aluminum, especially, must be handled with care when selecting a way of cleaning.”

What common issues do heat treaters experience in the cleaning process? And how can these be avoided?

Nitrex’s Hemsath explains, “There are various methods for cleaning from vapor degreasing to ultrasonic methods. Each has benefits and negatives, such as environmental impact issues or cleaning of various contaminants completely. Another issue is part orientation and cost of parts handling. Continuous small parts cleaning can allow better part orientation, say, for cylinders. However, the labor content adds to costs for individual parts placement. No operation, especially commercial heat treat operations, can have all the cleaning options. It is not uncommon to hand-clean parts that are difficult to clean in a batch or continuous processes. The biggest problem is not knowing what the exact contaminants are.”

“Complex part geometries and pack density of the load are common load issues that are faced. Regular maintenance of washers—filters, skimmers, titration practices to maintain chemical balance—will all affect their performance. A regimented SPC and quality control specification should be required to ensure all work is completed and signed off by appropriate quality team members,” states Hamizadeh of AAM.

Fritz of HEMO cautions, “The biggest issue is the white layer or spots on the parts which result from inorganic residues. They pollute their water-based cleaning media with oil and other organics and then the media is not strong enough to additionally clean off the inorganics. This can cause soft spots on the surface after the hardening process. “The second big thing,” he says, “is that the cleaning quality is decreasing with every cycle. In a solvent machine with a good distillation device, you always have a constant quality.”

Have you noticed any changing requirements or expectations in terms of cleaning quality for heat treat processes over the last 5 years?

Hamizadeh of AAM answers affirmatively, “Yes. Tighter specs for amount of carry over oil or oil residue on parts.”

HEMO’s Fritz concurs, “The requirements change because the industry is changing. We go to electric vehicles, which means we need to harden new kinds of parts that are made of new kinds of materials, alloys, and composites. This means a modification of the hardening and of the cleaning process.”

Ott from LINAMAR GEAR has noticed, “Parts are compared to vacuum heat treat, so the cleanliness is very important, especially in automotive.”

What challenges do you think will confront heat treaters in the next 5 years, specifically regarding parts cleaning? Where do you see trends heading?

“Electric drive units will require a reexamination of the part washing and available technologies. It’s going to become more difficult. Not easier,” believes AAM’s Hamizadeh.

Fritz of HEMO predicts, “The main challenge will be to stay alive. With the rise of the electric car, fewer parts will be heat treated. Heat treaters must offer the best possible quality for reasonable prices in order to survive. This is not possible with the old way of cleaning.” He sees trends “. . . still going to vacuum. LPC is very strong and will be increasing. Additionally, gas and plasma nitriding will increase. Especially in those cases, a clean surface is the only way to have a reliable hardening process with consistent quality.”

Fritz concludes, “The other trend is small batches. That is the reason why we redesigned our small cleaning machines to also be able to survive in the heat treatment environment.”

“Totally clean parts,” is the challenge Ott of LINAMAR GEAR sees.

How can heat treaters balance the need for component cleanliness and cost-effectiveness for their operation?

Ecoclean’s Wheeler maintains, “When searching for the balance between cleanliness and cost, defining what costs are genuinely associated with cleaning is essential. Some of these costs may be obvious, while others may not be so clear at first glance. In too many instances, the actual lifecycle costs of owning and operating a cleaning system are not taken into consideration as the main focus is instead the upfront investment of the machine itself.

Utility costs, chemical usage, waste disposal, and maintenance are only some of the expenses that will add up over the life of a piece of equipment which may significantly impact its cost-effectiveness over an alternative solution. One example in this instance is using a vacuum solvent cleaning system over an aqueous-based machine. While the solvent system will typically come with a higher upfront purchase price, it is generally more cost effective to own in the long run when compared to the water-based system.”

Wheeler continues, “The other question that one should ask when deciding on how much to spend on a cleaning system is what the cost of purchasing the wrong system is. How much will be spent on scrapped parts, repairing damaged heat treating equipment, and downtime caused by the improper cleaning of parts? These may not always seem obvious upfront, yet they are actual costs that every manufacturer may face. While there is no one-size-fits-all approach for every company, it is essential to consider all obvious and hidden costs associated with the cleaning process when looking for the balance between price and quality.”

“For captive heat treaters,” Hemsath of Nitrex answers, “their contaminant stream is much better understood, and a solution can be custom engineered to provide repeatable results. For commercial heat treat facilities, cleaning operations have to satisfy many part sizes, orientations, and a multitude of contaminations that are often not well understood. So, the cleaning operation must be a process that gets most of the contaminants on most of the parts. Good communication with the part maker is essential to prevent problems, especially in long-term programs where the same parts are heat treated for many years.”

“They must do a total cost of operation examination of their whole process in order to find the right system,” encourages Fritz of HEMO.

These experts have spoken and offered much valuable insight into the world of parts cleaning. No longer can this process be viewed as “a non-value-added necessity of manufacturing,” as Tyler Wheeler of Ecoclean observed. Today, parts cleaning is proving to be an important component for success in heat treating.

 

For more information, contact the experts:

Fred Hamizadeh, Director of Heat Treat & Facilities Process, American Axle & Manufacturing, Fred.Hamizadeh@aam.com

Mark Hemsath, Vice President of Sales, Americas, Nitrex Heat Treating Services, mark.hemsath@nitrex.com

Tyler Wheeler, Product Line Manager, Ecoclean, Tyler.Wheeler@ecoclean-group.net

Lindberg/MPH, lindbergmph@lindbergmph.com, 269.849.2700

Andreas Fritz, CEO, HEMO GmbH, a.fritz@hemo-gmbh-de

Richard Ott, Senior Process Engineer, LINAMAR GEAR, Richard.Ott@Linamar.com

Rick Sisson, George F. Fuller Professor & Director of the Center for Heating Excellence, Worchester Polytechnic Institute, sisson@wpi.edu

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